CN103755483A - Special controlled-release fertilizer for summer maize and production method thereof - Google Patents
Special controlled-release fertilizer for summer maize and production method thereof Download PDFInfo
- Publication number
- CN103755483A CN103755483A CN201410053926.7A CN201410053926A CN103755483A CN 103755483 A CN103755483 A CN 103755483A CN 201410053926 A CN201410053926 A CN 201410053926A CN 103755483 A CN103755483 A CN 103755483A
- Authority
- CN
- China
- Prior art keywords
- fertilizer
- production method
- coating
- urea
- granulation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000003337 fertilizer Substances 0.000 title claims abstract description 50
- 235000002017 Zea mays subsp mays Nutrition 0.000 title claims abstract description 21
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 14
- 240000008042 Zea mays Species 0.000 title abstract description 19
- 238000013270 controlled release Methods 0.000 title abstract description 4
- 235000016383 Zea mays subsp huehuetenangensis Nutrition 0.000 title abstract 4
- 235000009973 maize Nutrition 0.000 title abstract 4
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 claims abstract description 16
- 239000004202 carbamide Substances 0.000 claims abstract description 16
- WCUXLLCKKVVCTQ-UHFFFAOYSA-M Potassium chloride Chemical compound [Cl-].[K+] WCUXLLCKKVVCTQ-UHFFFAOYSA-M 0.000 claims abstract description 14
- LFVGISIMTYGQHF-UHFFFAOYSA-N ammonium dihydrogen phosphate Chemical compound [NH4+].OP(O)([O-])=O LFVGISIMTYGQHF-UHFFFAOYSA-N 0.000 claims abstract description 13
- 235000019837 monoammonium phosphate Nutrition 0.000 claims abstract description 13
- 229910000387 ammonium dihydrogen phosphate Inorganic materials 0.000 claims abstract description 12
- 239000006012 monoammonium phosphate Substances 0.000 claims abstract description 12
- NWONKYPBYAMBJT-UHFFFAOYSA-L zinc sulfate Chemical compound [Zn+2].[O-]S([O-])(=O)=O NWONKYPBYAMBJT-UHFFFAOYSA-L 0.000 claims abstract description 11
- 229910000368 zinc sulfate Inorganic materials 0.000 claims abstract description 11
- 229960001763 zinc sulfate Drugs 0.000 claims abstract description 11
- SVPXDRXYRYOSEX-UHFFFAOYSA-N bentoquatam Chemical compound O.O=[Si]=O.O=[Al]O[Al]=O SVPXDRXYRYOSEX-UHFFFAOYSA-N 0.000 claims abstract description 10
- 229910021538 borax Inorganic materials 0.000 claims abstract description 10
- 239000011790 ferrous sulphate Substances 0.000 claims abstract description 10
- 235000003891 ferrous sulphate Nutrition 0.000 claims abstract description 10
- BAUYGSIQEAFULO-UHFFFAOYSA-L iron(2+) sulfate (anhydrous) Chemical compound [Fe+2].[O-]S([O-])(=O)=O BAUYGSIQEAFULO-UHFFFAOYSA-L 0.000 claims abstract description 10
- 229910000359 iron(II) sulfate Inorganic materials 0.000 claims abstract description 10
- 239000000395 magnesium oxide Substances 0.000 claims abstract description 10
- CPLXHLVBOLITMK-UHFFFAOYSA-N magnesium oxide Inorganic materials [Mg]=O CPLXHLVBOLITMK-UHFFFAOYSA-N 0.000 claims abstract description 10
- AXZKOIWUVFPNLO-UHFFFAOYSA-N magnesium;oxygen(2-) Chemical compound [O-2].[Mg+2] AXZKOIWUVFPNLO-UHFFFAOYSA-N 0.000 claims abstract description 10
- 239000002245 particle Substances 0.000 claims abstract description 10
- 239000004328 sodium tetraborate Substances 0.000 claims abstract description 10
- 235000010339 sodium tetraborate Nutrition 0.000 claims abstract description 10
- MKGIQRNAGSSHRV-UHFFFAOYSA-N 1,1-dimethyl-4-phenylpiperazin-1-ium Chemical compound C1C[N+](C)(C)CCN1C1=CC=CC=C1 MKGIQRNAGSSHRV-UHFFFAOYSA-N 0.000 claims abstract 5
- 239000000463 material Substances 0.000 claims description 41
- 239000011248 coating agent Substances 0.000 claims description 22
- 238000000576 coating method Methods 0.000 claims description 19
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims description 18
- 235000005824 Zea mays ssp. parviglumis Nutrition 0.000 claims description 17
- 235000005822 corn Nutrition 0.000 claims description 17
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 claims description 16
