CN103704327A - Kiwi fruit preservative and preparation method thereof - Google Patents

Kiwi fruit preservative and preparation method thereof Download PDF

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CN103704327A
CN103704327A CN201310685521.0A CN201310685521A CN103704327A CN 103704327 A CN103704327 A CN 103704327A CN 201310685521 A CN201310685521 A CN 201310685521A CN 103704327 A CN103704327 A CN 103704327A
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parts
potassium sorbate
citric acid
solution
water
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CN103704327B (en
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包伟强
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Suzhou Antek Industrial Co Ltd
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Abstract

The invention relates to a kiwi fruit preservative and a preparation method thereof, and belongs to the technical field of preservatives. The kiwi fruit preservative is characterized by consisting of water, citric acid, starch, chitosan, vitamin C, cinnamic acid, sodium phosphate, sodium benzoate, beta-cyclodextrin, sodium acetate, green tea powder, calcium propionate and potassium sorbate. The kiwi fruit preservative provided by the invention is prepared from a variety of materials, and the cost of the used raw materials is low, so that the preparation cost is reduced; the proportions between the components are moderate, the kiwi fruit preservative is easy to store and is safe and non-toxic, moreover, the kiwi fruit preservative provided by the invention is a spray preservative, and when in use, a film formed on the fruit surface is good in antiseptic and bactericidal performance, long in refreshing time, good in moisturizing effect and is edible and non-toxic, so that no harm is generated to a human body.

