CN103691397B - Rosemary porous particles and application thereof in cigarettes - Google Patents

Rosemary porous particles and application thereof in cigarettes Download PDF

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CN103691397B
CN103691397B CN201310643991.0A CN201310643991A CN103691397B CN 103691397 B CN103691397 B CN 103691397B CN 201310643991 A CN201310643991 A CN 201310643991A CN 103691397 B CN103691397 B CN 103691397B
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rosemary
porous particles
cigarette
powder
mesh
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CN103691397A (en
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张伟
者为
朱保昆
王坚
宫玉鹏
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红云红河烟草(集团)有限责任公司
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Abstract

本发明公开了一种迷迭香多孔颗粒及其在卷烟中的应用。 The present invention discloses a porous particle rosemary and its application in cigarette. 以水分含量7~9%、粒径为100~160目的迷迭香粉末为原料,以甲基淀粉钠、明胶中的一种或几种作为粘合剂,采用流化床顶喷工艺制备得到20~60目的迷迭香多孔颗粒。 To give a moisture content of 7 to 9%, particle size of 100 to 160 mesh rosemary powder as raw materials, sodium starch glycolate, one or more of gelatin as a binder was prepared using a fluid bed top spray process 20 ~ 60 mesh rosemary porous particles. 该颗粒表面粗糙,具有较高的比表面积,显著提高颗粒材料与卷烟烟气的有效接触面积,能够选择性吸附卷烟烟气中的氨;在具有减害功能的同时,该颗粒能够丰富卷烟烟香、增强甜润感,同时具有提升烟气透发性的功效。 The rough surface of the particles, having a high specific surface area, significantly increase the effective contact area of ​​cigarette smoke and particulate material capable of selectively adsorbing ammonia in cigarette smoke; while having a function harm reduction, the cigarette smoke particle can enrich fragrant, sweet enhance a sense, through the hair also has to enhance the effectiveness of smoke. 本发明生产工艺简单,操作性及规范性强,原料易得、成本低廉,便于实现工业化生产,具有良好地应用前景。 Production process is simple, operability and strong normative, raw materials, low cost, ease of industrial production, having a good prospect.

Description

一种迷迭香多孔颗粒及其在卷烟中的应用 A porous particles and its application in cigarette rosemary

技术领域 FIELD

[0001] 本发明属于卷烟材料技术领域,具体涉及一种能够改善卷烟吸味品质的迷迭香多孔颗粒。 [0001] The present invention belongs to the technical field of tobacco material, particularly relates to an improved cigarette smoking quality rosemary porous particles. 同时,本发明还涉及该多孔颗粒在卷烟加工中的应用。 Also, the present invention further relates to the use of the porous particles in cigarette processing.

背景技术 Background technique

[0002] 迷迭香别名艾菊,为唇形科迷迭香属多年生常绿小灌木,原产于地中海沿岸,于1981年引人中国,目前在云南、贵州、广西、海南和新疆等地都有大面积栽种。 [0002] Rosemary alias tansy, Labiatae Rosemary is a perennial evergreen shrub native to the Mediterranean coast, was introduced into China in 1981, currently in Yunnan, Guizhou, Guangxi, Hainan and Xinjiang has a large area planted. 迷迭香药材中富含挥发油,其挥发油具有很好的抗菌、消炎、抗肿瘤等功效,可作为健胃药及利胆剂,能有效缓解由消化不良引起的胃胀,缓解小肠和胆道痉挛,增强结肠肌收缩,促进胆汁分泌。 Rosemary herbs rich in volatile oils, the volatile oil has a good anti-bacterial, anti-inflammatory, anti-tumor efficacy, as choleretic and stomachic agent, can effectively relieve indigestion caused by the bloating, intestinal and biliary spasm mitigation enhanced colonic muscle contraction, promote bile secretion. 天然迷迭香叶片中含有多种香味成分,主要分为萜类、黄酮类、有机酸类和精油类等,其具有浓郁的芳香性气味,广泛用于日用化工及食品工业增香,同时这些香味成分与烟草香味成分能够相互协调、补充,已有迷迭香提取物在卷烟中应用的相关报道,但较少见到关于其叶片和梗综合应用的报道。 Rosemary leaves contain a variety of natural flavor ingredients, mainly divided into terpenoids, flavonoids, organic acids and essential oils, etc., which has a strong aromatic odor, widely used in daily chemical and food industry aroma, while these flavor components of tobacco flavor components can be coordinated, complementary, there are reports of rosemary extract for use in cigarettes, but less likely to see reports on its leaves and stems integrated application.