- 229920002125 Sokalan® Polymers 0.000 claims description 16
- 239000004584 polyacrylic acid Substances 0.000 claims description 16
- 239000011591 potassium Substances 0.000 claims description 16
- 229910052700 potassium Inorganic materials 0.000 claims description 16
- 238000001035 drying Methods 0.000 claims description 13
- 238000005469 granulation Methods 0.000 claims description 10
- 230000003179 granulation Effects 0.000 claims description 10
- 229910052759 nickel Inorganic materials 0.000 claims description 9
- PXHVJJICTQNCMI-UHFFFAOYSA-N nickel Substances [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 claims description 9
- 238000001816 cooling Methods 0.000 claims description 8
- 239000008187 granular material Substances 0.000 claims description 7
- 238000012216 screening Methods 0.000 claims description 6
- 210000000582 semen Anatomy 0.000 claims description 6
- 238000012856 packing Methods 0.000 claims description 5
- 238000013467 fragmentation Methods 0.000 claims description 4
- 238000006062 fragmentation reaction Methods 0.000 claims description 4
- 238000009479 steam granulation Methods 0.000 claims description 4
- 238000003756 stirring Methods 0.000 claims description 4
- 238000002156 mixing Methods 0.000 claims description 3
- 239000011343 solid material Substances 0.000 claims description 3
- 238000005507 spraying Methods 0.000 claims description 3
- 241000209149 Zea Species 0.000 claims 2
- 239000000618 nitrogen fertilizer Substances 0.000 abstract description 11
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 abstract description 6
- 229910052757 nitrogen Inorganic materials 0.000 abstract description 4
- -1 enricher Chemical compound 0.000 abstract description 2
- 230000002035 prolonged effect Effects 0.000 abstract 2
- IIZPXYDJLKNOIY-JXPKJXOSSA-N 1-palmitoyl-2-arachidonoyl-sn-glycero-3-phosphocholine Chemical compound CCCCCCCCCCCCCCCC(=O)OC[C@H](COP([O-])(=O)OCC[N+](C)(C)C)OC(=O)CCC\C=C/C\C=C/C\C=C/C\C=C/CCCCC IIZPXYDJLKNOIY-JXPKJXOSSA-N 0.000 abstract 1
- 239000000440 bentonite Substances 0.000 abstract 1
- 229910000278 bentonite Inorganic materials 0.000 abstract 1
- 235000013877 carbamide Nutrition 0.000 abstract 1
- 239000000787 lecithin Substances 0.000 abstract 1
- 229940067606 lecithin Drugs 0.000 abstract 1
- 235000010445 lecithin Nutrition 0.000 abstract 1
- LGQLOGILCSXPEA-UHFFFAOYSA-L nickel sulfate Chemical compound [Ni+2].[O-]S([O-])(=O)=O LGQLOGILCSXPEA-UHFFFAOYSA-L 0.000 abstract 1
- 229910000363 nickel(II) sulfate Inorganic materials 0.000 abstract 1
- 239000001103 potassium chloride Substances 0.000 abstract 1
- 235000011164 potassium chloride Nutrition 0.000 abstract 1
- 229920005614 potassium polyacrylate Polymers 0.000 abstract 1
- 239000002689 soil Substances 0.000 description 11
- 230000000694 effects Effects 0.000 description 10
- LXKCHCXZBPLTAE-UHFFFAOYSA-N 3,4-dimethyl-1H-pyrazole phosphate Chemical compound OP(O)(O)=O.CC1=CNN=C1C LXKCHCXZBPLTAE-UHFFFAOYSA-N 0.000 description 7
- 229910052698 phosphorus Inorganic materials 0.000 description 4
- WURBVZBTWMNKQT-UHFFFAOYSA-N 1-(4-chlorophenoxy)-3,3-dimethyl-1-(1,2,4-triazol-1-yl)butan-2-one Chemical compound C1=NC=NN1C(C(=O)C(C)(C)C)OC1=CC=C(Cl)C=C1 WURBVZBTWMNKQT-UHFFFAOYSA-N 0.000 description 3
- 235000015097 nutrients Nutrition 0.000 description 3
- 239000002994 raw material Substances 0.000 description 3
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 2
- 238000010521 absorption reaction Methods 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- 230000036512 infertility Effects 0.000 description 2
- 208000000509 infertility Diseases 0.000 description 2
- 231100000535 infertility Toxicity 0.000 description 2
- 238000002386 leaching Methods 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 244000005700 microbiome Species 0.000 description 2
- 235000016709 nutrition Nutrition 0.000 description 2
- 230000035764 nutrition Effects 0.000 description 2
- 239000011574 phosphorus Substances 0.000 description 2
- 238000012360 testing method Methods 0.000 description 2
