CN103663652A - Preparation method of sewage treatment agent - Google Patents

Preparation method of sewage treatment agent Download PDF

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Publication number
CN103663652A
CN103663652A CN201310671593.XA CN201310671593A CN103663652A CN 103663652 A CN103663652 A CN 103663652A CN 201310671593 A CN201310671593 A CN 201310671593A CN 103663652 A CN103663652 A CN 103663652A
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Prior art keywords
sewage
preparation
treating agent
sewage treatment
treatment agent
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CN201310671593.XA
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CN103663652B (en
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牟军平
于春光
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FENGHE JINQI TECHNOLOGY (BEIJING) CO., LTD.
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SHANDONG HWAYA ENVIRONMENTAL PROTECTION TECHNOLOGY Co Ltd
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  • Separation Of Suspended Particles By Flocculating Agents (AREA)

Abstract

The invention discloses a preparation method of a sewage treatment agent. Residual activated sludge in sewage treatment is processed and then mixed with other assistants, so as to prepare the sewage treatment agent. The preparation method is simple in operation, and the prepared sewage treatment agent is low in cost, good in effect and applicable to large-scale production. By adopting the sewage treatment agent prepared by the method disclosed by the invention, the removal rate of effluent suspended solids after treatment can be up to 99.8%, the biochemical oxygen demand (BOD) removal rate is 98%, the chemical oxygen demand (COD) removal rate is 98.5%, and the chromaticity is 5.

Description

A kind of preparation method of sewage-treating agent
Technical field
The present invention relates to technical field of sewage, particularly relate to a kind of preparation method of sewage-treating agent.
Background technology
The biologic treating technique that the activated sludge process of take is representative is the main treatment process of current sanitary sewage and most of trade effluent, after the processing power of active sludge declines, the utility value of residual active sludge just reduces, and residual active sludge is generally used as farmland fertilizer etc.In excess sludge, mainly contain the absorption of microorganism, Institute of Micro-biology organism and microbial metabolism activity product, mud is concentrated and the sewage-treating agent of conditioning use etc., and some sandy soil and salt inorganics etc.The a large amount of microorganisms that wherein contain and polysaccharide, protein, cellulosic material, still can in sewage disposal, be used as biological sewage treatment agent, in sewage disposal, play a role, its cost is lower, but the residual active sludge after wastewater treatment is directly used, weak effect, therefore, how residual active sludge being recovered as to efficient sewage-treating agent, is to need now the problem of solution.
Summary of the invention
Object of the present invention is exactly that a kind of preparation method of sewage-treating agent is provided for the defect of above-mentioned existence.By the standby one-tenth of residual actived sludge in sewage disposal sewage-treating agent, effective, cost is low, is applicable to scale operation.
Preparation method's technical scheme of a kind of sewage-treating agent of the present invention is that step is as follows:
(1) sewage treatment plant residual mud is mixed with water, filter;
(2) filtrate in step (1) being added to concentration is that 10% hydrochloric acid condition pH is 2-4, adds hydrogen peroxide simultaneously, after stirring, and centrifugation;
(3) after mixing with silicon-dioxide, sodium-acetate, polyacrylamide, EDTA, wilkinite, ferrous sulfate, solid matter centrifugation in step (2) being obtained enters granulator granulation.
In step (1), the filter screen that filters use is 80-200 order.
The mass percent that adds hydrogen peroxide in step (2) is 0.1%.
In step (2), stirring velocity is 200-500r/min, and churning time is 15-30 minute.
In step (3), solid matter and silicon-dioxide, sodium-acetate, polyacrylamide, EDTA, wilkinite, ferrous sulfate are by weight:
Figure BDA0000434491830000021
Beneficial effect of the present invention is: the present invention mixes with other auxiliary agents by after residual active sludge in sewage disposal is processed again, prepare sewage-treating agent, simple to operate, the sewage-treating agent cost of preparing is low, the effect that impurity in waste water is flocculated is remarkable, and take full advantage of residual active sludge, solved the recycling problem of residual active sludge.Sewage-treating agent prepared by the inventive method, it is that 98%, COD clearance is 98.5% that the rear wastewater suspended substance clearance of processing reaches 99.8%, BOD clearance, colourity is 5.
Embodiment:
In order to understand better the present invention, with specific examples, describe technical scheme of the present invention in detail below, but the present invention is not limited thereto.
Embodiment 1
Preparation method's technical scheme of a kind of sewage-treating agent of the present invention is that step is as follows:
(1) sewage treatment plant residual mud is mixed with water, filter, the filter screen that filters use is 150 orders;
(2) filtrate in step (1) being added to concentration is that 10% hydrochloric acid condition pH is 2-4, and add mass percent is 0.1% hydrogen peroxide simultaneously, and stirring velocity is 300r/min, after within 20 minutes, stirring, and centrifugation;
(3) after mixing with silicon-dioxide, sodium-acetate, polyacrylamide, EDTA, wilkinite, ferrous sulfate, solid matter centrifugation in step (2) being obtained enters granulator granulation.Wherein solid matter and silicon-dioxide, sodium-acetate, polyacrylamide, EDTA, wilkinite, ferrous sulfate are by weight:
Sewage-treating agent prepared by the inventive method, it is that 98%, COD clearance is 98.5% that the rear wastewater suspended substance clearance of processing reaches 99.8%, BOD clearance, colourity is 5.
Embodiment 2
Preparation method's technical scheme of a kind of sewage-treating agent of the present invention is that step is as follows:
(1) sewage treatment plant residual mud is mixed with water, filter, the filter screen that filters use is 200 orders;
(2) filtrate in step (1) being added to concentration is that 10% hydrochloric acid condition pH is 2-4, and add mass percent is 0.1% hydrogen peroxide simultaneously, and stirring velocity is 500r/min, after within 15 minutes, stirring, and centrifugation;
(3) after mixing with silicon-dioxide, sodium-acetate, polyacrylamide, EDTA, wilkinite, ferrous sulfate, solid matter centrifugation in step (2) being obtained enters granulator granulation.Wherein solid matter and silicon-dioxide, sodium-acetate, polyacrylamide, EDTA, wilkinite, ferrous sulfate are by weight:
Figure BDA0000434491830000032
Sewage-treating agent prepared by the inventive method, it is that 98%, COD clearance is 98.5% that the rear wastewater suspended substance clearance of processing reaches 99.8%, BOD clearance, colourity is 5.
Embodiment 3
Preparation method's technical scheme of a kind of sewage-treating agent of the present invention is that step is as follows:
(1) sewage treatment plant residual mud is mixed with water, filter, the filter screen that filters use is 80 orders;
(2) filtrate in step (1) being added to concentration is that 10% hydrochloric acid condition pH is 2-4, and add mass percent is 0.1% hydrogen peroxide simultaneously, and stirring velocity is 200r/min, after within 30 minutes, stirring, and centrifugation;
(3) after mixing with silicon-dioxide, sodium-acetate, polyacrylamide, EDTA, wilkinite, ferrous sulfate, solid matter centrifugation in step (2) being obtained enters granulator granulation.Wherein solid matter and silicon-dioxide, sodium-acetate, polyacrylamide, EDTA, wilkinite, ferrous sulfate are by weight:
Figure BDA0000434491830000041
Sewage-treating agent prepared by the inventive method, it is that 98%, COD clearance is 98.5% that the rear wastewater suspended substance clearance of processing reaches 99.8%, BOD clearance, colourity is 5.