[0003] 随着吸烟与健康的问题越来越受到关注,如何提高卷烟的吸食安全性,降低卷烟烟气中的有害成分、提高抽吸的舒适感就成为各卷烟生产企业研发的热点。 [0003] As the smoking and health is a growing concern, how to improve the safety of cigarette smoking, reduce harmful ingredients in cigarette smoke, increase the comfort of sucking each cigarette manufacturer has become the hot research and development. 卷烟材料科研工作者利用天然植物材料已研发出一些滤棒颗粒材料,主要采用的方式是直接将植物材料粉碎成20〜80目之间的颗粒或者将植物材料通过挤压法制备成颗粒,虽然在卷烟增香、减害方面取得了一定的效果,但还存在以下几个方面的缺点:(1)直接将植物材料粉碎成颗粒,颗粒形状不均匀、物理性质不稳定,在卷烟滤棒成型时颗粒容易造碎从而产生大量粉尘,材料利用率不高;(2)通过挤压法制备颗粒,所添加的粘合剂容易将植物材料本身具有的孔洞包埋,颗粒材料与卷烟烟气的接触面积降低,其减害降焦作用有限,同时所制备的颗粒较为紧密、硬度较大,不利于卷烟复合滤棒的制备。 Cigarette use natural plant materials scientists have developed some of the plug material the particulate material is mainly used in a manner directly to the plant material into comminuted particles of between 20 to 80 mesh or plant material is prepared by extrusion into pellets, although made cigarette flavoring, less harmful aspects of a certain effect, but there is a disadvantage in the following aspects: (1) directly to the plant material into comminuted particles, non-uniform particle shape, physical properties unstable, the cigarette plug wrap when the particles are easily broken made to produce a lot of dust, material utilization is not high; (2) Preparation of granules by extrusion process, the adhesive is easily added plant material itself has a hole embedding particulate material in cigarette smoke reduce the contact area, which is limited tar harm reduction effect, while the granules produced more closely, greater hardness, it is not conducive to the preparation of composite cigarette filter rods. 针对上述缺点,如何采用适当的工艺技术,制备适合生产需求的植物多孔材料,以满足烟草行业在卷烟增香、减害方面的需求,就成为本领域尚待解决的技术难题。 In response to these shortcomings, how the use of appropriate technology, preparation of porous material suitable for plant production needs to meet the tobacco industry, cigarette flavoring, harm reduction aspects of the demand, has become the art of technical problems yet to be resolved.

发明内容 SUMMARY

[0004] 本发明的目的在于针对现有技术的不足,提供一种耐加工性强、颗粒均匀、安全性高、增香效果明显、具有一定减害效果的迷迭香多孔颗粒。 [0004] The object of the present invention is less than for the prior art to provide a strong process resistance, uniform particles, safe, flavoring effect is obvious, having harmful effects of certain reducing rosemary porous particles.

[0005] 本发明的目的还在于提供所述迷迭香多孔颗粒在卷烟生产中的应用。 [0005] The object of the present invention is to provide the use of porous particles rosemary cigarette production.

[0006] 本发明的目的通过下述技术方案予以实现。 [0006] The object of the present invention is realized by the following technical scheme.

[0007] *除非另有说明,本发明中所采用的百分数均为质量百分数。 [0007] * Unless otherwise indicated, the percentages employed in the present invention are in mass percentage.

