CN106256769A - A kind of preparation method of trade effluent cleaning agent - Google Patents

A kind of preparation method of trade effluent cleaning agent Download PDF

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Publication number
CN106256769A
CN106256769A CN201511011326.5A CN201511011326A CN106256769A CN 106256769 A CN106256769 A CN 106256769A CN 201511011326 A CN201511011326 A CN 201511011326A CN 106256769 A CN106256769 A CN 106256769A
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CN
China
Prior art keywords
weight portion
powder
cleaning agent
trade effluent
parts
Prior art date
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Granted
Application number
CN201511011326.5A
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Chinese (zh)
Other versions
CN106256769B (en
Inventor
李玉奇
梁英
黄升谋
林淦
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Hubei University of Arts and Science
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Hubei University of Arts and Science
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Priority to CN201511011326.5A priority Critical patent/CN106256769B/en
Publication of CN106256769A publication Critical patent/CN106256769A/en
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Publication of CN106256769B publication Critical patent/CN106256769B/en
Expired - Fee Related legal-status Critical Current
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    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00Treatment of water, waste water, or sewage
    • C02F1/52Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities
    • C02F1/5236Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities using inorganic agents
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00Treatment of water, waste water, or sewage
    • C02F1/52Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities
    • C02F1/5263Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities using natural chemical compounds
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00Treatment of water, waste water, or sewage
    • C02F1/52Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities
    • C02F1/54Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities using organic material
    • C02F1/56Macromolecular compounds

Abstract

The invention discloses the preparation method of a kind of trade effluent cleaning agent, by mixing with other auxiliary agents again after being processed by multiple biological raw material, prepare trade effluent cleaning agent.The present invention is simple to operate, the trade effluent cleaning agent low cost prepared, effective, is suitable for large-scale production.Trade effluent cleaning agent prepared by the inventive method, processes postindustrial wastewater suspended substance clearance and reaches more than 94%, and BOD clearance is more than 92%, and COD clearance is more than 93%.