- PXFBZOLANLWPMH-UHFFFAOYSA-N 16-Epiaffinine Natural products C1C(C2=CC=CC=C2N2)=C2C(=O)CC2C(=CC)CN(C)C1C2CO PXFBZOLANLWPMH-UHFFFAOYSA-N 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- GICXAEXCAZHIEE-UHFFFAOYSA-N P.[K+] Chemical group P.[K+] GICXAEXCAZHIEE-UHFFFAOYSA-N 0.000 description 1
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 1
- YUWBVKYVJWNVLE-UHFFFAOYSA-N [N].[P] Chemical compound [N].[P] YUWBVKYVJWNVLE-UHFFFAOYSA-N 0.000 description 1
- WZLMXYBCAZZIRQ-UHFFFAOYSA-N [N].[P].[K] Chemical compound [N].[P].[K] WZLMXYBCAZZIRQ-UHFFFAOYSA-N 0.000 description 1
- 239000013543 active substance Substances 0.000 description 1
- PPBAJDRXASKAGH-UHFFFAOYSA-N azane;urea Chemical compound N.NC(N)=O PPBAJDRXASKAGH-UHFFFAOYSA-N 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000009395 breeding Methods 0.000 description 1
- 230000001488 breeding effect Effects 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 239000003245 coal Substances 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000000280 densification Methods 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 230000018109 developmental process Effects 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 239000003995 emulsifying agent Substances 0.000 description 1
- 239000000839 emulsion Substances 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 210000003608 fece Anatomy 0.000 description 1
- 230000035558 fertility Effects 0.000 description 1
- 238000011049 filling Methods 0.000 description 1
- 239000007888 film coating Substances 0.000 description 1
- 238000009501 film coating Methods 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 239000004021 humic acid Substances 0.000 description 1
- 230000003993 interaction Effects 0.000 description 1
- 238000003973 irrigation Methods 0.000 description 1
- 230000002262 irrigation Effects 0.000 description 1
- 239000003077 lignite Substances 0.000 description 1
- 239000010871 livestock manure Substances 0.000 description 1
- 238000012423 maintenance Methods 0.000 description 1
- 231100000252 nontoxic Toxicity 0.000 description 1
- 230000003000 nontoxic effect Effects 0.000 description 1
- 230000000704 physical effect Effects 0.000 description 1
- 229940072033 potash Drugs 0.000 description 1
- BWHMMNNQKKPAPP-UHFFFAOYSA-L potassium carbonate Substances [K+].[K+].[O-]C([O-])=O BWHMMNNQKKPAPP-UHFFFAOYSA-L 0.000 description 1
- 235000015320 potassium carbonate Nutrition 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 230000007226 seed germination Effects 0.000 description 1
- 230000004083 survival effect Effects 0.000 description 1
- 239000011573 trace mineral Substances 0.000 description 1
- 235000013619 trace mineral Nutrition 0.000 description 1
- 230000001131 transforming effect Effects 0.000 description 1
- 230000017260 vegetative to reproductive phase transition of meristem Effects 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
- 239000011701 zinc Substances 0.000 description 1
Landscapes
- Fertilizers (AREA)
Abstract
The invention discloses a special controlled-release fertilizer for the summer maize and a production method of the special controlled-release fertilizer. The urea, monoammonium phosphate, potassium chloride, enricher, bentonite, magnesium oxide, zinc sulfate, ferrous sulfate, nickelous sulfate, borax and DMPP (dimethyl-phenyl-piperazinium) are pelleted to form inner-layer particles, and the outer layer is coated with lecithin/potassium polyacrylate. The fertilizer efficiency of the nitrogen fertilizer is prolonged from about 15 days to 100 days, and in addition, the fertilizer is released in a concentrated manner in the huge trumpet period of the maize, the fertilizer efficiency of the nitrogen fertilizer is prolonged greatly, and the nitrogen use efficiency of the summer maize is greatly increased.
Description
Technical field
The present invention relates to a kind of summer corn special-purpose control-release fertilizer and production method thereof, belong to technical field of fertilizers.
