CN103693942B - Low temperature and fast firing ceramic tile and production technique - Google Patents
Low temperature and fast firing ceramic tile and production technique Download PDFInfo
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- CN103693942B CN103693942B CN201310609264.2A CN201310609264A CN103693942B CN 103693942 B CN103693942 B CN 103693942B CN 201310609264 A CN201310609264 A CN 201310609264A CN 103693942 B CN103693942 B CN 103693942B
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P40/00—Technologies relating to the processing of minerals
- Y02P40/60—Production of ceramic materials or ceramic elements, e.g. substitution of clay or shale by alternative raw materials, e.g. ashes
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Abstract
The present invention relates to low temperature and fast firing ceramic tile and production technique.In this ceramic tile, at least one is that polished tile produces the subparticle material produced in grinding and polishing process; Produce through collecting polishing process the waste water containing subparticle, after precipitation, press filtration process, obtain polished waste material, this ceramic tile is made up of following component by weight percentage: polished waste material 48 ~ 73%; Porcelain sand 5 ~ 20%; Clay 20 ~ 27%; Mineralizer 2 ~ 5%.This production technique comprises: (1) collect polished waste material; Polished waste material for subsequent use for press filtration and other raw material are converted to dry weight, by formula batching, wet ball grinding form slurry; (2) spray drying of slip is made powder, dry-pressing formed ceramic adobe; (3) brick bat drying, glazing surface are decorated; (4) decorative blank is entered ceramic roller kiln to burn till; Its temperature of burning till fast is: 1050 DEG C ~ 1140 DEG C, and firing period 35 ~ 75 minutes, is fired into the porcelain brick that water-intake rate is less than 0.5%.
Description
Technical field
The present invention relates to a kind of low temperature and fast firing ceramic tile and production technique.
Background technology
CN200410079020.9 discloses " a kind of method utilizing polished waste material production ceramic tile ", and its object reasonably re-uses the vitrified tile polished waste material that current ceramic industry produces in a large number.This technical scheme: the waste water produced after the polishing of ceramic industry vitrified tile, waste residue are collected, polished waste material is obtained after precipitation, press filtration and old process, the polished waste material of 10 ~ 70%, 10 ~ 35% high temperature sand, the kaolin of 10 ~ 35%, the low temperature sandstone batch mixing of 10 ~ 30% are entered wet ball grinding in ball mill, cross 250 mesh screen residues 0.3 ~ 0.8%, utilize spray tower to dust in mud after deironing for subsequent use; Then, utilize ceramic press dry-pressing formed in gained dry powder; Ceramic tile base substrate after shaping is burnt till in ceramic roller kiln, firing temperature 1140 DEG C ~ 1200 DEG C, firing period 40 ~ 75 minutes.Its weak point is: final product is also only a kind of light-weight foam brick instead of ceramic tile, and limitation is larger.
Summary of the invention
The object of the invention is the polished waste material produced in the grinding and polishing operation that polished tile is produced for current ceramic industry, its particle fineness is distributed between 1.5 ~ 30 microns, median size is at 6 microns, the foamable reaction of the organism such as resin in sintering process is had because of what bring into containing bistrique in polishing slag, and provide a kind of by collecting the waste water that these contain subparticle, after precipitation, press filtration, in the blank formulation of ceramic tile production; Make full use of the feature that polishing slag particle is thin, specific surface area is large, firing temperature is low, accelerate the physical-chemical reaction of sintering process, the energy consumption of effective reduction ceramic tile, polishing waste is turned waste into wealth, and pass through the effect of low temperature mineralizer, organic volatile part is volatilized by low temperature and avoids further reaction at high temperature, that evades that bistrique in polishing slag brings into has the foamable reaction of the organism such as resin in sintering process, completes the low temperature and fast firing ceramic tile production technique of the porcelain process of burning till of ceramic tile at a lower temperature.Another object of the present invention is to provide a kind of for making in ceramic tile sintering process non-foaming by reduction firing temperature, shortening firing time, evade the nucleation temperature interval that high temperature burns till, after organism is discharged, under the effect of the reduction of solid state reaction temperature and mineralizer, make to be volatilized by low temperature organic volatile part and avoid further reaction at high temperature, complete the low temperature and fast firing ceramic tile of the sintering process of ceramic tile at a lower temperature.
