CN103691397A - Rosemary porous particles and application thereof in cigarettes - Google Patents
Rosemary porous particles and application thereof in cigarettes Download PDFInfo
- Publication number
- CN103691397A CN103691397A CN201310643991.0A CN201310643991A CN103691397A CN 103691397 A CN103691397 A CN 103691397A CN 201310643991 A CN201310643991 A CN 201310643991A CN 103691397 A CN103691397 A CN 103691397A
- Authority
- CN
- China
- Prior art keywords
- rosemary
- porous particle
- mingrosma rinus
- xue mingrosma
- rinus officinalis
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Landscapes
- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
Abstract
The invention discloses rosemary porous particles and application thereof in cigarettes. Rosemary powder, of which the water content is 7-9% and the particle size is 100-160 meshes, is used as the raw material to prepare the rosemary porous particle with the particle size of 20-60 meshes by a fluidized bed top shower technique by using one or more of sodium methyl starch and gelatin as an adhesive. The particles have coarse surfaces and higher specific area, thereby obviously enhancing the effective contact area between the particle material and the cigarette smoke; the particles can selectively adsorb ammonia in the cigarette smoke; and on the premise of having the function of reducing harmful substances, the particles can enrich the smoke flavors of cigarettes and enhance the sweetness, and meanwhile, have the effect of enhancing the inductivity of the smoke. The production technique is simple, has the advantages of high operability, high normalization, accessible raw materials and low cost, can conveniently implement industrialized production, and has favorable application prospects.
Description
Technical field
The invention belongs to cigarette material technical field, be specifically related to a kind of rosemary, Xue MingRosma rinus officinalis porous particle that can improve flavor quality of cigarette.Meanwhile, the invention still further relates to the application of this porous particle in Cigarette processing.
Background technology
Rosemary, Xue MingRosma rinus officinalis another name tansy, for Labiatae Rosmarinus perennial evergreen undershrub, originates in Mediterranean, in the China that induces one in 1981, at present in Yunnan, there is large area plantation on the ground such as Guizhou, Guangxi, Hainan and Xinjiang.In rosemary, Xue MingRosma rinus officinalis medicinal material, be rich in volatile oil, its volatile oil has well antibacterial, anti-inflammatory, the effect such as antitumor, can be used as stomachic tonic and cholagog, can effectively alleviate the gasteremphraxis being caused by indigestion, alleviate small intestine and biliary tract spasm, strengthen colonic muscle and shrink, promote choleresis.In natural rosemary, Xue MingRosma rinus officinalis blade, contain multiple fragrance composition, mainly be divided into terpene, flavonoids, organic acid and essential oil class etc., it has strong armaticity smell, be widely used in daily-use chemical industry and food industry flavouring, simultaneously these flavor components with tobacco flavor composition can be coordinated mutually, supplementary, the relevant report that existing Rosmarinus officinalis extract is applied in cigarette, but the less report of seeing about its blade and stalk integrated application.
Along with smoking and healthy problem more and more receive publicity, how to improve the security of sucking of cigarette, the comfort that reduce harmful components in cigarette smoke, improves suction just becomes the focus of each tobacco productive corporation research and development.Cigarette material researcher utilizes natural plant material to develop some filter stick granular materials, the main mode adopting is directly vegetable material is ground into the particle between 20～80 orders or vegetable material is prepared into particle by extrusion, although obtaining certain effect aspect cigarette flavouring, harm reduction, but also there is the shortcoming of the following aspects: (1) is directly ground into particle by vegetable material, grain shape is inhomogeneous, physical instability, when cigarette filter tip shaping, thereby particle is easily made broken a large amount of dust that produce, and stock utilization is not high; (2) by extrusion, prepare particle, the hole embedding that the adhesive adding easily has vegetable material itself, the contact area of granular materials and cigarette smoke reduces, its lowering harm and decreasing coking effect is limited, simultaneously prepared particle is comparatively tight, hardness is larger, is unfavorable for the preparation of cigarette composite filter.For above-mentioned shortcoming, how to adopt suitable technology, preparation is applicable to the plant porous material of Production requirement, to meet tobacco business in the demand aspect cigarette flavouring, harm reduction, just becomes this area and waits the technical barrier solving.
