CN103757889A - Shrinkage and pilling resistant finishing agent and preparation method thereof - Google Patents

Shrinkage and pilling resistant finishing agent and preparation method thereof Download PDF

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Publication number
CN103757889A
CN103757889A CN201310750885.2A CN201310750885A CN103757889A CN 103757889 A CN103757889 A CN 103757889A CN 201310750885 A CN201310750885 A CN 201310750885A CN 103757889 A CN103757889 A CN 103757889A
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parts
finishing agent
antipilling
contraction
preparation
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CN201310750885.2A
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CN103757889B (en
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张德轩
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Wujiang Dingneng textile finishing Co., Ltd
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SUZHOU XUANDE TEXTILE SCIENCE & TECHNOLOGY Co Ltd
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Abstract

The invention provides a shrinkage and pilling resistant finishing agent and a preparation method thereof. The shrinkage and pilling resistant finishing agent comprises the following components in parts by weight: 4-6 parts of petroleum sodium sulfonate, 1-2 parts of polypropylene glycol diglycidyl ether, 3-5 parts of alanine, 2-3 parts of dioctadecyl dimethyl ammonium chloride, 7-8 parts of pentanol, 2-3 parts of potassium phosphate, 1-2 parts of sodium sulfate and 230-240 parts of water. The finishing agent is prepared by mixing and stirring the components of the finishing agent. The prepared finishing agent can be used for finishing cotton clothes and can endow the cotton clothes with good shrinkage and pilling resistance.

Description

Finishing agent of a kind of anti-contraction ANTIPILLING and preparation method thereof
Technical field
The present invention relates to a kind of preparation method of finishing agent and finishing agent thereof of clothing, particularly relate to a kind of have the clothing finishing agent of anti-contraction, anti-pilling property and the preparation method of finishing agent.
Background technology
Conventional clothing, after repeatedly being cleaned, all can have the shrink phenomenon of part to produce.Cause reason that clothing shrinks to have a variety of, the fiber of for example clothing own, after repeatedly cleaning, wrapping phenomena occurring, also has certain metaboly simultaneously.Some clothing does not arrange through the finishing agent of special anti-contraction, therefore has certain shrink phenomenon and occurs.If cotton dress is in the process of dress, too much rubs with the external world, after the time is long, also can produce very serious pilling effect.Pilling effect affects the attractive in appearance of fabric very much, reduces the pilling effect of fabric after repeatedly rubbing, also extremely important.In sum, the raising anti-contraction of clothing and the performance of ANTIPILLING are very necessary.
Summary of the invention
The technical problem solving: common clothing does not have the performance of good anti-contraction and ANTIPILLING, the problem that clothing can significantly shrink after repeatedly cleaning, pilling effect is serious.
Technical scheme: the invention discloses a kind of finishing agent of anti-contraction ANTIPILLING, the finishing agent of anti-contraction ANTIPILLING is comprised of according to weight ratio following composition: petroleum sodium sulfonate is that 4~6 parts, polypropylene glycol diglycidyl ether are that 1~2 part, alanine are that 3~5 parts, dioctadecyl dimethyl ammonium chloride are that 2~3 parts, amylalcohol are that 7~8 parts, potassium phosphate are that 2~3 parts, sodium sulphate are that 1~2 part, water are 230~240 parts.
A kind of preparation method of finishing agent of anti-contraction ANTIPILLING, preparation method comprises the following steps: (1) gets petroleum sodium sulfonate is that 4~6 parts, polypropylene glycol diglycidyl ether are that 1~2 part, dioctadecyl dimethyl ammonium chloride are 2~3 parts, by mixing and stir after three kinds of composition heating, mix rear standby; (2) water intaking is 230~240 parts, then to add alanine be that 3~5 parts, amylalcohol are that 7~8 parts, potassium phosphate are that 2~3 parts, sodium sulphate are 1~2 part, and alanine, amylalcohol, potassium sulfate, sodium sulphate water are uniformly dissolved; (3) mixed liquor preparing in step (1) is added in the aqueous solution in step (2), stir with mechanical agitation oar, speed of agitator is 200~250rpm, stirs; (4) finally finishing agent is packed in hermetically sealed can, preserve.
Beneficial effect: after cotton clothing is arranged with dressing liquid of the present invention, cotton clothing only has 0.2% to 0.5% at 20 post-shrinkage ratios of washing, and the ANTIPILLING grade of cotton clothing is 4 to 5 grades, has good anti-contraction and the performance of ANTIPILLING.
The specific embodiment
Embodiment 1
(1) getting petroleum sodium sulfonate is that 4kg, polypropylene glycol diglycidyl ether are that 2kg, dioctadecyl dimethyl ammonium chloride are 3kg, by mixing and stir after three kinds of composition heating, mixes rear standby; (2) water intaking is for 230kg, then to add alanine be that 3kg, amylalcohol are that 8kg, potassium phosphate are that 2kg, sodium sulphate are 2kg, and alanine, amylalcohol, potassium sulfate, sodium sulphate water are uniformly dissolved; (3) mixed liquor preparing in step (1) is added in the aqueous solution in step (2), stir with mechanical agitation oar, speed of agitator is 200rpm, stirs; (4) finally finishing agent is packed in hermetically sealed can, preserve.
Embodiment 2
(1) getting petroleum sodium sulfonate is that 6kg, polypropylene glycol diglycidyl ether are that 1kg, dioctadecyl dimethyl ammonium chloride are 2kg, by mixing and stir after three kinds of composition heating, mixes rear standby; (2) water intaking is for 235kg, then to add alanine be that 5kg, amylalcohol are that 7kg, potassium phosphate are that 3kg, sodium sulphate are 1kg, and alanine, amylalcohol, potassium sulfate, sodium sulphate water are uniformly dissolved; (3) mixed liquor preparing in step (1) is added in the aqueous solution in step (2), stir with mechanical agitation oar, speed of agitator is 250rpm, stirs; (4) finally finishing agent is packed in hermetically sealed can, preserve.
Embodiment 3
(1) getting petroleum sodium sulfonate is that 5kg, polypropylene glycol diglycidyl ether are that 2kg, dioctadecyl dimethyl ammonium chloride are 2kg, by mixing and stir after three kinds of composition heating, mixes rear standby; (2) water intaking is for 240kg, then to add alanine be that 4kg, amylalcohol are that 8kg, potassium phosphate are that 2kg, sodium sulphate are 1kg, and alanine, amylalcohol, potassium sulfate, sodium sulphate water are uniformly dissolved; (3) mixed liquor preparing in step (1) is added in the aqueous solution in step (2), stir with mechanical agitation oar, speed of agitator is 230rpm, stirs; (4) finally finishing agent is packed in hermetically sealed can, preserve.
By textile clothes, dry after soaking 50min under the finishing agent room temperature with embodiment 1, embodiment 2, embodiment 3.Dry rear with washing machine cleaning 20 times.Shrinkage factor and the ANTIPILLING grade of measuring cotton clothes arrangement front and back, pilling grade bioassay standard is GB/T4802.2-1997.Test result is as following table.
? Reference examples Embodiment 1 Embodiment 2 Embodiment 3
Shrinkage factor 13% 0.2% 0.4% 0.5%
ANTIPILLING grade 1 grade 5 grades 4 grades 5 grades
After cotton clothes arranges through finishing agent, possessed excellent anti-contraction and the performance of ANTIPILLING.

