CN103668963A - Sterilization fabric softener and preparation method thereof - Google Patents
Sterilization fabric softener and preparation method thereof Download PDFInfo
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- CN103668963A CN103668963A CN201310609296.2A CN201310609296A CN103668963A CN 103668963 A CN103668963 A CN 103668963A CN 201310609296 A CN201310609296 A CN 201310609296A CN 103668963 A CN103668963 A CN 103668963A
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Abstract
The invention relates to a sterilization fabric softener and a preparation method thereof, and belongs to the technical field of daily chemicals. The sterilization fabric softener comprises the following components in parts by weight: 15-20 parts of tetramethylene-bia(lauroyloxyethyl dimethyl ammonium bromide), 8-10 parts of ditallow ethoxycarbonyl hydroxyethyl methyl ammonium methylsulfate, 2-4 parts of lavender, 5-10 parts of a ginkgo leaf, 0.1-0.5 part of a thickener, 0.2-2 parts of a color fixing agent, and 80-100 parts of deionized water. A favorable biodegradable Gemini cationic surface active agent and an esterquat surface active agent are used as active substances, so that the sterilization fabric softener not only has favorable softness and an antistatic property, but also is extremely environment-friendly, meanwhile, the sterilization fabric softener has a color fixing effect, and is excellent in sterilization effect. Besides, the preparation method is simple, and is easy to popularize and apply.
Description
Technical field
The invention belongs to household chemicals technical field, be specifically related to a kind of disinfectant fabric softener and preparation method thereof.
Background technology
Clothing is in washing process, fiber fines tends to be wound around, intertwine, even rupture, clothing is after repeatedly washing, the alkalescence effect of washing agent more makes the intrinsic slickness of fiber, extensibility and elasticity be affected, what show is that whole clothing seems to wear, do not have shape, touches feel stiff especially, and more this clothes washing number of times sensation be just more obvious.
It is main active that fabric softening agent great majority in the market adopt dioctadecyl dimethyl ammonium chloride, the shortcoming of this class softener maximum is that biological degradability is poor and xanthochromia is serious, along with the raising that require public awareness of people to environment-friendly quality, this series products can not meet the demand of social development.Meanwhile, on market, most of softener sterilizing functions are poor, and do not have fixation function, and therefore how overcoming the deficiencies in the prior art is problems that current household chemicals technical field is needed solution badly.
Summary of the invention
The object of the invention is, in order to solve the deficiencies in the prior art, provides a kind of disinfectant fabric softener and preparation method thereof, and this softener has good sterilization and colour fixation, and preparation technology is simple.
The technical solution used in the present invention is as follows:
A disinfectant fabric softener, comprises the following component according to parts by weight meter: 15 ~ 20 parts of tetramethylenes-bis-(lauroyl oxygen ethyl dimethyl ammonium bromide), 8 ~ 10 parts of two ox ester group ethoxycarbonyl ethoxy methylsulfuric acid ammonium methyls, 2 ~ 4 parts of lavenders, 5 ~ 10 parts of ginkgo leaves, 0.1 ~ 0.5 part of thickener, 0.2 ~ 2 part, color-fixing agent, 80 ~ 100 parts of deionized waters.
Further preferably described thickener is hydroxypropyl methylcellulose.
Further preferably described color-fixing agent is chitosan quaternary ammonium salt.
The preparation method of above-mentioned disinfectant fabric softener, comprises the steps:
Step (1), is crushed to 150 ~ 200 orders in the lump by lavender and ginkgo leaf, and the deionized water of usining carries out percolation extraction as leaching solvent, by the standing 12 ~ 48h of extract, gets supernatant liquor;
Step (2), the supernatant liquor of step (1) is heated to 30 ~ 40 ℃, add tetramethylene-bis-(lauroyl oxygen ethyl dimethyl ammonium bromides), two ox ester group ethoxycarbonyl ethoxy methylsulfuric acid ammonium methyl and color-fixing agent, after being stirred to and mixing, add wherein again thickener, continue to be stirred to and mix, obtain disinfectant fabric softener of the present invention.
compared with prior art, its beneficial effect is in the present invention:(1) because adopting, the present invention there is the Gemini cationic surfactant of good biological degradability and esterquat surfactant as active material, make product of the present invention not only there is good flexibility and antistatic behaviour, and extremely friendly to environment; (2) product of the present invention has tint retention, and bactericidal effect is good; (3) preparation method of the present invention is simple, is easy to apply.
Specific embodiment
Below in conjunction with embodiment, the present invention is described in further detail.
Embodiment 1
A disinfectant fabric softener, comprises the following component according to parts by weight meter: 15 parts of tetramethylenes-bis-(lauroyl oxygen ethyl dimethyl ammonium bromide), 8 parts of two ox ester group ethoxycarbonyl ethoxy methylsulfuric acid ammonium methyls, 2 parts of lavenders, 5 parts of ginkgo leaves, 0.1 part of hydroxypropyl methylcellulose, 0.2 ~ 2 part of chitosan quaternary ammonium salt, 80 parts of deionized waters.
The preparation method of the present embodiment disinfectant fabric softener, comprises the steps:
Step (1), is crushed to 150 ~ 200 orders in the lump by lavender and ginkgo leaf, and the deionized water of usining carries out percolation extraction as leaching solvent, by the standing 12h of extract, gets supernatant liquor;
Step (2), the supernatant liquor of step (1) is heated to 40 ℃, add tetramethylene-bis-(lauroyl oxygen ethyl dimethyl ammonium bromides), two ox ester group ethoxycarbonyl ethoxy methylsulfuric acid ammonium methyl and chitosan quaternary ammonium salt, after being stirred to and mixing, add wherein again hydroxypropyl methylcellulose, continue to be stirred to and mix, obtain the disinfectant fabric softener of the present embodiment.
Embodiment 2
A disinfectant fabric softener, comprises the following component according to parts by weight meter: 20 parts of tetramethylenes-bis-(lauroyl oxygen ethyl dimethyl ammonium bromide), 10 parts of two ox ester group ethoxycarbonyl ethoxy methylsulfuric acid ammonium methyls, 4 parts of lavenders, 10 parts of ginkgo leaves, 0.5 part of hydroxypropyl methylcellulose, 2 parts of chitosan quaternary ammonium salts, 100 parts of deionized waters.
The preparation method of the present embodiment disinfectant fabric softener, comprises the steps:
Step (1), is crushed to 150 ~ 200 orders in the lump by lavender and ginkgo leaf, and the deionized water of usining carries out percolation extraction as leaching solvent, by the standing 48h of extract, gets supernatant liquor;
Step (2), the supernatant liquor of step (1) is heated to 30 ℃, add tetramethylene-bis-(lauroyl oxygen ethyl dimethyl ammonium bromides), two ox ester group ethoxycarbonyl ethoxy methylsulfuric acid ammonium methyl and chitosan quaternary ammonium salt, after being stirred to and mixing, add wherein again hydroxypropyl methylcellulose, continue to be stirred to and mix, obtain the disinfectant fabric softener of the present embodiment.
Embodiment 3
A disinfectant fabric softener, comprises the following component according to parts by weight meter: 17 parts of tetramethylenes-bis-(lauroyl oxygen ethyl dimethyl ammonium bromide), 9 parts of two ox ester group ethoxycarbonyl ethoxy methylsulfuric acid ammonium methyls, 3 parts of lavenders, 8 parts of ginkgo leaves, 0.3 part of hydroxypropyl methylcellulose, 1.1 parts of chitosan quaternary ammonium salts, 90 parts of deionized waters.
The preparation method of the present embodiment disinfectant fabric softener, comprises the steps:
Step (1), is crushed to 150 ~ 200 orders in the lump by lavender and ginkgo leaf, and the deionized water of usining carries out percolation extraction as leaching solvent, by the standing 30h of extract, gets supernatant liquor;
Step (2), the supernatant liquor of step (1) is heated to 35 ℃, add tetramethylene-bis-(lauroyl oxygen ethyl dimethyl ammonium bromides), two ox ester group ethoxycarbonyl ethoxy methylsulfuric acid ammonium methyl and chitosan quaternary ammonium salt, after being stirred to and mixing, add wherein again hydroxypropyl methylcellulose, continue to be stirred to and mix, obtain the disinfectant fabric softener of the present embodiment.
Adopt the present embodiment 3 products and commercially available common softener to carry out rinsing clearly to cotton T-shirt, take clean-rinsing-be dried-detect as sequentially, its compliance and intensity of colour testing result are as shown in table 1.
Table 1 compliance and intensity of colour testing result
, the bactericidal property of the present embodiment 3 products is detected, its sterilizing power result is meanwhile: staphylococcus aureus 92%, Escherichia coli 90%, Candida albicans 86%.
Claims (4)
1. a disinfectant fabric softener, is characterized in that comprising the following component according to parts by weight meter: 15 ~ 20 parts of tetramethylenes-bis-(lauroyl oxygen ethyl dimethyl ammonium bromide), 8 ~ 10 parts of two ox ester group ethoxycarbonyl ethoxy methylsulfuric acid ammonium methyls, 2 ~ 4 parts of lavenders, 5 ~ 10 parts of ginkgo leaves, 0.1 ~ 0.5 part of thickener, 0.2 ~ 2 part, color-fixing agent, 80 ~ 100 parts of deionized waters.
2. disinfectant fabric softener according to claim 1, is characterized in that described thickener is hydroxypropyl methylcellulose.
3. disinfectant fabric softener according to claim 1, is characterized in that described color-fixing agent is chitosan quaternary ammonium salt.
4. the preparation method of disinfectant fabric softener claimed in claim 1, is characterized in that comprising the steps:
Step (1), is crushed to 150 ~ 200 orders in the lump by lavender and ginkgo leaf, and the deionized water of usining carries out percolation extraction as leaching solvent, by the standing 12 ~ 48h of extract, gets supernatant liquor;
Step (2), the supernatant liquor of step (1) is heated to 30 ~ 40 ℃, add tetramethylene-bis-(lauroyl oxygen ethyl dimethyl ammonium bromides), two ox ester group ethoxycarbonyl ethoxy methylsulfuric acid ammonium methyl and color-fixing agent, after being stirred to and mixing, add wherein again thickener, continue to be stirred to and mix, obtain disinfectant fabric softener of the present invention.
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Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104762811A (en) * | 2015-03-26 | 2015-07-08 | 苏州威尔德工贸有限公司 | Special natural softener for textiles and preparation method for special natural softener |
CN105350312A (en) * | 2015-12-18 | 2016-02-24 | 苏州富美纺织科技有限公司 | Preparation method of blended fabric finishing liquid |
CN105926286A (en) * | 2016-05-30 | 2016-09-07 | 太仓红桥服饰有限公司 | Antibacterial softener for fabric and preparation method of antibacterial softener |
CN106957746A (en) * | 2017-03-07 | 2017-07-18 | 广州小蜜蜂生物科技有限公司 | Baby's pro-skin plant liquid detergent |
CN111764160A (en) * | 2020-07-14 | 2020-10-13 | 罗彦明 | Fabric softener |
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CN1667181A (en) * | 2004-03-11 | 2005-09-14 | 何忠林 | Ultra-strong softening finishing agent and making process thereof |
CN101029454A (en) * | 2006-02-27 | 2007-09-05 | 权力敏 | Antibacterial fabric softener |
CN101736580A (en) * | 2009-12-21 | 2010-06-16 | 北京绿泽宇和科技有限公司 | Fabric maintenance softener |
CN101935949A (en) * | 2010-08-27 | 2011-01-05 | 上海制皂有限公司 | Clothes softener |
CN102162189A (en) * | 2011-02-28 | 2011-08-24 | 河南省道纯化工技术有限公司 | Method for preparing fabric softening agent |
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2013
- 2013-11-27 CN CN201310609296.2A patent/CN103668963B/en active Active
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
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CN1667181A (en) * | 2004-03-11 | 2005-09-14 | 何忠林 | Ultra-strong softening finishing agent and making process thereof |
CN101029454A (en) * | 2006-02-27 | 2007-09-05 | 权力敏 | Antibacterial fabric softener |
CN101736580A (en) * | 2009-12-21 | 2010-06-16 | 北京绿泽宇和科技有限公司 | Fabric maintenance softener |
CN101935949A (en) * | 2010-08-27 | 2011-01-05 | 上海制皂有限公司 | Clothes softener |
CN102162189A (en) * | 2011-02-28 | 2011-08-24 | 河南省道纯化工技术有限公司 | Method for preparing fabric softening agent |
Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104762811A (en) * | 2015-03-26 | 2015-07-08 | 苏州威尔德工贸有限公司 | Special natural softener for textiles and preparation method for special natural softener |
CN105350312A (en) * | 2015-12-18 | 2016-02-24 | 苏州富美纺织科技有限公司 | Preparation method of blended fabric finishing liquid |
CN105926286A (en) * | 2016-05-30 | 2016-09-07 | 太仓红桥服饰有限公司 | Antibacterial softener for fabric and preparation method of antibacterial softener |
CN106957746A (en) * | 2017-03-07 | 2017-07-18 | 广州小蜜蜂生物科技有限公司 | Baby's pro-skin plant liquid detergent |
CN111764160A (en) * | 2020-07-14 | 2020-10-13 | 罗彦明 | Fabric softener |
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CN103668963B (en) | 2016-01-20 |
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