Summary of the invention
The object of the invention is to for the deficiencies in the prior art, provide that a kind of resistance to processability is strong, uniform particles, safe, flavouring successful, there is the rosemary, Xue MingRosma rinus officinalis porous particle of certain harm reduction effect.
The present invention also aims to provide the application of described rosemary, Xue MingRosma rinus officinalis porous particle in production of cigarettes.
Object of the present invention is achieved by following technical proposals.
* except as otherwise noted, the percentage adopting in the present invention is mass percent.
A rosemary, Xue MingRosma rinus officinalis porous particle, the method by following steps makes:
(1) blade of fresh rosemary, Xue MingRosma rinus officinalis being adjusted to moisture with stalk under 20～25 ℃ of temperature, humidity 30%～40% condition is 7～9%, then further pulverizing is respectively 100～160 object powder, by blade powder and stalk powder, ratio according to parts by weight 60～70:30～40 mixes, standby;
(2) according to weight portion, take 6～8 parts of sodium carboxymethyl starches, 0～2 part, gelatin, with distilled water, being mixed with concentration is 6～10% binder solution, standby;
(3) take standby powder from rosemary 300～1000g and be placed in fluid bed granulation, prilling specifically comprises the steps:
(a) at fluidisation air pressure, be to keep 5～10 minutes under 0.15Bar, the condition of 50 ℃;
(b) 50～60 ℃ of fluidisation air pressure 0.12～0.15Bar, gas flow temperatures, under atomisation pressure 0.10～0.12Bar, the hydrojet speed condition of 10～12g/ minute, adopt top spray mode to apply the binder solution that step (2) is prepared, binder solution consumption is 40%～50% of dry material weight;
(c) after adhesive has applied, under fluidisation air pressure 0.12～0.2Bar, 50 ℃ of conditions of gas flow temperature, be dried 10～12 minutes, preparing moisture is 8～10%, and shaggy similar round particle is required rosemary, Xue MingRosma rinus officinalis porous particle.
Wherein, prepared its particle diameter of rosemary, Xue MingRosma rinus officinalis porous particle is 20～60 orders.
Described fluid bed is preferably Midi Glatt fluid bed.
Described rosemary, Xue MingRosma rinus officinalis porous particle is applied in cigarette filter rod, it is characterized in that: the rosemary, Xue MingRosma rinus officinalis porous particle that adds 1～2mg in every millimeter of cigarette filter rod.
Compared with prior art, the present invention has the following advantages:
1. prepared uniform particles, physicochemical property are stable, have good resistance to processability, have avoided granular materials in filter stick formation process to make broken and dust because of what machining produced, and granular materials can be uniformly distributed in filter stick tow.
2. rough, has higher specific area, significantly improves effective contact area of granular materials and cigarette smoke, the ammonia in can selective absorption cigarette smoke.
3. this particle can effectively enrich cigarette cigarette perfume, strengthen sweet sense, has the flue gas of the lifting effect of the property sent out thoroughly simultaneously.
4. the material that uses is food stage, has higher safety in utilization.
5. production technology is simple, and operability and standardization are strong, and raw material is easy to get, with low cost, is convenient to realize suitability for industrialized production, has application prospect well.
The specific embodiment
In order to make object of the present invention, technical scheme and advantage clearer, below in conjunction with embodiment, the present invention is described in further detail.Should be appreciated that specific embodiment described herein, only in order to explain the present invention, is not limited to the technical solution.