Background technology
About Huanghe valley summer corn general 100 days breeding times, needing fertile critical period be the typhon mouth phase, i.e. after planting (fertilizer efficiency period of urea is about 15 days) about 40 days.How by slow control film-coating technique, to realize a base and execute solution summer corn fertilizer in time of infertility needs, and nitrogenous fertilizer is concentrated release of typhon mouth phase, how to reduce cost of labor, is still one of important problem facing in production.
Utilize the coating agent such as macromolecular material to keep nitrogenous fertilizer, controlling and transforming gentle On The Drug Release is the important directions that improves fertilizer utilization efficiency.In agriculture production reality, coated fertilizer and nitrogenous fertilizer are usually used in conjunction with.But because the proportioning of dissimilar coated fertilizer and nitrogen fertilizers is unreasonable, cause coated fertilizer drought-resistant water-preserving effect to reduce, nitrogenous fertilizer maintenance and utilising efficiency are not high, affect to a certain extent the effect performance of coated fertilizer.Rationally application coated fertilizer can improve soil physical property, promotes seed germination and survival rate, reduces irrigation demand.Studies have shown that suitable coated fertilizer significantly reduces urea ammonia volatilization amount, and it is more obvious with macromolecular material consumption, to increase effect.
Summary of the invention
The present invention solves the deficiency that prior art exists, and a kind of summer corn special-purpose control-release fertilizer and production method thereof are provided, and the method is simple, and coating is effective, and fertilizer efficiency period is long, balanced in nutrition, and utilization rate of fertilizer is high, and safety and environmental protection, production cost are low, and fertilizer efficiency is remarkable.
Solving this technical problem adopted technical scheme is: a kind of summer corn special-purpose control-release fertilizer, it is characterized in that, it is with urea, monoammonium phosphate, Repone K, excellent of spy, wilkinite, magnesium oxide, zinc sulfate, ferrous sulfate, the sub-nickel of sulfuric acid, borax and DMPP(3,4-dimethyl pyrazole phosphoric acid salt) carry out forming inner layer granule after granulation; Outer with Yelkin TTS/polyacrylic acid potassium coating; The component of described inner layer granule and weight part are: urea 550～600, monoammonium phosphate 150～200, Repone K 150～200, special excellent 35, wilkinite 50, magnesium oxide 50, zinc sulfate 5, ferrous sulfate 2, the sub-nickel 2 of sulfuric acid, borax 1, DMPP 2; The component of described coated fertilizer and weight part are: Yelkin TTS 18, polyacrylic acid potassium 10 and Oleum Gossypii semen 32; The mass ratio of described inner layer granule and coated fertilizer is 100:5.5-6.5.
Production method, specific as follows:
(1) by following weight parts, take each raw material: urea 550～600, monoammonium phosphate 150～200, Repone K 150～200, special excellent 35, wilkinite 50, magnesium oxide 50, zinc sulfate 5, ferrous sulfate 2, the sub-nickel 2 of sulfuric acid, borax 1 and DMPP 2; The wherein content of main raw material: monoammonium phosphate (N 11%, P
2o
544%), Repone K (K
2o>=60%), urea (N>=46%); Special excellent is the good soil improvement agent of Taiwan Xing Nong company development and production, and effective constituent derives from 10% humic acids of weathered coal, brown coal.
First urea and DMPP are mixed, pulverized; Then add monoammonium phosphate, Repone K, excellent of spy, wilkinite, magnesium oxide, zinc sulfate, ferrous sulfate, the sub-nickel of sulfuric acid and borax, after mixing, form solid materials, then after crusher in crushing, enter rotary drum steam granulation machine granulation (vapour pressure 1.2 normal atmosphere);
(2) by conveying belt, the material input drying machine after granulation is dried, then sends into cooler and carry out cooling; 205 ~ 255 ℃ of described drying machine temperature ins, 65 ~ 85 ℃ of dry outlet material temperature; 45 ± 5 ℃ of described cooler outlet material temperature;
(3) by cooled material inputted vibration sieve, carry out the first screening, particle diameter is between the material input coating machine of 1-4mm, and all the other turn back to the crusher fragmentation again of step (1);
(4) coated fertilizer Yelkin TTS, polyacrylic acid potassium and Oleum Gossypii semen being poured in stirred pot by weight 18:10:32, after stirring is mixed, is 100:5.5-6.5 according to material and coating agent weight ratio, by hydro-pump, squeezes into coating machine spraying coating;
(5) input of the material after coating drying machine is dried, and then sends into cooler and carries out cooling; 185 ~ 200 ℃ of described drying machine temperature ins, 65 ~ 85 ℃ of dry outlet material temperature; 45 ± 5 ℃ of described cooler outlet material temperature;
(6) dried material inputted vibration sieve, sieves for the second time, is divided into macrobead, middle particle and three kinds of specifications of small-particle; Then metering packing warehouse-in.