[0008] 一种迷迭香多孔颗粒,通过以下步骤的方法制得: [0008] A rosemary porous particles, manufactured by the following method steps have:

[0009] (I)将新鲜迷迭香的叶片和梗在温度20〜25°C、湿度30%〜40%条件下调节至水分含量为7〜9%,然后分别进一步粉碎为100〜160目的粉末,将叶片粉末和梗粉末,按照重量份数60〜70:30〜40的比例混合均匀,备用; [0009] (I) fresh rosemary stems and leaves at a temperature regulating 20~25 ° C, humidity 30% ~ 40% to a moisture content condition of 7~9%, respectively, and then further pulverized to 100~160 object powder, the powder leaves and stem powder, 60 to 70 parts by weight according to: a mixed ratio of 30 to 40, alternate;

[0010] (2)按照重量份称取羧甲基淀粉钠6〜8份、明胶O〜2份,用蒸馏水配制成浓度为6〜10%的粘合剂溶液,备用; [0010] (2) Weigh 6 ~ 8 parts of sodium carboxymethyl starch, gelatin O~2 parts, formulated at a concentration of 6~10% of binder solution in accordance with alternate parts by weight of distilled water;

[0011] (3)称取备用的迷迭香粉末300〜100g置于流化床中造粒,造粒工艺具体包括如下步骤: [0011] (3) Weigh the standby rosemary powder 300~100g a fluidized bed granulation, the granulation process comprises the steps of:

[0012] (a)在流化气压为0.15Bar、50°C的条件下保持5〜10分钟; [0012] (a) the pressure of the fluidized 0.15Bar, maintained at 50 ° C under 5 to 10 minutes;

[0013] (b)在流化气压0.12〜0.15Bar、气流温度50〜60°C,喷雾压力0.10〜0.12Bar、喷液速率10〜12g/分钟的条件下,采用顶喷方式施加步骤(2)所配制的粘合剂溶液,粘合剂溶液用量为干物料重量的40%〜50% ; [0013] (b) at atmospheric pressure fluidized 0.12~0.15Bar, air flow temperature 50~60 ° C, 10~12g / min spray pressure conditions 0.10~0.12Bar, spray solution rate, the top-spray mode is applied in step (2 ) formulated binder solution, a binder solution in an amount of 40% ~ 50% by dry weight of the material;

[0014] (C)粘合剂施加完后,在流化气压0.12〜0.2Bar、气流温度50°C条件下干燥10〜12分钟,制备得到水分含量为8〜10%,表面粗糙的类圆形颗粒,即为所需的迷迭香多孔颗粒。 [0014] (C) After the adhesive is applied, in a fluid pressure 0.12~0.2Bar, dried 10~12 minutes at a temperature of 50 ° C air flow conditions, the moisture content of prepared 8~10%, the surface roughness of the circle class shaped particles, porous particles is the desired rosemary.

[0015] 其中,所制得的迷迭香多孔颗粒其粒径为20〜60目。 [0015] wherein the prepared porous particles having a particle size of rosemary 20~60 mesh.

[0016] 所述的流化床优选为Midi Glatt流化床。 [0016] The fluidized bed is preferably Midi Glatt fluidized bed.

[0017] 所述的迷迭香多孔颗粒在卷烟滤棒中应用,其特征在于:在每毫米卷烟滤棒中添加I〜2mg的迷迭香多孔颗粒。 [0017] The porous particles used in rosemary cigarette filter is characterized in that: ROSEMARY I~2mg porous particles per millimeter in the cigarette filter.

[0018] 与现有技术相比,本发明具有以下优点: [0018] Compared with the prior art, the present invention has the following advantages:

[0019] 1.所制备的颗粒均匀、理化性质稳定,具有较好的耐加工性,避免了滤棒成型过程中颗粒材料因机械加工而产生的造碎和粉尘,颗粒材料能够在滤棒丝束中均匀分布。 [0019] 1. The particles produced uniform, stable physical and chemical properties, having a good process resistance, and to avoid making dust crushed, particulate material particulate material plug molding process by machining can be generated in the wire plug uniform distribution of the beam.