Technical solution of the present invention is described low temperature and fast firing ceramic tile, and its special character is: in described ceramic tile, at least one is that polished tile produces the subparticle material produced in grinding and polishing process; By collecting the waste water containing subparticle that polishing process produces, after precipitation, press filtration process, obtain polished waste material, this ceramic tile is made up of following component by weight percentage:
Polished waste material 48% ~ 73% porcelain sand 5% ~ 20%
Clay 20% ~ 27% mineralizer 2% ~ 5%.
As preferably:
Described ceramic tile by weight percentage, is made up of following component further:
Polishing slag 65% porcelain sand 13%
Clay 20% wollastonite 2%.
As preferably: described mineralizer selects one or its combination: the low temperature flux raw material of wollastonite, diopside, talcum, triphane class.
Another technical solution of the present invention is the production technique of described low temperature and fast firing ceramic tile, and its special character is, comprises following operation:
(1) collect polished waste material; Polished waste material for subsequent use for press filtration and other raw material are converted to dry weight, by formula per-cent batching, wet ball grinding form slurry;
(2) spray drying of slip is made powder, dry-pressing formed ceramic adobe;
(3) brick bat drying, glazing surface are decorated;
(4) decorative blank is entered ceramic roller kiln to burn till; Its temperature of burning till: 1050 DEG C ~ 1140 DEG C, firing period 35 ~ 75 minutes, is fired into the porcelain brick that water-intake rate is less than 0.5%.
As preferably: the subparticle composition of described polished waste material is distributed between 1.5 ~ 30 microns, and median size is 6 microns.
As preferably: described operation surface decoration means (3), according to product decoration effect, adopt wherein a kind of or its combination: glaze spraying, drench glaze, silk screen, rubber roll, ink-jet printed, charity dry granular and finished bricks glaze paint glossing.
As preferably: described production method comprises further:
(1) collect polishing slag for subsequent use and detect moisture, enter ball mill goal grinding machine after batching is converted to the blank of butt, the wet-milling that adds water becomes mud, and the particle that moil fineness is greater than 40 microns is less than 2.50%, mud speed rate: 41 seconds/100ml; Mud moisture content: 34.0%, through sieving, deironing enters stock tank and stores for future use;
By the moisture controlled of powder 6% ~ 7%, unit weight 0.98 g/ml, dry-pressing formedly makes adobe and dry, decorates, send into ceramic roller kiln and burn till the surface of dry base;
(3) utilize ceramic roller kiln to burn till, firing temperature 1080 DEG C, firing period 45 minutes, product water-intake rate is less than 0.50%, makes porcelain brick finished product.
As preferably: the collection method of described polished waste material comprises:
(1) collect the waste water containing subparticle of rough polishing, the generation of essence throwing operation;
(2) waste water enters settling tank, precipitation by ditch;
(3) add flocculation agent in settling tank;
(4) the waste water in I and II settling tank send edging operation recycle;
(5) the high concentration ground paste in three grades of settling tanks is sent to pressure filter, and press filtration becomes mud cake;
(6) mud cake roll-over, homogenizing, old, for the blank of low-temperature sintering ceramic brick.
Compared with prior art, advantage of the present invention is:
(1) the firing temperature of low-temperature sintering ceramic brick of the present invention is: 1050 DEG C ~ 1140 DEG C, and firing period 35 ~ 75 minutes, is fired into the porcelain brick that water-intake rate is less than 0.5%.Compare traditional processing technology and reduce by 80 DEG C, firing period can shorten 15 ~ 20 minutes, reduces and burns till energy consumption 17% ~ 20%.Thus reduce fuel consumption, the energy-saving and emission-reduction of transforming traditional china industry and industry with modern technique are significant.