Claims (5)

1. a finishing agent for anti-contraction ANTIPILLING, is characterized in that the finishing agent of anti-contraction ANTIPILLING is comprised of according to weight ratio following composition: petroleum sodium sulfonate is that 4~6 parts, polypropylene glycol diglycidyl ether are that 1~2 part, alanine are that 3~5 parts, dioctadecyl dimethyl ammonium chloride are that 2~3 parts, amylalcohol are that 7~8 parts, potassium phosphate are that 2~3 parts, sodium sulphate are that 1~2 part, water are 230~240 parts.
2. the preparation method of the finishing agent of a kind of anti-contraction ANTIPILLING according to claim 1, it is characterized in that preparation method comprises the following steps: (1) gets petroleum sodium sulfonate is that 4~6 parts, polypropylene glycol diglycidyl ether are that 1~2 part, dioctadecyl dimethyl ammonium chloride are 2~3 parts, by mixing and stir after three kinds of composition heating, mix rear standby; (2) water intaking is 230~240 parts, then to add alanine be that 3~5 parts, amylalcohol are that 7~8 parts, potassium phosphate are that 2~3 parts, sodium sulphate are 1~2 part, and alanine, amylalcohol, potassium sulfate, sodium sulphate water are uniformly dissolved; (3) mixed liquor preparing in step (1) is added in the aqueous solution in step (2), stir with mechanical agitation oar, speed of agitator is 200~250rpm, stirs; (4) finally finishing agent is packed in hermetically sealed can, preserve.
3. the preparation method of the finishing agent of a kind of anti-contraction ANTIPILLING according to claim 2, is characterized in that the polypropylene glycol diglycidyl ether adding is 2 parts.
4. the preparation method of the finishing agent of a kind of anti-contraction ANTIPILLING according to claim 2, it is characterized in that adding alanine is 3 parts.
5. the preparation method of the finishing agent of a kind of anti-contraction ANTIPILLING according to claim 2, is characterized in that speed of agitator is 250rpm.
CN201310750885.2A 2013-12-31 2013-12-31 Finishing agent of a kind of resisted shrinkage ANTIPILLING and preparation method thereof Active CN103757889B (en)