[0020] 2.颗粒表面粗糙,具有较高的比表面积,显著提高颗粒材料与卷烟烟气的有效接触面积,能够选择性吸附卷烟烟气中的氨。 [0020] 2. The particle surface roughness, having a high specific surface area, significantly increase the effective contact area of ​​cigarette smoke and particulate material capable of selectively adsorbing ammonia in cigarette smoke.

[0021] 3.该颗粒能够有效丰富卷烟烟香、增强甜润感,同时具有提升烟气透发性的功效。 [0021] 3. The particles can effectively enrich cigarette smoke smell, sense of enhanced sweet, while through the hair with lifting effect of the flue gas.

[0022] 4.所使用材料均为食品级,具有较高的使用安全性。 [0022] 4. A food-grade materials are used, has a high safety of use.

[0023] 5.生产工艺简单,操作性及规范性强,原料易得、成本低廉,便于实现工业化生产,具有良好地应用前景。 [0023] The production process is simple, and operability strong normative, raw materials, low cost, ease of industrial production, having a good prospect.

具体实施方式 Detailed ways

[0024] 为了使本发明的目的、技术方案及优点更加清楚明白,以下结合实施例,对本发明作进一步详细说明。 [0024] To make the objectives, technical solutions and advantages of the present invention will become more apparent hereinafter in conjunction with embodiments of the present invention will be further described in detail. 应当理解,此处所描述的具体实施例仅仅用以解释本发明,并不是对本发明技术方案的限定。 It should be understood that the specific embodiments described herein are only intended to illustrate the invention and does not limit the technical solution of the present invention.

[0025] 实施例1 [0025] Example 1

[0026] 取新鲜迷迭香的叶片和梗在温度为20°C、湿度为30%条件下,调节至水分为7%,再分别将叶片和梗粉碎为100目的粉末,按照叶片粉末:梗粉末=60:40的重量比例混合,将混合后的粉末100g置于Midi Glatt流化床中造粒,流化床流化气压为0.15Bar、50°C条件下保持10分钟;然后将蒸馏水配制成浓度为8%的羧甲基淀粉钠粘合剂溶液,在流化气压为0.15Bar、气流温度为60°C,喷雾压力为0.12Bar、喷液速率为1g/分钟条件下,采用顶喷方式喷洒400g粘合剂溶液;粘合剂施加完后,设定流化气压0.2Bar、气流温度为50°C条件下干燥12分钟,将水分含量调节至8%,过60目筛即得卷烟滤棒用迷迭香多孔颗粒。 [0026] Fresh rosemary stems and leaves at a temperature of 20 ° C, 30% humidity conditions, water content was adjusted to 7%, respectively, and then the stems and leaves pulverized into 100 mesh powder, powder according to leaf: stem powder = 60: 40 mixture by weight ratio, the mixed powder was placed 100g Midi Glatt fluidized bed granulation, fluidization gas pressure holding 0.15Bar, 50 ° C for 10 minutes; the formulation was then distilled a concentration of 8% sodium carboxymethyl starch binder solution, in a fluidized gas pressure of 0.15 bar, air flow temperature is 60 ° C, spraying pressure 0.12Bar, spray solution rate of 1g / min under the conditions of the top-spray spray the binder solution 400g embodiment; after applying the adhesive, the air pressure of 0.2bar set flow, dried air flow temperature 50 ° C for 12 minutes condition, the moisture content was adjusted to 8%, i.e. 60 mesh to obtain cigarettes rosemary plug with porous particles.