Embodiment 1
Blade and the stalk of getting fresh rosemary, Xue MingRosma rinus officinalis are that 20 ℃, humidity are under 30% condition in temperature, being adjusted to moisture is 7%, by blade and stalk pulverizing, be 100 object powder respectively again, according to blade powder: the part by weight of stalk powder=60:40 mixes, mixed powder 1000g is placed in to the granulation of Midi Glatt fluid bed, and fluid bed fluidisation air pressure is to keep 10 minutes under 0.15Bar, 50 ℃ of conditions; Then distilled water is mixed with to concentration and is 8% sodium carboxymethyl starch binder solution, at fluidisation air pressure, be that 0.15Bar, gas flow temperature are 60 ℃, atomisation pressure is that 0.12Bar, hydrojet speed are under 10g/ minute condition, adopts top spray mode to spray 400g binder solution; After adhesive has applied, setting fluidisation air pressure 0.2Bar, gas flow temperature are to be dried 12 minutes under 50 ℃ of conditions, and moisture is adjusted to 8%, cross 60 mesh sieves and obtain cigarette filter rod rosemary, Xue MingRosma rinus officinalis porous particle.
Embodiment 2
Blade and the stalk of getting fresh rosemary, Xue MingRosma rinus officinalis are that 25 ℃, humidity are under 40% condition in temperature, being adjusted to moisture is 9%, by blade and stalk pulverizing, be 120 object powder respectively again, according to blade powder: the part by weight of stalk powder=70:30 mixes, mixed powder 500g is placed in to the granulation of Midi Glatt fluid bed, and fluid bed fluidisation air pressure is to keep 8 minutes under 0.15Bar, 50 ℃ of conditions; Then according to weight portion, take 8 parts of sodium carboxymethyl starches, 2 parts, gelatin, with distilled water, being mixed with concentration is 10% binder solution, at fluidisation air pressure, be that 0.12Bar, gas flow temperature are that 60 ℃, atomisation pressure are that 0.10Bar, hydrojet speed are under 12g/ minute condition, adopt top spray mode to spray 200g binder solution; After adhesive has applied, setting fluidisation air pressure 0.15Bar, gas flow temperature are to be dried 10 minutes under 50 ℃ of conditions, and moisture is adjusted to 9%, cross 40 mesh sieves and obtain cigarette filter rod rosemary, Xue MingRosma rinus officinalis porous particle.
Embodiment 3
Blade and the stalk of getting fresh rosemary, Xue MingRosma rinus officinalis are that 22 ℃, humidity are under 35% condition in temperature, being adjusted to moisture is 8%, by blade and stalk pulverizing, be 160 object powder respectively again, according to blade powder: the part by weight of stalk powder=65:35 mixes, powder 300g after mixing is placed in to the granulation of Midi Glatt fluid bed, and fluid bed fluidisation air pressure is to keep 5 minutes under 0.15Bar, 50 ℃ of conditions; Then according to weight portion, take 6 parts of sodium carboxymethyl starches, 2 parts, gelatin, with distilled water, being mixed with concentration is 8% binder solution, at fluidisation air pressure, be that 0.12Bar, gas flow temperature are that 55 ℃, atomisation pressure are that 0.10Bar, hydrojet speed are under 10g/ minute condition, adopt top spray mode to spray 150g binder solution; After adhesive has applied, setting fluidisation air pressure 0.12Bar, gas flow temperature are to be dried 10 minutes under 50 ℃ of conditions, and moisture is adjusted to 10%, cross 20 mesh sieves and obtain cigarette filter rod rosemary, Xue MingRosma rinus officinalis porous particle.
Application Example 1
Embodiment 1 is prepared to gained rosemary, Xue MingRosma rinus officinalis porous particle and be applied in cigarette composite filter, every millimeter of cigarette filter rod adds 1mg granular materials, is prepared into experiment cigarette, and the cigarette of not adding above-mentioned particle of take is carried out sensory evaluating smoking and harmful ingredients in flue gas detects as contrast.Analyses Methods for Sensory Evaluation Results shows: compared with the control, the cigarette fragrance that adds above-mentioned porous particle is abundanter, pleasant impression be improved significantly, the flue gas thoroughly property sent out obviously promotes; Harmful ingredients in flue gas detects and to show: ammonia reduced rate is 19.6%, and other harmful components change little, the ammonia of this porous particle in can selective absorption cigarette smoke.