(2) the invention solves the waste material that in polishing slag, grinding and polishing part produces, because containing a certain amount of grinding head for polishing loss in its composition, causing ceramic tile sintering process to foam, and the key issue that can not be widely used; Solve porcelain brick and burn till the key problem in technology problem such as product foaming, distortion in high-temperature liquid-phase sintering situation, the full ceramic tile for low water absorption is produced, and tile polished waste is applied in the porcelain brick blank of low temperature and fast firing.
(3) its particle of waste material that grinding and polishing process produces is thin, specific surface area large, and this fine particle reduces the temperature of high temperature solid state reaction, for reducing firing temperature, shortening the effect that firing time plays key.
(4) grinding and polishing process produce waste material contain the organic compositions such as resin, this technique has evaded the temperature range of the foaming that high temperature burns till, make organism discharge after, solid state reaction temperature reduce and mineralizer effect under, complete the sintering process of the porcelain of base substrate.
(5) the mineralizer in the blank formulation of low-temperature sintering ceramic brick of the present invention is wollastonite, diopside, talcum or containing one or more in lithium minerals raw material, amount ranges is 2% ~ 5%.Compare the chemical constitution of traditional porcelain adobe material, the introducing containing raw mineral materialss such as lithium, calcium, magnesium has certain guarantee effect for promotion low-temperature sintering.
(6) the present invention widely applies the waste material that polished tile production process produces, unsolved polished waste material discharge (maybe can only be used for light cinder brick) is for many years turned waste into wealth, achieve the application of polishing slag in porcelain brick blank formulation, expand the amount ranges of polishing slag, for ceramic polished brick manufacturing enterprise provides a kind of utilisation technology of polishing slag zero release, be less than in 0.5% porcelain brick formula for water-intake rate, firing temperature 80 DEG C can be reduced, firing period can shorten 10 ~ 20 minutes, ceramic industry energy-saving and emission-reduction are significant, great discovery and the innovation of ceramic raw material and production technique.Compare the firing temperature of traditional porcelain brick between 1180 DEG C ~ 1240 DEG C, firing period 60 ~ 90 points, consumption 17% ~ 20% capable of saving fuel.
(7) the present invention is applied in porcelain glazed tile blank formulation, and its quality meets standard GB/T/T41
The requirement of 00-2006 " ceramic tile " annex G.
(8) the present invention provides a kind of solution of the porcelain brick blank formulation for low temperature fast firing to the polishing slag that current ceramic industry produces in a large number, this solution takes full advantage of that polishing slag particle is thin, specific surface area is large, and the feature that under having evaded high temperature, organic resin binding agent bubbles, reduce the firing temperature of porcelain brick, can realize the consumption 17% ~ 20% of the energy, the waste of polishing is simultaneously turned waste into wealth thus.This invention proposes important approach for reference for the disposal and utilization of ceramic industry especially polished tile factory polishing slag.
Accompanying drawing explanation
Fig. 1 is the technological process of production schematic diagram of low temperature and fast firing ceramic tile of the present invention.
Fig. 2 is that the polishing slag of low temperature and fast firing ceramic tile of the present invention collects schematic diagram.
Embodiment
The present invention is further detailed in conjunction with the accompanying drawings below:
In described ceramic tile, at least one is that polished tile produces the subparticle material produced in grinding and polishing process; By collecting the waste material containing subparticle that polishing process produces, after precipitation, press filtration process, obtain polished waste material; The collection method of polished waste material comprises:
(1) collect the waste water containing subparticle of rough polishing, the generation of essence throwing operation;
(2) waste water enters settling tank, precipitation by ditch;
(3) add flocculation agent in settling tank;
(4) the waste water in I and II settling tank send edging operation recycle;
(5) the high concentration ground paste in three grades of settling tanks is sent to pressure filter, and press filtration becomes mud cake;
(6) mud cake roll-over, homogenizing, old, for the blank of low-temperature sintering ceramic brick.