[0027] 实施例2 [0027] Example 2

[0028] 取新鲜迷迭香的叶片和梗在温度为25°C、湿度为40%条件下,调节至水分为9%,再分别将叶片和梗粉碎为120目的粉末,按照叶片粉末:梗粉末=70:30的重量比例混合,将混合后的粉末500g置于Midi Glatt流化床中造粒,流化床流化气压为0.15Bar、50°C条件下保持8分钟;然后按照重量份称取羧甲基淀粉钠8份、明胶2份,用蒸馏水配制成浓度为10%的粘合剂溶液,在流化气压为0.12Bar、气流温度为60°C、喷雾压力为0.lOBar、喷液速率为12g/分钟条件下,采用顶喷方式喷洒200g粘合剂溶液;粘合剂施加完后,设定流化气压0.15Bar、气流温度为50°C条件下干燥10分钟,将水分含量调节至9%,过40目筛即得卷烟滤棒用迷迭香多孔颗粒。 [0028] Fresh rosemary stems and leaves at a temperature of 25 ° C, 40% humidity conditions, adjusted to a water content of 9%, respectively, and then the stems and leaves pulverized into 120 mesh powder, powder according to leaf: stem powder = 70: 30 mixture by weight ratio, the mixed powder was placed 500g Midi Glatt fluidized bed granulation, fluidization gas pressure holding 0.15Bar, 50 ° C condition 8 min; then follow parts by weight Weigh 8 parts of sodium carboxymethyl starch, 2 parts of gelatin, adding distilled water to a concentration of 10% binder solution in a fluidized gas pressure 0.12Bar, air flow temperature of 60 ° C, spraying pressure 0.lOBar, spray solution rate of 12g / min under the conditions of the top-spray binder solution 200g spray mode; after applying adhesive, the pressure of 0.15 bar set flow, the temperature of the gas flow is dried for 10 minutes 50 ° C for conditions, the moisture content is adjusted to 9%, i.e. 40 mesh sieve to obtain rosemary cigarette filter with porous particles.

[0029] 实施例3 [0029] Example 3

[0030] 取新鲜迷迭香的叶片和梗在温度为22°C、湿度为35%条件下,调节至水分为8%,再分别将叶片和梗粉碎为160目的粉末,按照叶片粉末:梗粉末=65:35的重量比例混合,将混合后粉末300g置于Midi Glatt流化床中造粒,流化床流化气压为0.15Bar、50°C条件下保持5分钟;然后按照重量份称取羧甲基淀粉钠6份、明胶2份,用蒸馏水配制成浓度为8%的粘合剂溶液,在流化气压为0.12Bar、气流温度为55°C、喷雾压力为0.lOBar、喷液速率为1g/分钟条件下,采用顶喷方式喷洒150g粘合剂溶液;粘合剂施加完后,设定流化气压0.12Bar、气流温度为50°C条件下干燥10分钟,将水分含量调节至10%,过20目筛即得卷烟滤棒用迷迭香多孔颗粒。 [0030] Fresh rosemary stems and leaves at a temperature of 22 ° C, 35% humidity conditions, adjusted to a water content of 8%, respectively, and then the stems and leaves pulverized into 160 mesh powder, powder according to leaf: stem powder = 65: 35 mixture by weight ratio, mixed powder was placed 300g Midi Glatt fluidized bed granulation, fluidization gas pressure holding 0.15Bar, 50 ° C for 5 minutes; then follow parts by weight of said take 6 parts of sodium carboxymethyl starch, 2 parts of gelatin, formulated at a concentration of 8% binder solution with distilled water, in a fluidized gas pressure 0.12Bar, air flow temperature of 55 ° C, spraying pressure 0.lOBar, spray liquid rate 1g / min under the conditions of the top-spray binder solution 150g spray mode; after adhesive application, the fluidizing air pressure set 0.12Bar, dried for 10 minutes the gas flow temperature of 50 ° C for conditions, the moisture content adjusted to 10% through a 20 mesh sieve to obtain rosemary cigarette filter with porous particles.