Application Example 2
Embodiment 2 is prepared to gained rosemary, Xue MingRosma rinus officinalis porous particle and be applied in cigarette composite filter, every millimeter of cigarette filter rod adds 2mg granular materials, is prepared into experiment cigarette, and the cigarette of not adding above-mentioned particle of take is carried out sensory evaluating smoking and harmful ingredients in flue gas detects as contrast.Analyses Methods for Sensory Evaluation Results shows: compared with the control, the cigarette fragrance that adds above-mentioned porous particle is abundanter, and sweet sense significantly strengthens, and the flue gas thoroughly property sent out obviously promotes; Harmful ingredients in flue gas detects and to show: ammonia reduced rate is 26.4%, and other harmful components change not obvious, this porous particle can selective absorption cigarette smoke in ammonia.
Application Example 3
Embodiment 3 is prepared to gained rosemary, Xue MingRosma rinus officinalis porous particle to be applied in cigarette composite filter, every millimeter of cigarette filter rod adds 1.5mg granular materials, be prepared into experiment cigarette, the cigarette of not adding above-mentioned particle of take is carried out sensory evaluating smoking and harmful ingredients in flue gas detects as contrast.Analyses Methods for Sensory Evaluation Results shows: compared with the control, the cigarette flue gas excitant of adding above-mentioned porous particle obviously reduces, pleasant impression be improved significantly, the flue gas thoroughly property sent out obviously promotes; Harmful ingredients in flue gas detects and to show: ammonia reduced rate is 22.8%, and other harmful components change not obvious, the ammonia of this porous particle in can selective absorption cigarette smoke.
The foregoing is only preferred embodiment of the present invention, not in order to limit the present invention, all any modifications of doing within the spirit and principles in the present invention, be equal to and replace and improvement etc., within all should being included in protection scope of the present invention.
Claims (4)
1. a rosemary, Xue MingRosma rinus officinalis porous particle, the method by following steps makes:
(1) blade of fresh rosemary, Xue MingRosma rinus officinalis being adjusted to moisture with stalk under 20～25 ℃ of temperature, humidity 30%～40% condition is 7～9%, then further pulverizing is respectively 100～160 object powder, according to blade powder: the part by weight of stalk powder=60～70:30～40 mixes rear standby;
(2) according to weight portion, take 6～8 parts of sodium carboxymethyl starches, 0～2 part, gelatin, with distilled water, being mixed with concentration is 6～10% binder solution, standby;
(3) take standby powder from rosemary 300～1000g and be placed in fluid bed granulation, prilling specifically comprises the steps:
(a) at fluidisation air pressure, be to keep 5～10 minutes under 0.15Bar, the condition of 50 ℃;
(b) 50～60 ℃ of fluidisation air pressure 0.12～0.15Bar, gas flow temperatures, under atomisation pressure 0.10～0.12Bar, the hydrojet speed condition of 10～12g/ minute, adopt top spray mode to apply the binder solution that step (2) is prepared, binder solution consumption is 40%～50% of dry material weight;
(c) after adhesive has applied, under fluidisation air pressure 0.12～0.2Bar, 50 ℃ of conditions of gas flow temperature, be dried 10～12 minutes, preparing moisture is 8～10%, and shaggy similar round particle is required rosemary, Xue MingRosma rinus officinalis porous particle.
2. rosemary, Xue MingRosma rinus officinalis porous particle according to claim 1, is characterized in that: prepared its particle diameter of rosemary, Xue MingRosma rinus officinalis porous particle is 20～60 orders.
3. rosemary, Xue MingRosma rinus officinalis porous particle according to claim 1, is characterized in that: described fluid bed is preferably Midi Glatt fluid bed.