The present invention, by polyacrylic acid potassium (A), Yelkin TTS/polyacrylic acid potassium (B) and 3 kinds of materials of Yelkin TTS (C) are kept to the research of effect rule to soil moisture, nitrogen phosphorus nutrient, finds that A type macromolecular material keeps effect best to soil moisture and phosphorus element; Type B macromolecular material is close, and C type macromolecular material effect is poor, and accumulative total leaching amount reduces 54%, 47% and 28% than contrast (normal soil) respectively; And to soil nitrogen, Type B macromolecular material fertilizer conservation effect is best, C type macromolecular material takes second place, and A type macromolecular material is the poorest, and accumulative total leaching amount reduces 79%, 77% and 54% than contrast (normal soil) respectively.Therefore select Yelkin TTS/polyacrylic acid potassium as coated fertilizer.
The invention has the beneficial effects as follows:
(1) coating agent-Yelkin TTS/polyacrylic acid potassium that the present invention uses, natural, nontoxic, pollution-free, nuisanceless, and can provide C, N and P source for soil microorganisms, and improve the structure of community of soil microorganisms, indirectly increase soil fertility;
(2) Yelkin TTS/polyacrylic acid potassium is a kind of tensio-active agent, emulsifying agent and water-holding agent preferably; not only water-soluble but also be dissolved in oil; reducing the water capillary while of oil, can on this bed interface, form the interfacial film of one deck densification, the particle disperseing is being had to provide protection.Because the effects such as the absorption of Yelkin TTS/polyacrylic acid potassium and friction make drop band point, band point drop forms double electrical layers in the both sides at interface, because making drop, the repulsive interaction of electrostatic double layer is difficult to cohesion simultaneously, thereby improved the stability of emulsion, coating effect is more satisfactory, firm and do not come off.Then by effects such as absorption, parcel, affine, chelatings, fertilizer is slowly discharged, particularly make the release period of nitrogenous fertilizer extend to 100 days, can guarantee needs in the time of infertility, need not topdress again, saved manually, realized the mechanize of summer corn fertilising.
(3) this coated fertilizer is for the fertile characteristic of need of the main summer corn soil nutrient supply present situation in Shandong Province and summer corn, the optimum formula filtering out, the fertilizer nitrogen phosphorus potassium total content>=50% (N:P producing
2o
5: K
2o=30:8:12), and contain trace element and the multiple nutrients such as Zn, balanced in nutrition, fertilizer efficiency is grown and remarkable, and quality meets GB15063-2000 standard completely.
(4) this coated fertilizer is selected slow-release material (Yelkin TTS/polyacrylic acid potassium) and controlled-release material (DMPP), the fertilizer efficiency period of nitrogenous fertilizer was brought up to 100 days from about 15 days, and concentrated release of corn typhon mouth phase, the fertilizer efficiency period of nitrogenous fertilizer and the utilization rate of nitrogen fertilizer of summer corn have greatly been improved, summer corn this season utilization rate of nitrogen fertilizer has improved 46%, and reduced the fixing of phosphorus potash fertilizer and run off, summer corn is worked as quaternary phosphonium potassium utilization rate and is improved respectively 17% and 6%.
Typical test situation is:
In Cao County, Shandong Province, Linqing and Boxing, take existing kind Zheng Dan 958 as test kind, 5000 plants/acre of planting densities, every mu of base is executed 50 kilograms of coat fertilizers of the present invention, (early stage 12 kilograms, the base manure urea take the not coating complex fertilizer of filling a prescription equally as control group, 8 kilograms of monoammonium phosphates, 10 kilograms, Repone K, 0.5 kilogram, zinc sulfate, the litmus mouth phase chases after flowering and boll-setting period and chases after 18 kilograms, urea), other fertilising is identical with control measures, control group summer corn per mu yield on three ground is respectively 678.8 kilograms, 662.5 kilograms and 627.3 kilograms, use coat fertilizer summer corn per mu yield of the present invention and be respectively 846.5 kilograms, 815.5 kilograms and 854.4 kilograms, visible, at rate of fertilizer under similar circumstances, use coat fertilizer of the present invention respectively than control group volume increase 24.7%, 23.1% and 36.2%.