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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105220496A (en) * 2015-09-29 2016-01-06 江苏金太阳纺织科技有限公司 A kind ofly improve the composition of all-cotton fabric anti-fuzz balls performance and anti-fuzz balls finishing technique
CN105484030A (en) * 2015-12-29 2016-04-13 绍兴海神印染制衣有限公司 Post-treatment technology for all-cotton fabric
CN106319952A (en) * 2016-08-19 2017-01-11 常熟市鑫博伟针纺织有限公司 After-finishing process of brushed fabric
CN106958144A (en) * 2017-05-24 2017-07-18 东台市联翔纺织有限公司 It is a kind of to prevent the textile material of balling-up
CN107893329A (en) * 2017-11-30 2018-04-10 苏州绣艳天下刺绣工艺有限公司 A kind of preparation method embroidered with anti-shrink finishing agent

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1363736A (en) * 2001-02-09 2002-08-14 广东溢达针织有限公司 Technology for knitting washing-resistant cotton fabric without ironing
CN1673444A (en) * 2005-03-08 2005-09-28 张家港市国泰华荣化工新材料有限公司 Synthesis method for anti-napping and anti-pilling conditioning agent for fabric
CN1687513A (en) * 2005-03-29 2005-10-26 东华大学 Method for fabricating wool keratin clad acrylon, polypropylene, capron and textiles
CN101302276A (en) * 2008-06-16 2008-11-12 宁波润禾化学工业有限公司 Preparation technology of soft highly-elastic fabric anti-fluffing anti-pilling finishing agent
CN102154828A (en) * 2011-03-22 2011-08-17 互太(番禺)纺织印染有限公司 Fluff resistant and pilling resistant cotton and elastic cotton knitted fabric and production method thereof

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1363736A (en) * 2001-02-09 2002-08-14 广东溢达针织有限公司 Technology for knitting washing-resistant cotton fabric without ironing
CN1673444A (en) * 2005-03-08 2005-09-28 张家港市国泰华荣化工新材料有限公司 Synthesis method for anti-napping and anti-pilling conditioning agent for fabric
CN1687513A (en) * 2005-03-29 2005-10-26 东华大学 Method for fabricating wool keratin clad acrylon, polypropylene, capron and textiles
CN101302276A (en) * 2008-06-16 2008-11-12 宁波润禾化学工业有限公司 Preparation technology of soft highly-elastic fabric anti-fluffing anti-pilling finishing agent
CN102154828A (en) * 2011-03-22 2011-08-17 互太(番禺)纺织印染有限公司 Fluff resistant and pilling resistant cotton and elastic cotton knitted fabric and production method thereof

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105220496A (en) * 2015-09-29 2016-01-06 江苏金太阳纺织科技有限公司 A kind ofly improve the composition of all-cotton fabric anti-fuzz balls performance and anti-fuzz balls finishing technique
CN105484030A (en) * 2015-12-29 2016-04-13 绍兴海神印染制衣有限公司 Post-treatment technology for all-cotton fabric
CN105484030B (en) * 2015-12-29 2017-09-29 绍兴海神印染制衣有限公司 A kind of aftertreatment technology of all-cotton fabric
CN106319952A (en) * 2016-08-19 2017-01-11 常熟市鑫博伟针纺织有限公司 After-finishing process of brushed fabric
CN106958144A (en) * 2017-05-24 2017-07-18 东台市联翔纺织有限公司 It is a kind of to prevent the textile material of balling-up
CN107893329A (en) * 2017-11-30 2018-04-10 苏州绣艳天下刺绣工艺有限公司 A kind of preparation method embroidered with anti-shrink finishing agent

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Inventor after: Zhang Dexuan

Inventor after: Zuo Donghua

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Effective date of registration: 20191223

Address after: 215200 Da Xie village, Shengze Town, Wujiang District, Suzhou, Jiangsu

Patentee after: Wujiang Dingneng textile finishing Co., Ltd

Address before: 7 groups of friendship village Songling town of Wujiang District of Suzhou City, Jiangsu province 215200 split eight community

Patentee before: SUZHOU XUANDE TEXTILE SCIENCE & TECHNOLOGY CO., LTD.