[0031] 应用实施例1 [0031] Application Example 1

[0032] 将实施例1制备所得迷迭香多孔颗粒应用于在卷烟复合滤棒中,每毫米卷烟滤棒添加Img颗粒材料,制备成实验烟支,以不添加上述颗粒的烟支为对照进行感官评吸和烟气有害成分检测。 [0032] The porous particles obtained in Example 1 was prepared rosemary embodiment will be applied to the composite filter rods in a cigarette, a cigarette filter is added per millimeter Img particulate material to prepare a test cigarettes, cigarettes was not added to the pellet to be controlled sensory evaluation harmful components and smoke detection. 感官评价结果表明:与对照相比,添加上述多孔颗粒的烟支香气更加丰富,余味得到明显改善,烟气透发性明显提升;烟气有害成分检测表明:氨降低率为19.6%,其它有害成分变化不大,该多孔颗粒能够选择性吸附卷烟烟气中的氨。 Sensory evaluation showed that: compared with the control, the addition of the porous particles cigarettes richer aroma, significantly improved aftertaste, enhance significantly the flue gas through the hair; smoke harmful components analysis showed that: 19.6% of ammonia was reduced, other harmful little change composition, the porous particles are capable of selectively adsorbing ammonia in cigarette smoke.

[0033] 应用实施例2 [0033] Application Example 2

[0034] 将实施例2制备所得迷迭香多孔颗粒应用于在卷烟复合滤棒中,每毫米卷烟滤棒添加2mg颗粒材料,制备成实验烟支,以不添加上述颗粒的烟支为对照进行感官评吸和烟气有害成分检测。 [0034] Example 2 Preparation of rosemary resulting porous particles embodiment is applied to the composite filter rods in a cigarette, the cigarette filter was added 2mg per millimeter particulate material to prepare a test cigarettes, cigarettes was not added to the pellet to be controlled sensory evaluation harmful components and smoke detection. 感官评价结果表明:与对照相比,添加上述多孔颗粒的烟支香气更加丰富,甜润感显著增强,烟气透发性明显提升;烟气有害成分检测表明:氨降低率为26.4%,其它有害成分变化不明显,该多孔颗粒能够选择性吸附卷烟烟气中氨。 Sensory evaluation showed that: compared with the control, the addition of the porous particles cigarettes richer aroma, sweet feeling significantly enhanced significantly enhance the flue gas through the hair; smoke harmful components analysis showed that: 26.4% of ammonia was reduced, other harmful composition did not change significantly, the porous particles are capable of selectively adsorbing ammonia in cigarette smoke.

[0035] 应用实施例3 [0035] Application Example 3

[0036] 将实施例3制备所得迷迭香多孔颗粒应用于在卷烟复合滤棒中,每毫米卷烟滤棒添加1.5mg颗粒材料,制备成实验烟支,以不添加上述颗粒的烟支为对照进行感官评吸和烟气有害成分检测。 [0036] The porous particles obtained in Example 3 Preparation of rosemary in the embodiment is applied to the composite filter rods in a cigarette, a cigarette filter is added 1.5mg per millimeter particulate material to prepare a test cigarette to cigarette without the addition of the particles is controlled for sensory evaluation harmful components and smoke detection. 感官评价结果表明:与对照相比,添加上述多孔颗粒的烟支烟气刺激性明显降低,余味得到明显改善,烟气透发性明显提升;烟气有害成分检测表明:氨降低率为22.8%,其它有害成分变化不明显,该多孔颗粒能够选择性吸附卷烟烟气中的氨。 Sensory evaluation showed that: compared with the control, the addition of the porous particles of the cigarette smoke irritation significantly reduced, significantly improved aftertaste, enhance significantly the flue gas through the hair; smoke harmful components analysis showed that: 22.8% of ammonia was reduced , other harmful components did not change significantly, the porous particles are capable of selectively adsorbing ammonia in cigarette smoke.