Claims (5)

1. a preparation method for sewage-treating agent, is characterized in that, step is as follows:
(1) sewage treatment plant residual mud is mixed with water, filter;
(2) filtrate in step (1) being added to concentration is that 10% hydrochloric acid condition pH is 2-4, adds hydrogen peroxide simultaneously, after stirring, and centrifugation;
(3) after mixing with silicon-dioxide, sodium-acetate, polyacrylamide, EDTA, wilkinite, ferrous sulfate, solid matter centrifugation in step (2) being obtained enters granulator granulation.
2. the preparation method of a kind of sewage-treating agent according to claim 1, is characterized in that, in step (1), the filter screen that filters use is 80-200 order.
3. the preparation method of a kind of sewage-treating agent according to claim 1, is characterized in that, the mass percent that adds hydrogen peroxide in step (2) is 0.1%.
4. the preparation method of a kind of sewage-treating agent according to claim 1, is characterized in that, in step (2), stirring velocity is 200-500r/min, and churning time is 15-30 minute.
5. the preparation method of a kind of sewage-treating agent according to claim 1, is characterized in that, in step (3), solid matter and silicon-dioxide, sodium-acetate, polyacrylamide, EDTA, wilkinite, ferrous sulfate are by weight:
Figure FDA0000434491820000011
CN201310671593.XA 2013-12-11 2013-12-11 Preparation method of sewage treatment agent Expired - Fee Related CN103663652B (en)