Embodiment
Embodiment 1
Proportioning (kilogram): urea 580, monoammonium phosphate 160, Repone K 180, special excellent 35, wilkinite 50, magnesium oxide 50, zinc sulfate 5, ferrous sulfate 2, sulfuric acid sub-nickel 2, borax 1, Yelkin TTS 18, polyacrylic acid potassium 10 and Oleum Gossypii semen 32.
The wherein content of main raw material: monoammonium phosphate (N 11-P
2o
544), Repone K (K
2o>=60%), urea (N>=46%), Yelkin TTS/polyacrylic acid potassium purity is more than 90%.
(1) metering, stirring, fragmentation
First urea and DMPP are mixed, are pulverized; Then add monoammonium phosphate, Repone K, excellent of spy, wilkinite, magnesium oxide, zinc sulfate, ferrous sulfate, the sub-nickel of sulfuric acid and borax, after metering, mixing, form solid materials, then after fragmentation, enter the granulation of rotary drum steam granulation machine;
Urea crusher L800(ω=1200r/min); Chain breaker, post-type mixer model are respectively: XW-100, φ 3.2m.
(2) granulation
15 minutes granulation time, rotary drum steam granulation φ 2.2 × 7m, vapour pressure is 1.2 normal atmosphere.
(3) dry
By conveying belt, the material input drying machine after granulation is dried.Drying machine φ 2.2 × 24m, 205 ~ 255 ℃ of drying machine temperature ins, 65 ~ 85 ℃ of dry outlet material temperature.
(4) cooling
By conveying belt, by dried material input cooler, carry out cooling.Cooler φ 2.2 × 24m, 45 ± 5 ℃ of cooler outlet material temperature.
(5) screening
By conveying belt, cooled material inputted vibration is sieved, carry out the first screening, the material input coating machine of particle diameter between 1-4mm, it is again broken that all the other turn back to crusher.Vibratory screening apparatus model ZS-10.
(6) coating
Coated fertilizer Yelkin TTS, polyacrylic acid potassium and Oleum Gossypii semen are poured in stirred pot, after stirring is mixed, material and coating agent are squeezed into coating machine spraying coating by hydro-pump.Packing machine φ 1.2 × 8.5m; Hydro-pump CST300.
(7) input of the material after coating drying machine is dried, and then sends into cooler and carries out cooling; 185 ~ 200 ℃ of described drying machine temperature ins, 65 ~ 85 ℃ of dry outlet material temperature; 45 ± 5 ℃ of described cooler outlet material temperature.
(8) dried material inputted vibration sieve, sieves for the second time, is divided into macrobead, middle particle and three kinds of specifications of small-particle.Vibratory screening apparatus model ZS-7.
(9) metering packing.BFT-3 computer automatic quantitative packing machine.
(10) finished product warehouse-in.
Claims (5)
1. a summer corn special-purpose control-release fertilizer, is characterized in that, it is to carry out forming inner layer granule after granulation with urea, monoammonium phosphate, Repone K, excellent of spy, wilkinite, magnesium oxide, zinc sulfate, ferrous sulfate, the sub-nickel of sulfuric acid, borax and DMPP; Outer with Yelkin TTS/polyacrylic acid potassium coating; The component of described inner layer granule and weight part are: urea 550～600, monoammonium phosphate 150～200, Repone K 150～200, special excellent 35, wilkinite 50, magnesium oxide 50, zinc sulfate 5, ferrous sulfate 2, the sub-nickel 2 of sulfuric acid, borax 1, DMPP 2; The component of described coated fertilizer and weight part are: Yelkin TTS 18, polyacrylic acid potassium 10 and Oleum Gossypii semen 32; The mass ratio of described inner layer granule and coated fertilizer is 100:5.5-6.5.
2. the production method of summer corn special-purpose control-release fertilizer claimed in claim 1, is characterized in that,
(1) in ratio claimed in claim 1, get each component of inner layer granule and coated fertilizer;
First urea and DMPP are mixed, pulverized; Then add monoammonium phosphate, Repone K, excellent of spy, wilkinite, magnesium oxide, zinc sulfate, ferrous sulfate, the sub-nickel of sulfuric acid and borax, after mixing, form solid materials, then after crusher in crushing, enter the granulation of rotary drum steam granulation machine;
(2) by conveying belt, the material input drying machine after granulation is dried, then sends into cooler and carry out cooling;
(3) by cooled material inputted vibration sieve, carry out the first screening, particle diameter is between the material input coating machine of 1-4mm, and all the other turn back to the crusher fragmentation again of step (1);
(4) coated fertilizer Yelkin TTS, polyacrylic acid potassium and Oleum Gossypii semen are poured in stirred pot, after stirring is mixed, particle diameter is squeezed into coating machine spraying coating between material and the coated fertilizer of 1-4mm by hydro-pump;
(5) input of the material after coating drying machine is dried, and then sends into cooler and carries out cooling;
(6) dried material inputted vibration sieves rear metering packing.
3. production method as claimed in claim 2, is characterized in that, the drying machine temperature in of described step (2) is 205 ~ 255 ℃, and dry outlet material temperature is 65 ~ 85 ℃.
4. production method as claimed in claim 2, is characterized in that, the dry cooling machine outlet material temperature of described step (2) or (5) is 45 ± 5 ℃.
5. production method as claimed in claim 2, is characterized in that, the drying machine temperature in of described step (5) is 185 ~ 200 ℃, and dry outlet material temperature is 65 ~ 85 ℃.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410053926.7A CN103755483B (en) | 2014-02-18 | 2014-02-18 | A kind of Special controlled-release fertilizer for summer maize and production method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410053926.7A CN103755483B (en) | 2014-02-18 | 2014-02-18 | A kind of Special controlled-release fertilizer for summer maize and production method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103755483A true CN103755483A (en) | 2014-04-30 |
| CN103755483B CN103755483B (en) | 2016-01-20 |
Family
ID=50522848
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410053926.7A Expired - Fee Related CN103755483B (en) | 2014-02-18 | 2014-02-18 | A kind of Special controlled-release fertilizer for summer maize and production method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN103755483B (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104030803A (en) * | 2014-05-23 | 2014-09-10 | 刘凯 | Special controlled-release fertilizer for winter wheat and production method of fertilizer |
| CN105085124A (en) * | 2015-07-31 | 2015-11-25 | 安徽省化工设计院 | Coated water retention slow release fertilizer and preparation method thereof |
| CN108929148A (en) * | 2017-05-27 | 2018-12-04 | 山东红日化工股份有限公司 | A kind of drought-resistant water-preserving fertilizer and preparation method thereof |
| CN112679276A (en) * | 2021-01-28 | 2021-04-20 | 平原县释乐补农业科技有限公司 | Polyurethane coated urea for further improving nitrogen utilization rate |
Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5938813A (en) * | 1997-01-27 | 1999-08-17 | Sqm Nitratos, S.A. | Granular coated particles containing urea and metal nitrate, and process for making the same |
| CN1609077A (en) * | 2004-11-03 | 2005-04-27 | 中国农业科学院土壤肥料研究所 | Production process of slowly/controlled releasing fertilizer for summer corn |
| CN102424641A (en) * | 2011-09-20 | 2012-04-25 | 山东大学 | Corn slow-release fertilizer |
| CN102491838A (en) * | 2011-11-30 | 2012-06-13 | 新疆慧尔农业科技发展有限公司 | Special long-acting slow release fertilizer for corn and preparation method thereof |
| CN103058751A (en) * | 2012-12-26 | 2013-04-24 | 施可丰化工股份有限公司 | Preparation method for special slow-release long-acting compound fertilizer for corn |
| CN103058754A (en) * | 2012-12-26 | 2013-04-24 | 施可丰化工股份有限公司 | Slow-release compound fertilizer applicable to plantation of corn |
| CN103102223A (en) * | 2013-03-05 | 2013-05-15 | 孟庆华 | Special lecithin-coated slow release fertilizer for cotton and production method of fertilizer |
-
2014
- 2014-02-18 CN CN201410053926.7A patent/CN103755483B/en not_active Expired - Fee Related
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5938813A (en) * | 1997-01-27 | 1999-08-17 | Sqm Nitratos, S.A. | Granular coated particles containing urea and metal nitrate, and process for making the same |
| CN1609077A (en) * | 2004-11-03 | 2005-04-27 | 中国农业科学院土壤肥料研究所 | Production process of slowly/controlled releasing fertilizer for summer corn |
| CN102424641A (en) * | 2011-09-20 | 2012-04-25 | 山东大学 | Corn slow-release fertilizer |
| CN102491838A (en) * | 2011-11-30 | 2012-06-13 | 新疆慧尔农业科技发展有限公司 | Special long-acting slow release fertilizer for corn and preparation method thereof |
| CN103058751A (en) * | 2012-12-26 | 2013-04-24 | 施可丰化工股份有限公司 | Preparation method for special slow-release long-acting compound fertilizer for corn |
| CN103058754A (en) * | 2012-12-26 | 2013-04-24 | 施可丰化工股份有限公司 | Slow-release compound fertilizer applicable to plantation of corn |
| CN103102223A (en) * | 2013-03-05 | 2013-05-15 | 孟庆华 | Special lecithin-coated slow release fertilizer for cotton and production method of fertilizer |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104030803A (en) * | 2014-05-23 | 2014-09-10 | 刘凯 | Special controlled-release fertilizer for winter wheat and production method of fertilizer |
| CN105085124A (en) * | 2015-07-31 | 2015-11-25 | 安徽省化工设计院 | Coated water retention slow release fertilizer and preparation method thereof |
| CN108929148A (en) * | 2017-05-27 | 2018-12-04 | 山东红日化工股份有限公司 | A kind of drought-resistant water-preserving fertilizer and preparation method thereof |
| CN112679276A (en) * | 2021-01-28 | 2021-04-20 | 平原县释乐补农业科技有限公司 | Polyurethane coated urea for further improving nitrogen utilization rate |
Also Published As
| Publication number | Publication date |
|---|---|
| CN103755483B (en) | 2016-01-20 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN103664343A (en) | Special controlled-release fertilizer for fast-growing eucalyptus and preparation method thereof | |
| CN103102223B (en) | Special lecithin-coated slow release fertilizer for cotton and production method of fertilizer | |
| CN103102213B (en) | Preparation method of special long-term slow-release compound fertilizer for wheat | |
| CN103058761B (en) | Slow release compound fertilizer applicable to plantation of wheat | |
| CN103626589B (en) | Biomass charcoal-based compound fertilizer special for wheat and preparation method of biomass charcoal-based compound fertilizer | |
| CN104529674A (en) | Special humic acid fertilizer for sweet potatoes and preparation method of special humic acid fertilizer | |
| CN104058891A (en) | Microelement-rich compound coated fertilizer for crops and preparation method of compound coated fertilizer | |
| CN104030803A (en) | Special controlled-release fertilizer for winter wheat and production method of fertilizer | |
| CN104230529A (en) | Special higher-utilization-ratio environment-friendly coated fertilizer for blueberries and preparation method thereof | |
| CN103755483B (en) | A kind of Special controlled-release fertilizer for summer maize and production method thereof | |
| CN104311319A (en) | Special high-fertilize-efficiency composite coated fertilizer for wheat and preparation method of special high-fertilize-efficiency composite coated fertilizer | |
| CN103058751B (en) | Preparation method for special slow-release long-acting compound fertilizer for corn | |
| WO2017206743A1 (en) | Method for rapid manufacturing of novel micronutrient-containing urea | |
| CN103058753B (en) | Slow release compound fertilizer applicable to plantation of soybeans | |
| CN103058754B (en) | Slow-release compound fertilizer applicable to plantation of corn | |
| CN103058762B (en) | Slow-release compound fertilizer suitable for fruit tree planting | |
| CN103058752A (en) | Preparation method for special slow-release long-acting compound fertilizer for paddy rice | |
| CN104446803B (en) | high nitrogen type water-soluble fertilizer containing fulvic acid | |
| CN101638343B (en) | Special corn fertilizer and preparation method thereof | |
| CN103613465B (en) | Special biomass charcoal-based compound fertilizer for rapes and preparation method thereof | |
| CN103058755A (en) | Slow release compound fertilizer applicable to plantation of cotton | |
| CN103058756A (en) | Preparation method for special slow-release long-acting compound fertilizer for cotton | |
| CN103058760A (en) | Slow release compound fertilizer applicable to plantation of tobacco | |
| CN104045423A (en) | Corn special biological organic coated fertilizer and preparation method thereof | |
| CN103274813A (en) | Composite fertilizer specially used for corns |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| TR01 | Transfer of patent right | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20201202 Address after: No.001, Chuangxin Road, Laihe Town, Shan county, Heze City, Shandong Province, 274300 Patentee after: Huang Yanhong Address before: 250100 science and technology industry department, Ji'nan Academy of Agricultural Sciences, 202 industrial North Road, Licheng District, Shandong, Shandong Patentee before: Meng Qinghua Patentee before: JINAN FEITIAN AGRICULTURAL SCIENCE AND TECHNOLOGY Co.,Ltd. |
|
| TR01 | Transfer of patent right | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20210222 Address after: 152002 Dongfu Township, Beilin District, Suihua City, Heilongjiang Province Patentee after: Heilongjiang Bairun fertilizer Co.,Ltd. Address before: 274300 No.001, Chuangxin Road, Laihe Town, Shan county, Heze City, Shandong Province Patentee before: Huang Yanhong |
|
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20160120 |