[0037] 以上所述仅为本发明的较佳实施例而已,并不用以限制本发明,凡在本发明的精神和原则之内所作的任何修改、等同替换和改进等,均应包含在本发明的保护范围之内。 [0037] The foregoing is only preferred embodiments of the present invention but are not intended to limit the present invention, any modifications within the spirit and principle of the present invention, equivalent substitutions and improvements should be included in the present within the scope of the invention.

Claims (4)

1.一种迷迭香多孔颗粒,通过以下步骤的方法制得: (1)将新鲜迷迭香的叶片和梗在温度20〜25°C、湿度30%〜40%条件下调节至水分含量为7〜9%,然后分别进一步粉碎为100〜160目的粉末,按照叶片粉末:梗粉末=60〜70:30〜40的重量比例混合均匀后备用; (2)按照重量份称取羧甲基淀粉钠6〜8份、明胶O〜2份,用蒸馏水配制成浓度质量百分数为6〜10%的粘合剂溶液,备用; (3)称取备用的迷迭香粉末300〜100g置于流化床中造粒,造粒工艺具体包括如下步骤: (a)在流化气压为0.15Bar、50°C的条件下保持5〜10分钟; (b)在流化气压0.12〜0.15Bar、气流温度50〜60°C,喷雾压力0.10〜0.12Bar、喷液速率10〜12g/分钟的条件下,采用顶喷方式施加步骤(2)所配制的粘合剂溶液,粘合剂溶液用量为干物料重量的40%〜50% ; (c)粘合剂施加完后,在流化气压0.12〜0.2Bar、气流温度50°C条件下干燥10〜12分 A rosemary porous particles, prepared by the following steps to give: (1) fresh rosemary leaves and stems to a moisture content adjusted at a temperature of 20~25 ° C, humidity 30% ~ 40% Condition is 7~9%, respectively and then further pulverized to 100~160 mesh powder, the powder according to leaf: stem powder = 60 to 70: 30 to 40 by weight ratio of the mixed after use; (2) Weigh carboxymethylcellulose accordance parts by weight 6 ~ 8 parts of sodium starch, gelatin O~2 parts, adding distilled water to a concentration of 6~10% by mass percentage of binder solution, the standby; (3) Weigh the standby flow rosemary powder was placed 300~100g fluidized bed granulation, the granulation process comprises the steps of: (a) the pressure is maintained in the fluidized under 0.15Bar, 50 ° C in 5 to 10 minutes; (b) 0.12~0.15Bar fluidizing air pressure in the air flow temperature 50~60 ° C, under 10~12g / min spray pressure conditions 0.10~0.12Bar, spray solution rate, the top-spray mode is applied in step (2) of the formulated binder solution, the amount of adhesive dry solution 40% ~ 50% by weight of the material; (c) after the adhesive is applied, and dried at 10~12 minutes fluidization pressure 0.12~0.2Bar, air flow temperature condition of 50 ° C ,制备得到水分含量为8〜10%,表面粗糙的类圆形颗粒,即为所需的迷迭香多孔颗粒。 , Prepared to give a water content of 8~10%, surface roughness round particles, porous particles is the desired rosemary.
2.根据权利要求1所述的迷迭香多孔颗粒,其特征在于:所制得的迷迭香多孔颗粒其粒径为20〜60目。 The rosemary said porous particles according to claim 1, characterized in that: the prepared rosemary porous particles having a particle size of 20~60 mesh.
3.根据权利要求1所述的迷迭香多孔颗粒,其特征在于:所述的流化床优选为MidiGlatt流化床。 The porous particles according to claim rosemary in claim 1, wherein: said fluidized bed is preferably MidiGlatt.
4.权利要求1所述的迷迭香多孔颗粒在卷烟滤棒中的应用,其特征在于:在每毫米卷烟滤棒中添加I〜2mg的迷迭香多孔颗粒。 Application of rosemary said porous particles in a cigarette filter of claim 1, wherein: the added rosemary I~2mg porous particles per millimeter in a cigarette filter.
CN201310643991.0A 2013-12-03 2013-12-03 Rosemary porous particles and application thereof in cigarettes CN103691397B (en)

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