4. rosemary, Xue MingRosma rinus officinalis porous particle claimed in claim 1 is applied in cigarette filter rod, it is characterized in that: the rosemary, Xue MingRosma rinus officinalis porous particle that adds 1～2mg in every millimeter of cigarette filter rod.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310643991.0A CN103691397B (en) | 2013-12-03 | 2013-12-03 | Rosemary porous particles and application thereof in cigarettes |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310643991.0A CN103691397B (en) | 2013-12-03 | 2013-12-03 | Rosemary porous particles and application thereof in cigarettes |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103691397A true CN103691397A (en) | 2014-04-02 |
| CN103691397B CN103691397B (en) | 2015-06-17 |
Family
ID=50353156
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201310643991.0A Active CN103691397B (en) | 2013-12-03 | 2013-12-03 | Rosemary porous particles and application thereof in cigarettes |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN103691397B (en) |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102553543A (en) * | 2012-02-20 | 2012-07-11 | 丰顺县洋西坑生态农业科技有限公司 | Cigarette filter tip adsorbing material and preparation method thereof |
| CN102860586A (en) * | 2011-07-04 | 2013-01-09 | 湖北中烟工业有限责任公司 | Non-woven fabric filter tip material with materia medica incense smoke and preparation method thereof |
| EP1478248B1 (en) * | 2002-02-22 | 2013-03-13 | Philip Morris Products S.A. | Flavored carbon useful as filtering material of smoking article |
-
2013
- 2013-12-03 CN CN201310643991.0A patent/CN103691397B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP1478248B1 (en) * | 2002-02-22 | 2013-03-13 | Philip Morris Products S.A. | Flavored carbon useful as filtering material of smoking article |
| CN102860586A (en) * | 2011-07-04 | 2013-01-09 | 湖北中烟工业有限责任公司 | Non-woven fabric filter tip material with materia medica incense smoke and preparation method thereof |
| CN102553543A (en) * | 2012-02-20 | 2012-07-11 | 丰顺县洋西坑生态农业科技有限公司 | Cigarette filter tip adsorbing material and preparation method thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN103691397B (en) | 2015-06-17 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN103689802B (en) | Tobacco porous particle and application thereof in cigarette | |
| CN103689801B (en) | Kudzuvine root porous particles and application thereof to cigarettes | |
| CN101822425B (en) | Preparation method of cigarette absorption type flavor compensation material | |
| CN105595421B (en) | A kind of cigarette filter rod plant compound granular and preparation method thereof | |
| CN103876285A (en) | Fragrance enhanced granular additive for filter sticks and preparation method and application thereof | |
| CN102911408B (en) | Method for preparing pearl-powder composite porous starch crystalline particles and application of pearl-powder composite porous starch crystalline particles to cigarette filtering tip | |
| CN103704882B (en) | Cocoa shell porous particles and application thereof in cigarettes | |
| CN103689796B (en) | Lemon grass porous particle and application thereof to cigarettes | |
| CN103222678A (en) | Method for preparing agilawood-sheet health care cut tobacco | |
| CN103932394A (en) | Multi-section composite cigarette filtering stick, preparation method thereof and application of turgid plant granules | |
| CN103876286A (en) | Filter rod particle additive with coffee or cocoa flavor and preparation method and application thereof | |
| CN103689785B (en) | A kind of offal porous particle and the application in cigarette thereof | |
| CN101912161B (en) | Mint tobacco filter stick and preparation method thereof | |
| CN103689795B (en) | Peony porous particle and application thereof to cigarettes | |
| CN1442096A (en) | Cigarette containing loess and its manufacturing method | |
| CN103720045A (en) | Functional film composite particle, manufacturing method and filter stick formed by functional film composite particle | |
| CN103689794B (en) | Pelargonium graveolens porous particle and application thereof to cigarette | |
| CN106666825B (en) | A kind of cigarette filter rod preparation method for adding yew plants particle | |
| CN103695174B (en) | Violet porous particles and application thereof in cigarettes | |
| CN103689799B (en) | Radix ophiopogonis porous particle and application thereof to cigarettes | |
| CN103691397B (en) | Rosemary porous particles and application thereof in cigarettes | |
| CN103689798B (en) | Gingko leaf porous particle and application thereof in cigarette | |
| CN104801276A (en) | Gastrodia elata porous particle and applications thereof | |
| CN104705786A (en) | Stem particles capable of improving taste of cigarette and preparation method and application thereof | |
| CN104801277A (en) | Bombax ceiba flower porous particle and applications thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant |