CN103694368A - 米糠多糖的提取方法 - Google Patents
米糠多糖的提取方法 Download PDFInfo
- Publication number
- CN103694368A CN103694368A CN201310694933.0A CN201310694933A CN103694368A CN 103694368 A CN103694368 A CN 103694368A CN 201310694933 A CN201310694933 A CN 201310694933A CN 103694368 A CN103694368 A CN 103694368A
- Authority
- CN
- China
- Prior art keywords
- rice bran
- finings
- supernatant liquor
- bran polysaccharide
- extracting method
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 235000007164 Oryza sativa Nutrition 0.000 title claims abstract description 51
- 235000009566 rice Nutrition 0.000 title claims abstract description 51
- 150000004676 glycans Chemical class 0.000 title claims abstract description 46
- 229920001282 polysaccharide Polymers 0.000 title claims abstract description 46
- 239000005017 polysaccharide Substances 0.000 title claims abstract description 46
- 238000000034 method Methods 0.000 title claims abstract description 31
- 240000007594 Oryza sativa Species 0.000 title 1
- 241000209094 Oryza Species 0.000 claims abstract description 50
- 239000006228 supernatant Substances 0.000 claims abstract description 21
- 239000012535 impurity Substances 0.000 claims abstract description 11
- 239000000047 product Substances 0.000 claims abstract description 4
- 239000000243 solution Substances 0.000 claims description 17
- 238000001556 precipitation Methods 0.000 claims description 8
- 238000009413 insulation Methods 0.000 claims description 6
- 239000011259 mixed solution Substances 0.000 claims description 6
- 238000003756 stirring Methods 0.000 claims description 6
- 238000005507 spraying Methods 0.000 claims description 4
- 238000001291 vacuum drying Methods 0.000 claims description 4
- 238000009835 boiling Methods 0.000 claims description 3
- 239000000706 filtrate Substances 0.000 claims description 3
- 229920006395 saturated elastomer Polymers 0.000 claims description 3
- 238000000605 extraction Methods 0.000 abstract description 21
- 238000005516 engineering process Methods 0.000 abstract description 8
- 238000005265 energy consumption Methods 0.000 abstract description 3
- 230000007613 environmental effect Effects 0.000 abstract description 3
- 238000001179 sorption measurement Methods 0.000 abstract description 3
- AXCZMVOFGPJBDE-UHFFFAOYSA-L calcium dihydroxide Chemical compound [OH-].[OH-].[Ca+2] AXCZMVOFGPJBDE-UHFFFAOYSA-L 0.000 abstract 1
- 229910001861 calcium hydroxide Inorganic materials 0.000 abstract 1
- 235000011116 calcium hydroxide Nutrition 0.000 abstract 1
- 239000000920 calcium hydroxide Substances 0.000 abstract 1
- 238000005119 centrifugation Methods 0.000 abstract 1
- 238000009776 industrial production Methods 0.000 abstract 1
- 239000004615 ingredient Substances 0.000 abstract 1
- 239000002244 precipitate Substances 0.000 abstract 1
- 102000004169 proteins and genes Human genes 0.000 abstract 1
- 108090000623 proteins and genes Proteins 0.000 abstract 1
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical group [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 9
- 239000000284 extract Substances 0.000 description 6
- 239000000203 mixture Substances 0.000 description 5
- IMQLKJBTEOYOSI-GPIVLXJGSA-N Inositol-hexakisphosphate Chemical compound OP(O)(=O)O[C@H]1[C@H](OP(O)(O)=O)[C@@H](OP(O)(O)=O)[C@H](OP(O)(O)=O)[C@H](OP(O)(O)=O)[C@@H]1OP(O)(O)=O IMQLKJBTEOYOSI-GPIVLXJGSA-N 0.000 description 4
- IMQLKJBTEOYOSI-UHFFFAOYSA-N Phytic acid Natural products OP(O)(=O)OC1C(OP(O)(O)=O)C(OP(O)(O)=O)C(OP(O)(O)=O)C(OP(O)(O)=O)C1OP(O)(O)=O IMQLKJBTEOYOSI-UHFFFAOYSA-N 0.000 description 4