Description

Kiwi berry antistaling agent and preparation method thereof
technical field:
The present invention relates to a kind of Kiwi berry antistaling agent and preparation method thereof, belong to antistaling agent technical field.
background technology:
Along with the raising of people's living standard, fruit has been one of indispensable living material during people live, and Kiwi berry is because its vitamin content is high and very popular.Along with the rising of Kiwi berry demand, the quantity at Kiwi berry plantation family also increases sharply, yet the Kiwi berry of this season is due to the increase in a period of time of supply, cannot when fruit maturation, they all be sold out at all, therefore, must carry out fresh-keeping to Kiwi berry.The fresh-keeping major technique of Kiwi berry has at present: low temperature controlled atmosphere method, and this method is expensive, can not reduce ethylene gas and discharge, and also have putrefactive phenomenon after long-time preservation; Chemical preservative method, affects health owing to having residual, the difficult removal of the chemical agent of toxic and side effect, therefore will accomplish the exploitation of the Kiwi berry antistaling agent of safe, nontoxic and pure natural, and application prospect is very extensive.
Kiwi berry antistaling agent on market is of a great variety, and function is also different, but Kiwi berry antistaling agent ubiquity fresh keeping time of the prior art is not long, complex manufacturing technology, cost of manufacture is high, inconvenient problem with use, and some antistaling agents also contain harmful chemical composition.
summary of the invention:
The present invention seeks to, be used for making up the deficiencies in the prior art, and a kind of Kiwi berry antistaling agent and preparation method thereof is provided, cost of manufacture is low, can not work the mischief to human body, and good refreshing effect.
To achieve these goals, Kiwi berry antistaling agent of the present invention, is characterized in that: water, citric acid, starch, shitosan, vitamin C, cinnamic acid, sodium phosphate, Sodium Benzoate, beta-schardinger dextrin-, sodium acetate, green tea powder, calcium propionate, potassium sorbate, consist of.
Described water is 60~75 parts;
Described citric acid is 5~8 parts;
Described starch is 10~13 parts;
Described shitosan is 3~5 parts;
Described vitamin C is 4~6 parts;
Described cinnamic acid is 1~3 part;
Described sodium phosphate is 2~4 parts;
Described Sodium Benzoate is 1~2 part;
Described beta-schardinger dextrin-is 2~3 parts;
Described sodium acetate is 3~5 parts;
Described green tea powder is 6~9 parts;
Described calcium propionate is 4~6 parts;
Described potassium sorbate is 3~5 parts;
Described umber is parts by weight.
Preferred version of the present invention is as follows:
One,
Described water is 65 parts;
Described citric acid is 6 parts;
Described starch is 11 parts;
Described shitosan is 3 parts;
Described vitamin C is 4 parts;
Described cinnamic acid is 2 parts;
Described sodium phosphate is 2 parts;
Described Sodium Benzoate is 1 part;
Described beta-schardinger dextrin-is 2 parts;
Described sodium acetate is 4 parts;
Described green tea powder is 7 parts;
Described calcium propionate is 4 parts;
Described potassium sorbate is 4 parts.
Two,
Described water is 70 parts;
Described citric acid is 8 parts;
Described starch is 12 parts;
Described shitosan is 5 parts;
Described vitamin C is 6 parts;
Described cinnamic acid is 2 parts;
Described sodium phosphate is 3 parts;
Described Sodium Benzoate is 2 parts;
Described beta-schardinger dextrin-is 3 parts;
Described sodium acetate is 4 parts;
Described green tea powder is 8 parts;
Described calcium propionate is 5 parts;
Described potassium sorbate is 5 parts.
The preparation method of Kiwi berry antistaling agent of the present invention, comprises following step:
(A) water, shitosan, sodium phosphate, Sodium Benzoate, beta-schardinger dextrin-, calcium propionate are required to send in mixer to be uniformly mixed and to obtain solution No. one according to parts by weight, the mixing speed of described mixer is per minute 25~38 to turn, described in be uniformly mixed actuator temperature and be controlled at 45~56 ℃;
(B) solution is precipitated to 10~15 hours, then supernatant is extracted and obtains solution No. two;
(C) sending lemon raw material to pulverizer pulverizes, add concentration and be 50%~70% ethanol water, again by solidliquid mixture ultrasonic wave assisted extraction, ultrasonic wave extraction conditions: ultrasonic temperature is that 45~56 ℃, supersonic frequency are that 20~30kHz, ultrasonic extraction time are 1~2 hour, then by solidliquid mixture suction filtration under 20~30kPa vacuum condition, get filtrate decompression distillation under 15~25kPa vacuum, 45~50 ℃ of conditions, reclaim ethanol, obtain citric acid;
(D) sending sorb raw material to pulverizer pulverizes, add concentration and be 60%~70% ethanol water, again by solidliquid mixture ultrasonic wave assisted extraction, ultrasonic wave extraction conditions: ultrasonic temperature is that 45~55 ℃, supersonic frequency are that 20~30kHz, ultrasonic extraction time are 1~2 hour, then by solidliquid mixture suction filtration under 25~35kPa vacuum condition, get filtrate decompression distillation under 20~30kPa vacuum, 35~50 ℃ of conditions, reclaim ethanol, obtain sorbic acid, then obtain potassium sorbate with KOH solution mixing system;
(E) No. two solution and vitamin C, citric acid, green tea powder, potassium sorbate, starch, cinnamic acid, sodium acetate are required to send in mixer to be uniformly mixed and to obtain solution No. three according to parts by weight, the mixing speed of described mixer is per minute 15~25 to turn, described in be uniformly mixed actuator temperature and be controlled at 25~34 ℃;
(F) No. three solution are crossed to 75 mesh sieves and filter, make Kiwi berry antistaling agent.
Beneficial effect of the present invention is as follows:
The present invention selects multiple material formulated, and the cost of raw material of use is cheap, thereby cost of manufacture is low; Ratio between various compositions is moderate, be easy to store, safety non-toxic, and the present invention is spray antistaling agent, the film forming at fruit surface during use has that antisepsis and sterilization performance is good, long fresh-keeping period, moisture-keeping efficacy is good and it is nontoxic to eat, and can not work the mischief to human body.
the specific embodiment:
For technological means, creation characteristic that the present invention is realized, reach object and effect is easy to understand, further set forth the present invention.
Embodiment 1:
In the present embodiment, described water is 65 parts; Described citric acid is 6 parts; Described starch is 11 parts; Described shitosan is 3 parts; Described vitamin C is 4 parts; Described cinnamic acid is 2 parts; Described sodium phosphate is 2 parts; Described Sodium Benzoate is 1 part; Described beta-schardinger dextrin-is 2 parts; Described sodium acetate is 4 parts; Described green tea powder is 7 parts; Described calcium propionate is 4 parts; Described potassium sorbate is 4 parts.
Described umber is parts by weight.
The preparation method of the Kiwi berry antistaling agent described in the present embodiment comprises following step:
(A) water, shitosan, sodium phosphate, Sodium Benzoate, beta-schardinger dextrin-, calcium propionate are required to send in mixer to be uniformly mixed and to obtain solution No. one according to parts by weight, the mixing speed of described mixer is per minute 30 to turn, described in be uniformly mixed actuator temperature and be controlled at 48 ℃;
(B) solution is precipitated to 13 hours, then supernatant is extracted and obtains solution No. two;
(C) sending lemon raw material to pulverizer pulverizes, add concentration and be 70% ethanol water, again by solidliquid mixture ultrasonic wave assisted extraction, ultrasonic wave extraction conditions: ultrasonic temperature is that 50 ℃, supersonic frequency are that 25kHz, ultrasonic extraction time are 2 hours, then by solidliquid mixture suction filtration under 25kPa vacuum condition, get filtrate decompression distillation under 20kPa vacuum, 47 ℃ of conditions, reclaim ethanol, obtain citric acid;
(D) sending sorb raw material to pulverizer pulverizes, add concentration and be 65% ethanol water, again by solidliquid mixture ultrasonic wave assisted extraction, ultrasonic wave extraction conditions: ultrasonic temperature is that 50 ℃, supersonic frequency are that 25kHz, ultrasonic extraction time are 1 hour, then by solidliquid mixture suction filtration under 30kPa vacuum condition, get filtrate decompression distillation under 25kPa vacuum, 40 ℃ of conditions, reclaim ethanol, obtain sorbic acid, then obtain potassium sorbate with KOH solution mixing system;
(E) No. two solution and vitamin C, citric acid, green tea powder, potassium sorbate, starch, cinnamic acid, sodium acetate are required to send in mixer to be uniformly mixed and to obtain solution No. three according to parts by weight, the mixing speed of described mixer is per minute 20 to turn, described in be uniformly mixed actuator temperature and be controlled at 30 ℃;
(F) No. three solution are crossed to 75 mesh sieves and filter, make Kiwi berry antistaling agent.
During use, Kiwi berry antistaling agent is sprayed directly on the Kiwi berry picking, very easy to use, Kiwi berry is fresh-keeping generally at four to five months, has facilitated people to live edible.The present invention selects multiple material formulated, and the cost of raw material of use is cheap, thereby cost of manufacture is low; Ratio between various compositions is moderate, be easy to store, safety non-toxic, and the present invention is spray antistaling agent, the film forming at fruit surface during use has antisepsis and sterilization performance good (being mainly reflected on sodium acetate component), long fresh-keeping period, moisture-keeping efficacy is good and it is nontoxic to eat, and can not work the mischief to human body.
Embodiment 2:
In this enforcement, described water is 70 parts; Described citric acid is 8 parts; Described starch is 12 parts; Described shitosan is 5 parts; Described vitamin C is 6 parts; Described cinnamic acid is 2 parts; Described sodium phosphate is 3 parts; Described Sodium Benzoate is 2 parts; Described beta-schardinger dextrin-is 3 parts; Described sodium acetate is 4 parts; Described green tea powder is 8 parts; Described calcium propionate is 5 parts; Described potassium sorbate is 5 parts.
Described umber is parts by weight.
The preparation method of the Kiwi berry antistaling agent described in the present embodiment comprises following step:
(A) water, shitosan, sodium phosphate, Sodium Benzoate, beta-schardinger dextrin-, calcium propionate are required to send in mixer to be uniformly mixed and to obtain solution No. one according to parts by weight, the mixing speed of described mixer is per minute 35 to turn, described in be uniformly mixed actuator temperature and be controlled at 53 ℃;
(B) solution is precipitated to 14 hours, then supernatant is extracted and obtains solution No. two;
(C) sending lemon raw material to pulverizer pulverizes, add concentration and be 60% ethanol water, again by solidliquid mixture ultrasonic wave assisted extraction, ultrasonic wave extraction conditions: ultrasonic temperature is that 50 ℃, supersonic frequency are that 20kHz, ultrasonic extraction time are 1 hour, then by solidliquid mixture suction filtration under 30kPa vacuum condition, get filtrate decompression distillation under 20kPa vacuum, 49 ℃ of conditions, reclaim ethanol, obtain citric acid;
(D) sending sorb raw material to pulverizer pulverizes, add concentration and be 65% ethanol water, again by solidliquid mixture ultrasonic wave assisted extraction, ultrasonic wave extraction conditions: ultrasonic temperature is that 49 ℃, supersonic frequency are that 26kHz, ultrasonic extraction time are 1.5 hours, then by solidliquid mixture suction filtration under 28kPa vacuum condition, get filtrate decompression distillation under 30kPa vacuum, 50 ℃ of conditions, reclaim ethanol, obtain sorbic acid, then obtain potassium sorbate with KOH solution mixing system;
(E requires No. two solution and vitamin C, citric acid, green tea powder, potassium sorbate, starch, cinnamic acid, sodium acetate to send in mixer to be uniformly mixed and to obtain solution No. three according to parts by weight, the mixing speed of described mixer is per minute 15 to turn, described in be uniformly mixed actuator temperature and be controlled at 32 ℃;
(F) No. three solution are crossed to 75 mesh sieves and filter, make Kiwi berry antistaling agent.
Using method is with embodiment mono-.
More than show and described basic principle of the present invention and principal character and advantage of the present invention.The technical staff of the industry should understand; the present invention is not restricted to the described embodiments; that in above-described embodiment and description, describes just illustrates principle of the present invention; without departing from the spirit and scope of the present invention; the present invention also has various changes and modifications, and these changes and improvements all fall in the claimed scope of the invention.The claimed scope of the present invention is defined by appending claims and equivalent thereof
Figure 2013106855210100002DEST_PATH_IMAGE001
Figure 906994DEST_PATH_IMAGE001
Figure 761818DEST_PATH_IMAGE001
Figure 541555DEST_PATH_IMAGE001
.

Claims (4)

1. a Kiwi berry antistaling agent, is characterized in that: water, citric acid, starch, shitosan, vitamin C, cinnamic acid, sodium phosphate, Sodium Benzoate, beta-schardinger dextrin-, sodium acetate, green tea powder, calcium propionate, potassium sorbate, consist of;
Described water is 60~75 parts;
Described citric acid is 5~8 parts;
Described starch is 10~13 parts;
Described shitosan is 3~5 parts;
Described vitamin C is 4~6 parts;
Described cinnamic acid is 1~3 part;
Described sodium phosphate is 2~4 parts;
Described Sodium Benzoate is 1~2 part;
Described beta-schardinger dextrin-is 2~3 parts;
Described sodium acetate is 3~5 parts;
Described green tea powder is 6~9 parts;
Described calcium propionate is 4~6 parts;
Described potassium sorbate is 3~5 parts;
Described umber is parts by weight.
2. Kiwi berry antistaling agent according to claim 1, is characterized in that,
Described water is 65 parts;
Described citric acid is 6 parts;
Described starch is 11 parts;
Described shitosan is 3 parts;
Described vitamin C is 4 parts;
Described cinnamic acid is 2 parts;
Described sodium phosphate is 2 parts;
Described Sodium Benzoate is 1 part;
Described beta-schardinger dextrin-is 2 parts;
Described sodium acetate is 4 parts;
Described green tea powder is 7 parts;
Described calcium propionate is 4 parts;
Described potassium sorbate is 4 parts.
3. Kiwi berry antistaling agent according to claim 1, is characterized in that,
Described water is 70 parts;
Described citric acid is 8 parts;
Described starch is 12 parts;
Described shitosan is 5 parts;
Described vitamin C is 6 parts;
Described cinnamic acid is 2 parts;
Described sodium phosphate is 3 parts;
Described Sodium Benzoate is 2 parts;
Described beta-schardinger dextrin-is 3 parts;
Described sodium acetate is 4 parts;
Described green tea powder is 8 parts;
Described calcium propionate is 5 parts;
Described potassium sorbate is 5 parts.
4. according to the preparation method of the Kiwi berry antistaling agent described in claim 2 or 3 any one, it is characterized in that, comprise following step:
(A) water, shitosan, sodium phosphate, Sodium Benzoate, beta-schardinger dextrin-, calcium propionate are required to send in mixer to be uniformly mixed and to obtain solution No. one according to the parts by weight of claim 2, the mixing speed of described mixer is per minute 25~38 to turn, described in be uniformly mixed actuator temperature and be controlled at 45~56 ℃;
(B) solution is precipitated to 10~15 hours, then supernatant is extracted and obtains solution No. two;
(C) sending lemon raw material to pulverizer pulverizes, add concentration and be 50%~70% ethanol water, again by solidliquid mixture ultrasonic wave assisted extraction, ultrasonic wave extraction conditions: ultrasonic temperature is that 45~56 ℃, supersonic frequency are that 20~30kHz, ultrasonic extraction time are 1~2 hour, then by solidliquid mixture suction filtration under 20~30kPa vacuum condition, get filtrate decompression distillation under 15~25kPa vacuum, 45~50 ℃ of conditions, reclaim ethanol, obtain citric acid;
(D) sending sorb raw material to pulverizer pulverizes, add concentration and be 60%~70% ethanol water, again by solidliquid mixture ultrasonic wave assisted extraction, ultrasonic wave extraction conditions: ultrasonic temperature is that 45~55 ℃, supersonic frequency are that 20~30kHz, ultrasonic extraction time are 1~2 hour, then by solidliquid mixture suction filtration under 25~35kPa vacuum condition, get filtrate decompression distillation under 20~30kPa vacuum, 35~50 ℃ of conditions, reclaim ethanol, obtain sorbic acid, then obtain potassium sorbate with KOH solution mixing system;
(E) No. two solution and vitamin C, citric acid, green tea powder, potassium sorbate, starch, cinnamic acid, sodium acetate are required to send in mixer to be uniformly mixed and to obtain solution No. three according to the parts by weight of claim 2, the mixing speed of described mixer is per minute 15~25 to turn, described in be uniformly mixed actuator temperature and be controlled at 25~34 ℃;
(F) No. three solution are crossed to 75 mesh sieves and filter, make Kiwi berry antistaling agent.
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Cited By (11)

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CN104489553A (en) * 2015-01-15 2015-04-08 四川省苍溪漓山粮油有限公司 Kiwi fruit buccal tablet preparing method
CN105028888A (en) * 2015-07-24 2015-11-11 四川兴食尚科技有限公司 Preparation method of selenium-enriched kiwifruit yogurt ice cream
CN105724560A (en) * 2016-03-03 2016-07-06 和县朱韩瓜果种植家庭农场 Method for preparing dried figs
CN105767134A (en) * 2016-03-03 2016-07-20 和县朱韩瓜果种植家庭农场 Preparation method of dried kiwi fruits
CN105918450A (en) * 2016-05-11 2016-09-07 龙岩泰华实业有限公司 Fruit preservative as well as preparation method and use thereof
CN106359558A (en) * 2015-07-22 2017-02-01 南阳师范学院 Natural cherry fresh keeping agent and preparation method thereof
CN106376642A (en) * 2016-08-31 2017-02-08 宁波浩丰农业科技有限公司 Biological preservative for storage of kiwifruit fruits after picking
CN106666046A (en) * 2016-12-20 2017-05-17 钦州阜康农副食品有限公司 Preserved kiwifruits and manufacture method thereof
CN107223705A (en) * 2017-06-02 2017-10-03 青川弘森猕猴桃开发有限公司 A kind of antistaling agent and its preservation method for Kiwi berry
CN107509805A (en) * 2017-09-29 2017-12-26 雅安市猕猴桃产业技术研究院 A kind of natural Actinidia chinensis antistaling and antiseptic agent
CN109258784A (en) * 2017-07-18 2019-01-25 吕朝妮 Kiwi fruit preservative and preparation method thereof

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EP3170403A1 (en) * 2015-11-18 2017-05-24 Purac Biochem B.V. Preservative system and use thereof in edible products

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104489553A (en) * 2015-01-15 2015-04-08 四川省苍溪漓山粮油有限公司 Kiwi fruit buccal tablet preparing method
CN104489553B (en) * 2015-01-15 2017-06-09 四川省苍溪漓山粮油有限公司 A kind of preparation method of Kiwi berry buccal tablet
CN106359558A (en) * 2015-07-22 2017-02-01 南阳师范学院 Natural cherry fresh keeping agent and preparation method thereof
CN105028888A (en) * 2015-07-24 2015-11-11 四川兴食尚科技有限公司 Preparation method of selenium-enriched kiwifruit yogurt ice cream
CN105724560A (en) * 2016-03-03 2016-07-06 和县朱韩瓜果种植家庭农场 Method for preparing dried figs
CN105767134A (en) * 2016-03-03 2016-07-20 和县朱韩瓜果种植家庭农场 Preparation method of dried kiwi fruits
CN105918450A (en) * 2016-05-11 2016-09-07 龙岩泰华实业有限公司 Fruit preservative as well as preparation method and use thereof
CN106376642A (en) * 2016-08-31 2017-02-08 宁波浩丰农业科技有限公司 Biological preservative for storage of kiwifruit fruits after picking
CN106666046A (en) * 2016-12-20 2017-05-17 钦州阜康农副食品有限公司 Preserved kiwifruits and manufacture method thereof
CN107223705A (en) * 2017-06-02 2017-10-03 青川弘森猕猴桃开发有限公司 A kind of antistaling agent and its preservation method for Kiwi berry
CN109258784A (en) * 2017-07-18 2019-01-25 吕朝妮 Kiwi fruit preservative and preparation method thereof
CN107509805A (en) * 2017-09-29 2017-12-26 雅安市猕猴桃产业技术研究院 A kind of natural Actinidia chinensis antistaling and antiseptic agent

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