CN103741478A - Anti-shrinkage curtain finishing liquid and preparation method thereof - Google Patents
Anti-shrinkage curtain finishing liquid and preparation method thereof Download PDFInfo
- Publication number
- CN103741478A CN103741478A CN201310687560.4A CN201310687560A CN103741478A CN 103741478 A CN103741478 A CN 103741478A CN 201310687560 A CN201310687560 A CN 201310687560A CN 103741478 A CN103741478 A CN 103741478A
- Authority
- CN
- China
- Prior art keywords
- parts
- dressing liquid
- curtain
- preparation
- shrink
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000007788 liquid Substances 0.000 title claims abstract description 31
- 238000002360 preparation method Methods 0.000 title claims abstract description 13
- 238000003756 stirring Methods 0.000 claims abstract description 21
- CQEYYJKEWSMYFG-UHFFFAOYSA-N butyl acrylate Chemical compound CCCCOC(=O)C=C CQEYYJKEWSMYFG-UHFFFAOYSA-N 0.000 claims abstract description 9
- OOCMUZJPDXYRFD-UHFFFAOYSA-L calcium;2-dodecylbenzenesulfonate Chemical compound [Ca+2].CCCCCCCCCCCCC1=CC=CC=C1S([O-])(=O)=O.CCCCCCCCCCCCC1=CC=CC=C1S([O-])(=O)=O OOCMUZJPDXYRFD-UHFFFAOYSA-L 0.000 claims abstract description 8
- 239000012153 distilled water Substances 0.000 claims abstract description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 8
- -1 poly(tributoxy titanium) Polymers 0.000 claims description 17
- 229920001230 polyarylate Polymers 0.000 claims description 7
- 238000002156 mixing Methods 0.000 abstract description 2
- BOTDANWDWHJENH-UHFFFAOYSA-N Tetraethyl orthosilicate Chemical compound CCO[Si](OCC)(OCC)OCC BOTDANWDWHJENH-UHFFFAOYSA-N 0.000 abstract 1
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 abstract 1
- 238000010438 heat treatment Methods 0.000 abstract 1
- 239000000178 monomer Substances 0.000 abstract 1
- 229920000742 Cotton Polymers 0.000 description 8
- 239000003795 chemical substances by application Substances 0.000 description 4
- 238000004140 cleaning Methods 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- 238000010028 chemical finishing Methods 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 102000000429 Factor XII Human genes 0.000 description 1
- 108010080865 Factor XII Proteins 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
Landscapes
- Detergent Compositions (AREA)
- Materials For Medical Uses (AREA)
Abstract
The invention relates to an anti-shrinkage curtain finishing liquid and a preparation method thereof, the anti-shrinkage curtain finishing liquid comprises the following components by weight: 3-5 parts of polyarylester, 2-4 parts of butyl acrylate monomer, 2-3 parts of polybutyl titanate, 5-8 parts of ethyl silicate, 6-9 parts of calcium dodecyl benzene sulfonate and 145-165 parts of distilled water. The anti-shrinkage curtain finishing liquid is prepared by the steps of mixing, heating and stirring. The prepared anti-shrinkage curtain finishing liquid has excellent function for avoiding the shrinkage of the curtain.
Description
Technical field
The present invention relates to a kind of dressing liquid and preparation method thereof, particularly relate to a kind of anti-shrink curtains dressing liquid and preparation method thereof.
Background technology
The material of curtain is more, has the materials such as cotton, silk, fiber, blending.Wherein cotton curtain has certain shrink phenomenon after cleaning.This has affected the attractive in appearance of curtain greatly.By curtain is arranged, give curtain certain anti-contractility, may reduce the shrinkage factor of curtain, extend the service time of curtain.Common finishing agent is generally the mixture of resin and some other chemical composition, after curtain is arranged with common chemical finishing agent, the anti-contractility of curtain improves and is not obvious, and the one-tenth that need to change conventional chemical finishing agent is grouped into, to improve the performance of finishing agent.
Summary of the invention
The technical problem solving: cotton curtain repeatedly cleans the problem that post-shrinkage ratio is higher.
Technical scheme: the invention discloses a kind of anti-shrink curtains dressing liquid and preparation method thereof, anti-shrink curtains dressing liquid consisting of according to weight ratio: polyarylate is that 3～5 parts, butyl acrylate are that 2～4 parts, poly(tributoxy titanium) are that 2～3 parts, silester are that 5～8 parts, calcium dodecyl benzene sulfonate are that 6～9 parts, distilled water are 145～165 parts.
A preparation method for anti-shrink curtains dressing liquid, preparation method comprises the following steps: (1) gets distilled water is 145～165 parts, is transferred in reactor capping still after being heated to 50 ℃～55 ℃; (2) opening reactor, is that 5～8 parts, calcium dodecyl benzene sulfonate are 6～9 parts to adding silester in reactor, seals stirring with dasher, stirs; (3) temperature of reaction kettle is risen to 80 ℃, then open reactor, adding wherein polyarylate is that 3～5 parts, butyl acrylate are that 2～4 parts, poly(tributoxy titanium) are 2～3 parts again, reuses dasher and seals stirring, stirs; (4) dressing liquid is incubated after 2h～3h at 80 ℃, naturally cools to room temperature, be prepared into curtain dressing liquid.
By dressing liquid is incubated to 2h～3h at 80 ℃, can promotes mutual dissolving and the reaction of composition wherein, and then improve the anti-contracility energy of curtain while arranging.
Beneficial effect: common cotton curtain is cleaning after 10 times, and shrinkage factor is 12%, arranges curtain later through dressing liquid of the present invention, and it cleans after 10 times, and shrinkage factor only has 1.7% to 2.1%.
The specific embodiment
Embodiment 1
(1) getting distilled water is 145kg, is transferred in reactor capping still after being heated to 55 ℃; (2) opening reactor, is that 8kg, calcium dodecyl benzene sulfonate are 9kg to adding silester in reactor, seals stirring with dasher, stirs; (3) temperature of reaction kettle is risen to 80 ℃, then open reactor, adding wherein polyarylate is that 3kg, butyl acrylate are that 4kg, poly(tributoxy titanium) are 3kg again, reuses dasher and seals stirring, stirs; (4) dressing liquid is incubated after 3h at 80 ℃, naturally cools to room temperature, be prepared into curtain dressing liquid.
Embodiment 2
(1) getting distilled water is 155kg, is transferred in reactor capping still after being heated to 50 ℃; (2) opening reactor, is that 5kg, calcium dodecyl benzene sulfonate are 6kg to adding silester in reactor, seals stirring with dasher, stirs; (3) temperature of reaction kettle is risen to 80 ℃, then open reactor, adding wherein polyarylate is that 5kg, butyl acrylate are that 3kg, poly(tributoxy titanium) are 2kg again, reuses dasher and seals stirring, stirs; (4) dressing liquid is incubated after 2h at 80 ℃, naturally cools to room temperature, be prepared into curtain dressing liquid.
Embodiment 3
(1) getting distilled water is 165kg, is transferred in reactor capping still after being heated to 55 ℃; (2) opening reactor, is that 7kg, calcium dodecyl benzene sulfonate are 7kg to adding silester in reactor, seals stirring with dasher, stirs; (3) temperature of reaction kettle is risen to 80 ℃, then open reactor, adding wherein polyarylate is that 4kg, butyl acrylate are that 2kg, poly(tributoxy titanium) are 3kg again, reuses dasher and seals stirring, stirs; (4) dressing liquid is incubated after 2h at 80 ℃, naturally cools to room temperature, be prepared into curtain dressing liquid.
Get two of identical pure cotton curtain, get wherein in a curtain dressing liquid that immerses embodiment 1, embodiment 2, embodiment 3 and soak after 2h, preliminary drying 40min at 80 ℃, more thoroughly dry at 105 ℃.Untrimmed cotton curtain and treated cotton curtain routine are cleaned after 10 times, measure their shrinkage factor, result is as follows.
| ? | Reference examples | Embodiment 1 | Embodiment 2 | Embodiment 3 |
| Shrinkage factor | 12% | 1.9% | 2.1% | 1.7% |
Through dressing liquid, arrange cotton curtain later, its shrinkage factor after repeatedly cleaning significantly reduces, and has effectively avoided curtain repeatedly to clean the too much problem of after-contraction and has occurred, utilization rate and the service time of having improved curtain.
Claims (5)
1. an anti-shrink curtains dressing liquid, is characterized in that anti-shrink curtains dressing liquid consisting of according to weight ratio: polyarylate is that 3～5 parts, butyl acrylate are that 2～4 parts, poly(tributoxy titanium) are that 2～3 parts, silester are that 5～8 parts, calcium dodecyl benzene sulfonate are that 6～9 parts, distilled water are 145～165 parts.
2. the preparation method of a kind of anti-shrink curtains dressing liquid according to claim 1, is characterized in that preparation method comprises the following steps: (1) gets distilled water is 145～165 parts, is transferred in reactor capping still after being heated to 50 ℃～55 ℃; (2) opening reactor, is that 5～8 parts, calcium dodecyl benzene sulfonate are 6～9 parts to adding silester in reactor, seals stirring with dasher, stirs; (3) temperature of reaction kettle is risen to 80 ℃, then open reactor, adding wherein polyarylate is that 3～5 parts, butyl acrylate are that 2～4 parts, poly(tributoxy titanium) are 2～3 parts again, reuses dasher and seals stirring, stirs; (4) dressing liquid is incubated after 2h～3h at 80 ℃, naturally cools to room temperature, be prepared into curtain dressing liquid.
3. the preparation method of a kind of anti-shrink curtains dressing liquid according to claim 2, is characterized in that the silester adding is 8 parts.
4. the preparation method of a kind of anti-shrink curtains dressing liquid according to claim 2, is characterized in that the poly(tributoxy titanium) adding is 3 parts.
5. the preparation method of a kind of anti-shrink curtains dressing liquid according to claim 2, is characterized in that the butyl acrylate adding is 2 parts.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310687560.4A CN103741478B (en) | 2013-12-17 | 2013-12-17 | A kind of resisted shrinkage curtain dressing liquid and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310687560.4A CN103741478B (en) | 2013-12-17 | 2013-12-17 | A kind of resisted shrinkage curtain dressing liquid and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103741478A true CN103741478A (en) | 2014-04-23 |
| CN103741478B CN103741478B (en) | 2015-09-23 |
Family
ID=50498538
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201310687560.4A Active CN103741478B (en) | 2013-12-17 | 2013-12-17 | A kind of resisted shrinkage curtain dressing liquid and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN103741478B (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105401411A (en) * | 2015-12-25 | 2016-03-16 | 常熟市格林染整有限公司 | Velvet fabric dyeing and finishing technology |
| CN107893329A (en) * | 2017-11-30 | 2018-04-10 | 苏州绣艳天下刺绣工艺有限公司 | A kind of preparation method embroidered with anti-shrink finishing agent |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1070238A (en) * | 1991-07-18 | 1993-03-24 | 日本纯药株式会社 | The agent composition that is used for leather, fur and fibrous material |
| CN1751153A (en) * | 2003-02-19 | 2006-03-22 | 罗狄亚化学公司 | Use of a cross-linkable liquid silicon formulation as a textile coating base |
| CN101302276A (en) * | 2008-06-16 | 2008-11-12 | 宁波润禾化学工业有限公司 | Preparation technology of soft highly-elastic fabric anti-fluffing anti-pilling finishing agent |
-
2013
- 2013-12-17 CN CN201310687560.4A patent/CN103741478B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1070238A (en) * | 1991-07-18 | 1993-03-24 | 日本纯药株式会社 | The agent composition that is used for leather, fur and fibrous material |
| CN1751153A (en) * | 2003-02-19 | 2006-03-22 | 罗狄亚化学公司 | Use of a cross-linkable liquid silicon formulation as a textile coating base |
| CN101302276A (en) * | 2008-06-16 | 2008-11-12 | 宁波润禾化学工业有限公司 | Preparation technology of soft highly-elastic fabric anti-fluffing anti-pilling finishing agent |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105401411A (en) * | 2015-12-25 | 2016-03-16 | 常熟市格林染整有限公司 | Velvet fabric dyeing and finishing technology |
| CN107893329A (en) * | 2017-11-30 | 2018-04-10 | 苏州绣艳天下刺绣工艺有限公司 | A kind of preparation method embroidered with anti-shrink finishing agent |
Also Published As
| Publication number | Publication date |
|---|---|
| CN103741478B (en) | 2015-09-23 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN103659979B (en) | A kind of thick purple willow tenderizer and preparation method thereof | |
| CN104452291A (en) | Finishing process of wool fabric | |
| CN103643510A (en) | Antibacterial finishing technique of knitted fabric | |
| CN103741478B (en) | A kind of resisted shrinkage curtain dressing liquid and preparation method thereof | |
| CN103938441B (en) | Crinis Carbonisatus wig slipping agent and preparation technology thereof and the method that wig is arranged | |
| CN104499268A (en) | Linen fabric finishing process | |
| CN103451943A (en) | Treating agent for wool fabric and preparation method of treating agent | |
| CN105064012A (en) | Finishing process for garment fabric | |
| CN103757889B (en) | Finishing agent of a kind of resisted shrinkage ANTIPILLING and preparation method thereof | |
| CN103741452A (en) | Shirt finishing liquid and preparation method | |
| CN105542982A (en) | Liquid laundry detergent | |
| CN105369595A (en) | Production process of velcro cloth | |
| CN103757895B (en) | A kind of cotton dress dressing liquid and preparation method thereof | |
| CN102167996B (en) | Wig shampoo, preparation process thereof, and method for clearing up wig | |
| CN105019269A (en) | Cloth dyeing method | |
| CN105506972A (en) | Dyeing and finishing process for cotton shell fabric | |
| CN105506994A (en) | Coral fleece fabric | |
| CA2880042C (en) | Continuous process to make amine oxide | |
| CN105544254A (en) | Special cleaning solution for dyed fabrics | |
| CN103643509A (en) | Antibacterial finishing technique of knitted fabric | |
| CN103410002B (en) | Woolen sweater treating fluid containing polyoxyethylene glycol bisstearate | |
| CN105484038A (en) | Composite fabric dyeing and finishing process | |
| CN108221359A (en) | A kind of preparation process of the composite fibre with anti-mite function | |
| CN105525508A (en) | Garment fabric dyeing and finishing process | |
| CN103696231A (en) | Ultraviolet-proof finishing process of dacron knitted fabric |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| ASS | Succession or assignment of patent right |
Owner name: GU XIANGMAO Free format text: FORMER OWNER: GOLDSUN HOLDING GROUP CO., LTD. Effective date: 20150828 |
|
| C41 | Transfer of patent application or patent right or utility model | ||
| TA01 | Transfer of patent application right |
Effective date of registration: 20150828 Address after: 266000 Licang, Qingdao, No. nine East water road, No. 320, No. Applicant after: Gu Xiangmao Address before: 226300 Jiangsu city of Nantong province Tongzhou District Industrial Park building sun Zhihao Applicant before: Goldsun Holding Group Co., Ltd. |
|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CP02 | Change in the address of a patent holder | ||
| CP02 | Change in the address of a patent holder |
Address after: 225327 Jiangsu city of Taizhou province Yongan high port Zhou Zhen rain Road No. 26 Patentee after: Gu Xiangmao Address before: 266000 Licang, Qingdao, No. nine East water road, No. 320, No. Patentee before: Gu Xiangmao |
|
| CP02 | Change in the address of a patent holder | ||
| CP02 | Change in the address of a patent holder |
Address after: Tian Zhen Qing Guan Lu Pingdu City 266700 Shandong city of Qingdao province No. 11 Patentee after: Gu Xiangmao Address before: 225327 Jiangsu city of Taizhou province Yongan high port Zhou Zhen rain Road No. 26 Patentee before: Gu Xiangmao |
|
| CP02 | Change in the address of a patent holder | ||
| CP02 | Change in the address of a patent holder |
Address after: 210000 Longshi Center, No. 2 Guangzhou Road (221 Central Road), Gulou District, Nanjing City, Jiangsu Province Patentee after: Gu Xiangmao Address before: 266700 11 Tsing Guan Road, Tian Zhuang Town, Pingdu City, Qingdao, Shandong Patentee before: Gu Xiangmao |
|
| TR01 | Transfer of patent right | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20191012 Address after: 314000 Fengming Street Industrial Park, Tongxiang City, Jiaxing City, Zhejiang Province Patentee after: Zhejiang Jiaming dyeing and finishing Co., Ltd. Address before: 210000 Longshi center, No. 2, Guangzhou road, Gulou District, Nanjing City, Jiangsu Province Patentee before: Gu Xiang Mao |