- 238000005352 clarification Methods 0.000 description 4
- 229940068041 phytic acid Drugs 0.000 description 4
- 235000002949 phytic acid Nutrition 0.000 description 4
- 239000000467 phytic acid Substances 0.000 description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
- 239000003153 chemical reaction reagent Substances 0.000 description 3
- 230000007423 decrease Effects 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- 238000011160 research Methods 0.000 description 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- 235000013339 cereals Nutrition 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- OQUKIQWCVTZJAF-UHFFFAOYSA-N phenol;sulfuric acid Chemical compound OS(O)(=O)=O.OC1=CC=CC=C1 OQUKIQWCVTZJAF-UHFFFAOYSA-N 0.000 description 2
- 238000012545 processing Methods 0.000 description 2
- 241000050051 Chelone glabra Species 0.000 description 1
- 229920002101 Chitin Polymers 0.000 description 1
- 229920002307 Dextran Polymers 0.000 description 1
- 108010010803 Gelatin Proteins 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 230000003321 amplification Effects 0.000 description 1
- 238000004440 column chromatography Methods 0.000 description 1
- 230000024203 complement activation Effects 0.000 description 1
- 230000006378 damage Effects 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000012869 ethanol precipitation Methods 0.000 description 1
- 238000013401 experimental design Methods 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 239000000499 gel Substances 0.000 description 1
- 239000008273 gelatin Substances 0.000 description 1
- 229920000159 gelatin Polymers 0.000 description 1
- 235000019322 gelatine Nutrition 0.000 description 1
- 235000011852 gelatine desserts Nutrition 0.000 description 1
- 239000004519 grease Substances 0.000 description 1
- 230000002519 immonomodulatory effect Effects 0.000 description 1
- 230000003053 immunization Effects 0.000 description 1
- 238000002649 immunization Methods 0.000 description 1
- 210000004698 lymphocyte Anatomy 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000003199 nucleic acid amplification method Methods 0.000 description 1
- 210000003024 peritoneal macrophage Anatomy 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 238000007634 remodeling Methods 0.000 description 1
- 230000004044 response Effects 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 238000003809 water extraction Methods 0.000 description 1
Landscapes
- Polysaccharides And Polysaccharide Derivatives (AREA)
Abstract
Description
Claims (4)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN201310694933.0A CN103694368B (zh) | 2013-12-18 | 2013-12-18 | 米糠多糖的提取方法 |
Applications Claiming Priority (1)
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CN201310694933.0A CN103694368B (zh) | 2013-12-18 | 2013-12-18 | 米糠多糖的提取方法 |
Publications (2)
Publication Number | Publication Date |
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CN103694368A true CN103694368A (zh) | 2014-04-02 |
CN103694368B CN103694368B (zh) | 2015-10-28 |
Family
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Family Applications (1)
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CN201310694933.0A Active CN103694368B (zh) | 2013-12-18 | 2013-12-18 | 米糠多糖的提取方法 |
Country Status (1)
Country | Link |
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CN (1) | CN103694368B (zh) |
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104306391A (zh) * | 2014-09-18 | 2015-01-28 | 河北科星药业有限公司 | 米糠多糖口服液、注射液和可溶性粉末及相应的制备方法 |
CN105166626A (zh) * | 2015-09-29 | 2015-12-23 | 江苏锦宇环境工程有限公司 | 一种米糠多糖口含片的制备方法 |
CN107267571A (zh) * | 2017-07-15 | 2017-10-20 | 合肥市晶谷米业有限公司 | 一种米糠多糖的提取方法 |
CN109608560A (zh) * | 2019-01-24 | 2019-04-12 | 中南林业科技大学 | 一种米糠多糖的提取方法及其制作的饼干和方法 |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1995069A (zh) * | 2006-12-26 | 2007-07-11 | 江南大学 | 一种米糠多糖的分离纯化方法 |
CN1995070A (zh) * | 2006-12-26 | 2007-07-11 | 江南大学 | 一种米糠多糖的超声波提取方法 |
CN103416313A (zh) * | 2013-06-28 | 2013-12-04 | 江苏大学 | 用于米糠和麸皮全料液态发酵生产灰树花多糖的菌株 |
-
2013
- 2013-12-18 CN CN201310694933.0A patent/CN103694368B/zh active Active
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1995069A (zh) * | 2006-12-26 | 2007-07-11 | 江南大学 | 一种米糠多糖的分离纯化方法 |
CN1995070A (zh) * | 2006-12-26 | 2007-07-11 | 江南大学 | 一种米糠多糖的超声波提取方法 |
CN103416313A (zh) * | 2013-06-28 | 2013-12-04 | 江苏大学 | 用于米糠和麸皮全料液态发酵生产灰树花多糖的菌株 |
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104306391A (zh) * | 2014-09-18 | 2015-01-28 | 河北科星药业有限公司 | 米糠多糖口服液、注射液和可溶性粉末及相应的制备方法 |
CN105166626A (zh) * | 2015-09-29 | 2015-12-23 | 江苏锦宇环境工程有限公司 | 一种米糠多糖口含片的制备方法 |
CN107267571A (zh) * | 2017-07-15 | 2017-10-20 | 合肥市晶谷米业有限公司 | 一种米糠多糖的提取方法 |
CN109608560A (zh) * | 2019-01-24 | 2019-04-12 | 中南林业科技大学 | 一种米糠多糖的提取方法及其制作的饼干和方法 |
Also Published As
Publication number | Publication date |
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CN103694368B (zh) | 2015-10-28 |
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Effective date of registration: 20210113 Address after: 570145 room 1506, Yusha international, 11-8 Yusha Road, Longhua District, Haikou City, Hainan Province Patentee after: Quanku (Hainan) Intellectual Property Operation Co.,Ltd. Address before: 050200 No.114 Changsheng street, high tech Industrial Development Zone, Luquan City, Shijiazhuang City, Hebei Province Patentee before: HEBEI KEXING PHARMACEUTICAL Co.,Ltd. |
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Effective date of registration: 20210126 Address after: 050200 No.114 Changsheng street, Luquan Development Zone, Shijiazhuang City, Hebei Province Patentee after: HEBEI KEXING PHARMACEUTICAL Co.,Ltd. Address before: 570145 room 1506, Yusha international, 11-8 Yusha Road, Longhua District, Haikou City, Hainan Province Patentee before: Quanku (Hainan) Intellectual Property Operation Co.,Ltd. |
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Application publication date: 20140402 Assignee: HEBEI GREENLAND ANIMAL PHARMACEUTICAL Co.,Ltd. Assignor: HEBEI KEXING PHARMACEUTICAL Co.,Ltd. Contract record no.: X2024980002827 Denomination of invention: Extraction method of rice bran polysaccharides Granted publication date: 20151028 License type: Common License Record date: 20240314 Application publication date: 20140402 Assignee: Hebei jianjiale duck industry Co.,Ltd. Assignor: HEBEI KEXING PHARMACEUTICAL Co.,Ltd. Contract record no.: X2024980002825 Denomination of invention: Extraction method of rice bran polysaccharides Granted publication date: 20151028 License type: Common License Record date: 20240313 Application publication date: 20140402 Assignee: Shijiazhuang Huifeng Animal Health Products Co.,Ltd. Assignor: HEBEI KEXING PHARMACEUTICAL Co.,Ltd. Contract record no.: X2024980002822 Denomination of invention: Extraction method of rice bran polysaccharides Granted publication date: 20151028 License type: Common License Record date: 20240313 |
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