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Cited By (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104071880A (en) * 2014-06-27 2014-10-01 南昌格润环保科技有限公司 Extensive wastewater treatment capture agent
CN104192965A (en) * 2014-09-19 2014-12-10 山东华亚环保科技有限公司 Papermaking sewage treatment agent
CN104291391A (en) * 2014-09-23 2015-01-21 博瑞德(南京)净化技术有限公司 Dyeing sewage treating agent and application method thereof
CN105439268A (en) * 2015-12-16 2016-03-30 无锡吉进环保科技有限公司 Preparation method of novel sewage processing agent
CN105776468A (en) * 2016-03-16 2016-07-20 徐亚萍 Preparation method of sewage cleansing agent
CN105906006A (en) * 2015-10-16 2016-08-31 湖北文理学院 Preparation method of domestic sewage treatment agent
CN105923731A (en) * 2015-10-16 2016-09-07 湖北文理学院 Preparation method of industrial water drainage treatment agent
CN106115810A (en) * 2016-07-29 2016-11-16 无锡信大气象传感网科技有限公司 A kind of sewage-treating agent and preparation method thereof
CN106186105A (en) * 2016-08-24 2016-12-07 米桂琼 A kind of preparation method of alkaline sewage inorganic agent
CN106186104A (en) * 2016-08-24 2016-12-07 米桂琼 A kind of preparation method of alkaline sewage inorganic agent
CN106256769A (en) * 2015-12-30 2016-12-28 湖北文理学院 A kind of preparation method of trade effluent cleaning agent
CN106277257A (en) * 2016-09-21 2017-01-04 芜湖扬展新材料科技服务有限公司 Efficient composite powdery sewage-treating agent for desized wastewater and preparation method thereof
CN106315803A (en) * 2016-09-21 2017-01-11 芜湖扬展新材料科技服务有限公司 Composite powder-shaped sewage treating agent for PVA (polyvinyl alcohol) desizing waste water and preparation method thereof
CN106315874A (en) * 2016-09-21 2017-01-11 芜湖扬展新材料科技服务有限公司 High-efficient composite powder-shaped sewage treating agent for desizing waste water and preparation method thereof
CN106335989A (en) * 2015-12-30 2017-01-18 湖北文理学院 Preparation method of domestic sewage cleaning agent

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US6203711B1 (en) * 1999-05-21 2001-03-20 E. I. Du Pont De Nemours And Company Method for treatment of substantially aqueous fluids derived from processing inorganic materials
CN101254959A (en) * 2008-03-25 2008-09-03 浙江华特新材料股份有限公司 Bentonite sewage water treating method
CN101885526A (en) * 2009-05-16 2010-11-17 兰州大欣水工业有限责任公司 Ternary composite type flocculant, preparation and application

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6203711B1 (en) * 1999-05-21 2001-03-20 E. I. Du Pont De Nemours And Company Method for treatment of substantially aqueous fluids derived from processing inorganic materials
CN101254959A (en) * 2008-03-25 2008-09-03 浙江华特新材料股份有限公司 Bentonite sewage water treating method
CN101885526A (en) * 2009-05-16 2010-11-17 兰州大欣水工业有限责任公司 Ternary composite type flocculant, preparation and application

Cited By (20)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104071880A (en) * 2014-06-27 2014-10-01 南昌格润环保科技有限公司 Extensive wastewater treatment capture agent
CN104192965A (en) * 2014-09-19 2014-12-10 山东华亚环保科技有限公司 Papermaking sewage treatment agent
CN104192965B (en) * 2014-09-19 2016-05-25 冯进器 A kind for the treatment of agent for papermaking wastewater
CN104291391A (en) * 2014-09-23 2015-01-21 博瑞德(南京)净化技术有限公司 Dyeing sewage treating agent and application method thereof
CN105923731B (en) * 2015-10-16 2018-08-17 湖北文理学院 A kind of preparation method of industrial water drainage inorganic agent
CN105906006B (en) * 2015-10-16 2018-08-17 湖北文理学院 A kind of preparation method of living drainage inorganic agent
CN105906006A (en) * 2015-10-16 2016-08-31 湖北文理学院 Preparation method of domestic sewage treatment agent
CN105923731A (en) * 2015-10-16 2016-09-07 湖北文理学院 Preparation method of industrial water drainage treatment agent
CN105439268A (en) * 2015-12-16 2016-03-30 无锡吉进环保科技有限公司 Preparation method of novel sewage processing agent
CN106256769B (en) * 2015-12-30 2019-05-03 湖北文理学院 A kind of preparation method of trade effluent detergent
CN106335989B (en) * 2015-12-30 2019-05-03 湖北文理学院 A kind of preparation method of sanitary sewage detergent
CN106256769A (en) * 2015-12-30 2016-12-28 湖北文理学院 A kind of preparation method of trade effluent cleaning agent
CN106335989A (en) * 2015-12-30 2017-01-18 湖北文理学院 Preparation method of domestic sewage cleaning agent
CN105776468A (en) * 2016-03-16 2016-07-20 徐亚萍 Preparation method of sewage cleansing agent
CN106115810A (en) * 2016-07-29 2016-11-16 无锡信大气象传感网科技有限公司 A kind of sewage-treating agent and preparation method thereof
CN106186104A (en) * 2016-08-24 2016-12-07 米桂琼 A kind of preparation method of alkaline sewage inorganic agent
CN106186105A (en) * 2016-08-24 2016-12-07 米桂琼 A kind of preparation method of alkaline sewage inorganic agent
CN106315874A (en) * 2016-09-21 2017-01-11 芜湖扬展新材料科技服务有限公司 High-efficient composite powder-shaped sewage treating agent for desizing waste water and preparation method thereof
CN106315803A (en) * 2016-09-21 2017-01-11 芜湖扬展新材料科技服务有限公司 Composite powder-shaped sewage treating agent for PVA (polyvinyl alcohol) desizing waste water and preparation method thereof
CN106277257A (en) * 2016-09-21 2017-01-04 芜湖扬展新材料科技服务有限公司 Efficient composite powdery sewage-treating agent for desized wastewater and preparation method thereof

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