The chemical composition composition of tile polished waste, be the fabric composition of polished brick in porcelain character substantially, difference wears away containing grinding head for polishing the organic binder bond composition brought in composition, and composition display loss on ignition increases to some extent:
Loss on ignition 3.0% ~ 3.5%; SiO
2: 68% ~ 72%; Al
2o
3: 17% ~ 22%; Na
2o+K
2o: 3% ~ 5.5%; CaO:0.5% ~ 1.0; MgO:1% ~ 2.5%.
[embodiment 1] low temperature and fast firing ceramic tile and the first production technique:
(1) detecting moisture by collecting polishing slag for subsequent use, preparing burden by weight percentage, being converted to the blank formulation of butt: polishing slag 65%, clay 20%, porcelain sand 13%, wollastonite 2%; Admixture: Xylo-Mucine 0.08%, trimerization 0.06%%, Sodium salts humic acids 0.03%, water glass 0.25%; To prepare burden into ball mill, the wet-milling that adds water becomes mud, and the particle that mud is greater than 40 microns is less than 2.30%(i.e. 325 mesh screen residues 2.3%), through sieving, deironing enters stock tank and stores for future use.
(2) spraying dry prepares powder, and the moisture controlled of powder is 6% ~ 7%, and unit weight 0.98%, dry-pressing formed adobe also drying of making 330 mm × 330mm, thickness 9.6 mm ± 0.3mm, decorates the surface of dry base, send into ceramic roller kiln and burn till.
(3) utilize ceramic tile roller kiln to burn till, firing temperature 1080 DEG C, firing period 45 minutes, product water-intake rate is 0.42%, and product appearance quality and physical and chemical performance meet GB/T4100-2006 " ceramic tile " annex G standard-required.
[embodiment 2] low temperature and fast firing ceramic tile and the second production technique:
(1) polishing slag 50%, clay 23%, porcelain sand 17%, wollastonite 3%, wilkinite 2%, high temperature potassium sand 5% are prepared burden, ball milling slurrying; Additional Xylo-Mucine 0.1%, trimerization 0.2%, wet ball grinding becomes mud, detect fineness be greater than 40 microns be 2.14% (325 mesh screen residue 2.14%), mud through deironing, sieve, be delivered to spray tower, be dried to powder and store for future use;
(2) powder is utilized the existing KD3800 hydraulic press of production line, be pressed into that specification is 600 × 600mm, drying is carried out in the adobe of thickness 10.0 ± 0.3mm, by executing ground-coat enamel, cover-coat enamel, ink-jet is decorated, and is conveyed into roller kiln and burns till, firing temperature 1140 DEG C by Multi-functional ornamental moulding, firing period 60 minutes, make porcelain brick finished product, water-intake rate is 0.32%, and quality product meets GB/T4100 ~ 2006 " ceramic tile " annex G standard-required.
The foregoing is only preferred embodiment of the present invention, all equalizations done according to the claims in the present invention scope change and modify, and all should belong to the covering scope of the claims in the present invention.
