CN103689791A - Peanut shell particle compound tip stick - Google Patents
Peanut shell particle compound tip stick Download PDFInfo
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- CN103689791A CN103689791A CN201310643586.9A CN201310643586A CN103689791A CN 103689791 A CN103689791 A CN 103689791A CN 201310643586 A CN201310643586 A CN 201310643586A CN 103689791 A CN103689791 A CN 103689791A
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Abstract
The invention discloses a peanut shell particle compound tip stick. The peanut shell particles are prepared by performing microwave expansion, smashing, granulating, baking and modulating on peanut shells. The peanut shell particles are applied to a cigarette filter tip and are added into a tip stick in an amount of 17-53 percent of the total weight of the tip stick, and a prepared binary compound tip stick is applied to cigarettes. As proved by practical application, the components of tar, nicotine, phenol, crotonaldehyde and the like in cigarette smoke can be reduced effectively. The peanut shell particle compound filter tip is easy and convenient to operate, is low in cost, and has a good application prospect.
Description
Technical field
The invention belongs to cigarette material technical field, relate to cigarette filter mouth rod, specifically relate to a kind of peanut shell granular composite tip stick that can reduce harmful constituents in cigarette flue gas.
Background technology
Peanut is the main oil crops of China, and its total output and export volume all occupy first place in the world. China's peanut gross annual output amount reaches ten thousand tons of left and right of l500, accounts for 42% of Peanut total output, approximately can produce every year 5000000 tons of peanut shells.It is reported, the maximum composition of peanut shell is crude fibre, content 65.7%～79.3%.In peanut shell, other nutritional labeling is also very abundant, crude protein 4.8%～7.2%, crude fat 1.2%～1.8%, reduced sugar 0.3%～1.8%, disaccharide 1.7%～2.5%, pentose 16.1%～17.8%, starch 0.7%, also contain some mineral matters, as calcic 0.20%, phosphorus 0.06%, magnesium 0.07%, potassium 0.57%, nitrogen 1.09%, iron 262mg/kg, manganese 45mg/kg, zinc 13mg/kg, copper 10mg/kg, boron 13mg/kg, aluminium 454mg/kg, strontium 262mg/kg, barium 16mg/kg, sodium 66mg/kg.In addition, in peanut shell, also contain some medicinal ingredients (as: cupreol, carrotene, saponin, wood sugar etc.), also can extract after treatment some important industrial chemicals (as acetic acid, furfural, acetone, methyl alcohol, luxuriant and rich with fragrance fourth etc.).Therefore, for many years researcher has carried out large quantity research to peanut shell comprehensive development and utilization, as for multiple fields such as agricultural fertilizer, feed, food, adhesive, composite, active carbon sewage disposal, catalyzing manufacturing of hydrogen.
Because peanut shell itself has the architectural feature of porous, there is good absorption property, after having carried out chemical modification and be translated into activated carbon peanut shell, researcher for sewage disposal, can adsorb well the chemical pollutants such as heavy metal in sewage and phenol.And along with smoking and healthy problem more and more receive publicity, the comfort of sucking security, reduce harmful components in cigarette smoke, improving suction that how to improve cigarette just becomes the focus of each tobacco productive corporation research and development.But less for the report of porous material aspect that raw material preparation can effectively reduce the chemical compositions such as tar in cigarette smoke, nicotine, hydrogen cyanide, phenol and crotonaldehyde about utilizing peanut shell, this is also that this area waits the technical barrier solving.
Summary of the invention
The object of the invention is to for the deficiencies in the prior art, a kind of peanut shell granular composite tip stick that can effectively reduce part harmful components in cigarette mainstream flue gas is provided.
Object of the present invention is achieved by following technical proposals.
* except as otherwise noted, the percentage adopting in the present invention is mass percent.
A peanut shell granular composite tip stick, the method by following steps makes:
(1) peanut shell that is 20%～25% by moisture content, is placed in microwave expansion equipment, at microwave power, is the 30～60s that expands under 1000～1500W condition;
(2) peanut shell after expanding sprays repeatedly with distilled water, regulates moisture content to 22%～26%, and is positioned under room temperature balance 6～12 hours, standby;
(3) the good peanut hull meal of balance is broken to 20～80 order particles, the baking oven that is placed in 60～80 ℃ toasts 10～30 minutes, keeps pellet moisture between 8～10%, standby;
(4) take by weight 5～10 parts of propane diols, 0～10 part of glycerine and 10～30 parts of pure water, standby after stirring;
(5) solution of being prepared by step (4) is sprayed onto in the prepared particle of step (3) equably according to 0.8～1.2% ratio, at room temperature places 4～8 hours, obtains required peanut shell granular;
(6) prepared peanut shell granular is added in cigarette filter by composite filter forming machine, prepare binary composite tip stick.
Addition is preferably 17～53% of mouth rod gross weight.
Described peanut shell is Virginia type peanut shell, pearl type peanut shell, Valencia type peanut shell, the raw type peanut shell of dragon.
Compared with prior art, the present invention has the following advantages:
1. adopting peanut shell is raw material, and environmental protection, turns waste into wealth, constant product quality;
2. described in, peanut shell granular composite tip stick is applied in cigarette, can effectively reduce the chemical compositions such as tar in cigarette smoke, nicotine, ammonia.
3. the present invention is easy and simple to handle, raw material is easy to get, with low cost, there is application prospect well.
The specific embodiment
In order to make object of the present invention, technical scheme and advantage clearer, below in conjunction with embodiment, the present invention is described in further detail.Should be appreciated that specific embodiment described herein, only in order to explain the present invention, is not limited to the technical solution.
Embodiment 1
Take 100g Virginia type peanut shell, regulating moisture is 22%, then be placed in microwave expansion equipment, under 1000w power, expand 30 seconds, peanut shell after expanding is sprayed repeatedly with distilled water, the moisture content that makes peanut shell is 22%, and under room temperature, place and after 6 hours, be crushed into 50 object particles, prepared peanut shell granular is positioned in the baking oven of 60 ℃ simultaneously and toasts about 20 minutes, the moisture content that makes particle is 10% left and right, then will contain 10 parts of propane diols, the mixed solution of 20 parts of distilled water is sprayed onto in peanut shell granular according to 0.8% ratio uniformly, under room temperature, place 4 hours, obtain required peanut shell granular.
Embodiment 2
Take 2kg pearl type peanut shell, regulating moisture is 25%, then be placed in microwave expansion equipment, under 1500w power, expand 60 seconds, peanut shell after expanding is sprayed repeatedly with distilled water, the moisture content that makes peanut shell is 26%, and under room temperature, place and after 12 hours, be crushed into 80 object particles, prepared peanut shell granular is positioned in the baking oven of 80 ℃ simultaneously and toasts about 20 minutes, the moisture content that makes particle is 8% left and right, then will contain 5 parts of propane diols, 10 parts of glycerine, the mixed solution of 30 parts of distilled water is sprayed onto in peanut shell granular according to 1.2% ratio uniformly, with under room temperature, place 8 hours, obtain required plant porous material.
Embodiment 3
Repeat embodiment 1, have following difference: peanut shell is pearl type peanut shell.
Embodiment 4
Repeat embodiment 1, have following difference: peanut shell is Valencia type peanut shell.
Embodiment 5
Repeat embodiment 1, have following difference: the raw type peanut shell of peanut shell dragon.
Embodiment 6
Repeat embodiment 2, have following difference: peanut shell is Virginia type peanut shell.
Embodiment 7
Repeat embodiment 2, have following difference: peanut shell is Valencia type peanut shell.
Embodiment 8
Repeat embodiment 2, have following difference: peanut shell is the raw type peanut shell of dragon.
Application Example 1
In process at composite tip stick shaping mechanism for composite tip stick, add the peanut shell granular of mouth rod weight 18% embodiment 1 preparation, prepare peanut shell granular mouth rod, mode with binary mouth rod is prepared into cigarette, identical with the fabrication process condition of contrast blank sample, carry out cigarette composition detection simultaneously.Result shows: tar reduction by 11% in cigarette smoke, nicotine reduction by 10%, NH
3reduce by 30%.Sample is carried out sensory evaluation and shown with contrasting, and this sample obviously can enrich cigarette nature fragrance, and cigarette whole style feature is had no significant effect.
Application Example 2
In process at composite tip stick shaping mechanism for composite tip stick, add the peanut shell granular of mouth rod weight 50% embodiment 1 preparation, prepare peanut shell granular mouth rod, mode with binary mouth rod is prepared into cigarette, identical with the fabrication process condition of contrast blank sample, carry out cigarette composition detection simultaneously.Result shows: tar reduction by 8% in cigarette smoke, nicotine reduction by 7% and NH
3reduce by 26%.Sample is carried out sensory evaluation and shown with contrasting, and this sample obviously can enrich cigarette nature fragrance, and cigarette whole style feature is had no significant effect.
The foregoing is only preferred embodiment of the present invention, not in order to limit the present invention, all any modifications of doing within the spirit and principles in the present invention, be equal to and replace and improvement etc., within all should being included in protection scope of the present invention.
Claims (2)
1. a peanut shell granular composite tip stick, the method by following steps makes:
(1) peanut shell that is 20%～25% by moisture content, is placed in microwave expansion equipment, at microwave power, is the 30～60s that expands under 1000～1500W condition;
(2) peanut shell after expanding sprays repeatedly with distilled water, regulates moisture content to 22%～26%, and is positioned under room temperature balance 6～12 hours, standby;
(3) the good peanut hull meal of balance is broken to 20～80 order particles, the baking oven that is placed in 60～80 ℃ toasts 10～30 minutes, keeps pellet moisture between 8～10%, standby;
(4) take by weight 5～10 parts of propane diols, 0～10 part of glycerine and 10～30 parts of pure water, standby after stirring;
(5) solution of being prepared by step (4) is sprayed onto in the prepared particle of step (3) equably according to 0.8～1.2% ratio, at room temperature places 4～8 hours, obtains required peanut shell granular;
(6) prepared peanut shell granular is added in cigarette filter by composite filter forming machine, prepare binary composite tip stick.
2. peanut shell granular composite tip stick according to claim 1, is characterized in that: the addition of described peanut shell granular is preferably 17～53% of mouth rod gross weight.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310643586.9A CN103689791B (en) | 2013-12-03 | 2013-12-03 | Peanut shell particle compound tip stick |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310643586.9A CN103689791B (en) | 2013-12-03 | 2013-12-03 | Peanut shell particle compound tip stick |
Publications (2)
| Publication Number | Publication Date |
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| CN103689791A true CN103689791A (en) | 2014-04-02 |
| CN103689791B CN103689791B (en) | 2015-04-08 |
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| CN201310643586.9A Active CN103689791B (en) | 2013-12-03 | 2013-12-03 | Peanut shell particle compound tip stick |
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Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20040167019A1 (en) * | 2001-07-17 | 2004-08-26 | Zhi-Wei Liang | Oxidative thermochemical drying process for changing hydrophilic/hydrophobic characteristics of natural organic substances |
| CN102119786A (en) * | 2011-04-07 | 2011-07-13 | 红云红河烟草(集团)有限责任公司 | Soybean residue composite filter tip and manufacturing method thereof |
| CN103169146A (en) * | 2013-02-07 | 2013-06-26 | 赵鸿 | Raw materials for cigarettes, production method and equipment thereof |
| CN103355743A (en) * | 2013-08-14 | 2013-10-23 | 中国烟草总公司郑州烟草研究院 | Preparation and application of crop waste cigarette filter additive carrier materials |
| CN103393219A (en) * | 2013-08-14 | 2013-11-20 | 中国烟草总公司郑州烟草研究院 | Modified natural plant filter tip additive material capable of selectively reducing burst size of hydrogen cyanide in main stream smoke of cigarettes and preparation method of modified natural plant filter tip additive material |
-
2013
- 2013-12-03 CN CN201310643586.9A patent/CN103689791B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20040167019A1 (en) * | 2001-07-17 | 2004-08-26 | Zhi-Wei Liang | Oxidative thermochemical drying process for changing hydrophilic/hydrophobic characteristics of natural organic substances |
| CN102119786A (en) * | 2011-04-07 | 2011-07-13 | 红云红河烟草(集团)有限责任公司 | Soybean residue composite filter tip and manufacturing method thereof |
| CN103169146A (en) * | 2013-02-07 | 2013-06-26 | 赵鸿 | Raw materials for cigarettes, production method and equipment thereof |
| CN103355743A (en) * | 2013-08-14 | 2013-10-23 | 中国烟草总公司郑州烟草研究院 | Preparation and application of crop waste cigarette filter additive carrier materials |
| CN103393219A (en) * | 2013-08-14 | 2013-11-20 | 中国烟草总公司郑州烟草研究院 | Modified natural plant filter tip additive material capable of selectively reducing burst size of hydrogen cyanide in main stream smoke of cigarettes and preparation method of modified natural plant filter tip additive material |
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| CN103689791B (en) | 2015-04-08 |
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