Claims (4)
1. a production technique for low temperature and fast firing ceramic tile, comprises following operation:
(1) collect polished waste material; Polished waste material for subsequent use for press filtration and other raw material are converted to dry weight, wherein, in the composition of tile polished waste, wear away containing grinding head for polishing the organic binder bond composition brought into, the increase of organic binder bond composition display loss on ignition: loss on ignition 3.0% ~ 3.5%; The chemical composition composition of tile polished waste: SiO
2: 68% ~ 72%; Al
2o
3: 17% ~ 22%; Na
2o+K
2o: 3% ~ 5.5%; CaO:0.5% ~ 1.0%; MgO:1% ~ 2.5%; By the polished waste material of 48% ~ 73%, the porcelain sand of 5% ~ 20%, the clay of 20% ~ 27% and 2% ~ 5% mineralizer batch mixing, wet ball grinding form slurry; The subparticle composition of described polished waste material is distributed between 1.5 ~ 30 microns, and median size is 6 microns;
(2) collect polished waste material for subsequent use and detect moisture, enter ball mill after batching is converted to the blank of butt, the wet-milling that adds water becomes mud, and the particle that moil fineness is greater than 40 microns is less than 2. 50%, the flow velocity of mud: 32 ~ 41 seconds/100ml; Mud moisture content: 33 ~ 35.0%, through sieving, deironing enters stock tank and stores for future use;
It is characterized in that:
(3) spray drying of slip is made powder, then by the moisture controlled of powder 6% ~ 7%, unit weight 0.98g/ml, dry-pressing formedly make adobe;
(4) brick bat drying, glazing surface are decorated; Described surface decoration means, according to product decoration effect, adopt wherein a kind of or its combination: glaze spraying, drench glaze, silk screen, rubber roll, ink-jet printed, charity dry granular and finished bricks glaze paint glossing;
(5) decorative blank is entered ceramic roller kiln to burn till, firing temperature 1080 DEG C, firing period 45 minutes, product water-intake rate is less than 0.50%, makes porcelain brick finished product.
2. the production technique of low temperature and fast firing ceramic tile according to claim 1, the collection method of described polished waste material comprises:
(1) collect the waste water containing subparticle of rough polishing, the generation of essence throwing operation;
It is characterized in that:
(2) waste water enters settling tank, precipitation by ditch;
(3) add flocculation agent in settling tank;
(4) the waste water in I and II settling tank send edging operation recycle;
(5) the high concentration ground paste in three grades of settling tanks is sent to pressure filter, and press filtration becomes mud cake;
(6) mud cake roll-over, homogenizing, old, for the blank of low-temperature sintering ceramic brick.
3. the ceramic tile made of the production technique of low temperature and fast firing ceramic tile according to claim 1, in described ceramic tile, at least one is that polished tile produces the subparticle material produced in grinding and polishing process; By collecting the waste water containing subparticle that polishing process produces, after precipitation, press filtration process, obtaining polished waste material, it is characterized in that: this ceramic tile is made up of following component by weight percentage:
Polished waste material 48% ~ 73% porcelain sand 5% ~ 20% clay 20% ~ 27%
Mineralizer 2% ~ 5%;
Its firing temperature: 1080 DEG C, firing period 45 minutes; Described mineralizer selects one or its combination: the low temperature flux raw material of wollastonite, diopside, talcum, triphane class.
4. low temperature and fast firing ceramic tile according to claim 3, is characterized in that: described ceramic tile by weight percentage, is made up of following component further:
Polished waste material 65% porcelain sand 13% clay 20%
Wollastonite 2%.
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Inventor after: Huang Jianping Inventor after: Chen Zhichuan Inventor after: Wang Yongqiang Inventor after: Yang Fuwei Inventor after: Wang Ruifeng Inventor after: Liu Xuebin Inventor after: Fu Changqing Inventor before: Huang Jianping Inventor before: Xie Yuezeng Inventor before: Wang Yongqiang Inventor before: Chen Zhichuan Inventor before: Yang Fuwei Inventor before: Li Jiongzhi Inventor before: Man Lizhu |
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Free format text: CORRECT: INVENTOR; FROM: HUANG JIANPING XIE YUEZENG WANG YONGQIANG CHEN ZHICHUAN YANG FUWEI LI JIONGZHI MAN LIZHU TO: HUANG JIANPING CHEN ZHICHUAN WANG YONGQIANG YANG FUWEI WANG RUIFENG LIU XUEBIN FU CHANGQING |
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