Description

A kind of preparation method of trade effluent cleaning agent
Technical field
The present invention relates to technical field of industrial sewage treatment, particularly relate to the preparation method of a kind of trade effluent cleaning agent.
Background technology
Industrial wastewater refers to waste water, sewage and the waste liquid produced in industrial processes, wherein contains the pollutant produced in commercial production materials, intermediate product and the product and production process outflowed with water.Along with developing rapidly of industry, kind and the quantity of waste water rapidly increase, and the pollution to water body is the most extensive and serious, threatens the health and safety of the mankind.Therefore, for protection environment, processing of industrial wastewater is more even more important than the process of municipal sewage.Industrial waste water treatment agent mainly has at present, aluminum sulfate, iron sulfate, iron chloride, titanium tetrachloride and inorganic bronsted lowry acids and bases bronsted lowry, ATMP (ATMP), 1-hydroxy ethylidene-1,1-diphosphonic acid (HEDP), sodium polyacrylate (PAAS), liquid chlorine, calcium hypochlorite etc..These inorganic agents mostly are single component, all can only remove pollutant limited in waste water, it is difficult to reach the purpose of comprehensive control industrial wastewater.
Summary of the invention
The purpose of the present invention is aiming at the defect of above-mentioned existence and provides the preparation method of a kind of trade effluent cleaning agent.Multiple biological raw material is prepared as trade effluent cleaning agent, effective, low cost, it is suitable for large-scale production.
The technical scheme is that
(1) multiple biological raw material is uniformly mixed with water weight ratio 1:8, filters;
(2) filtrate in step (1) being added concentration is the acetic acid of 10%, and regulation pH is 1-4, is simultaneously introduced potassium permanganate solid, after stirring, centrifugation;
(3) by the solid matter being centrifugally separating to obtain in step (2) and silicon dioxide, sodium chloride, magnesium sulfate, sodium peroxydisulfate, polyacrylamide, acrylamide, enter granulator granulation after the mixing of calcium phosphate, bentonite;
Solid matter and silicon dioxide, sodium chloride in step (3), magnesium sulfate, sodium peroxydisulfate, polyacrylamide, acrylamide, calcium phosphate, bentonite be by weight:
Solid matter 70-80 weight portion
Silica 1 0-15 weight portion
Sodium chloride 10-15 weight portion
Magnesium sulfate 5-10 weight portion
Sodium peroxydisulfate 5-10 weight portion
Polyacrylamide 10-15 weight portion
Acrylamide 10-20 weight portion
Calcium phosphate 5-10 weight portion
Bentonite 10-15 weight portion.
In step (1), mixing speed is 100-200rpm, and mixing time is 20-30 minute, and the filter screen filtered is 50-100 mesh.
The total solution weight percentage ratio adding potassium permanganate in step (2) is 8%.
In step (2), mixing speed is 100-200rpm, and mixing time is 20-30 minute, and centrifugal speed is 3000rpm, and centrifugation time is 10 minutes.
Multiple biological raw material includes rice meal, Carnis Gallus domesticus powder, fish powder, flour, Rhizoma Dioscoreae powder, dry scallop powder, peanut powder, and multiple biological raw material weight ratio is rice meal 5 parts, Carnis Gallus domesticus powder 3 parts, fish powder 5 parts, 5 parts of flour, Rhizoma Dioscoreae powder 5 parts, 1 part of dry scallop powder, peanut powder 5 parts.
The invention have the benefit that by mixing with other auxiliary agents after being processed by multiple biological raw material again, prepare trade effluent cleaning agent, simple to operate, the trade effluent cleaning agent low cost prepared, the effect flocculating the impurity in waste water is notable.Trade effluent cleaning agent prepared by the inventive method, processes postindustrial wastewater suspended substance clearance and reaches more than 94%, and BOD clearance is more than 92%, and COD clearance is more than 93%.
Detailed description of the invention:
In order to be more fully understood that the present invention, describe technical scheme in detail with instantiation below, but the invention is not limited in this.
Embodiment 1
The preparation method of a kind of trade effluent cleaning agent is as follows:
(1) multiple biological raw material is uniformly mixed with water weight ratio 1:8, filters;
(2) filtrate in step (1) being added concentration is the acetic acid of 10%, and regulation pH is 1, is simultaneously introduced potassium permanganate solid, after stirring, centrifugation;
(3) by the solid matter being centrifugally separating to obtain in step (2) and silicon dioxide, sodium chloride, magnesium sulfate, sodium peroxydisulfate, polyacrylamide, acrylamide, enter granulator granulation after the mixing of calcium phosphate, bentonite;
Solid matter and silicon dioxide, sodium chloride in step (3), magnesium sulfate, sodium peroxydisulfate, polyacrylamide, acrylamide, calcium phosphate, bentonite be by weight:
Solid matter 70 weight portion
Silica 10 weight portion
Sodium chloride 10 weight portion
Magnesium sulfate 5 weight portion
Sodium peroxydisulfate 5 weight portion
Polyacrylamide 10 weight portion
Acrylamide 10 weight portion
Calcium phosphate 5 weight portion
Bentonite 10 weight portion.
In step (1), mixing speed is 100rpm, and mixing time is 20 minutes, and the filter screen filtered is 50 mesh.
The total solution weight percentage ratio adding potassium permanganate solid in step (2) is 8%.
In step (2), mixing speed is 100rpm, and mixing time is 20 minutes.Centrifugal speed is 3000rpm, and centrifugation time is 10 minutes.
Multiple biological raw material includes rice meal, Carnis Gallus domesticus powder, fish powder, flour, Rhizoma Dioscoreae powder, dry scallop powder, peanut powder.Multiple biological raw material weight ratio is rice meal 5 parts, Carnis Gallus domesticus powder 3 parts, fish powder 5 parts, 5 parts of flour, Rhizoma Dioscoreae powder 5 parts, 1 part of dry scallop powder, peanut powder 5 parts.
Trade effluent cleaning agent prepared by the inventive method, processes postindustrial wastewater suspended substance clearance and reaches 94%, and BOD clearance is 92%, and COD clearance is 93%.
Embodiment 2
The preparation method of a kind of trade effluent cleaning agent is as follows:
(1) multiple biological raw material is uniformly mixed with water weight ratio 1:8, filters;
(2) filtrate in step (1) being added concentration is the acetic acid of 10%, and regulation pH is 2, is simultaneously introduced potassium permanganate solid, after stirring, centrifugation;
(3) by the solid matter being centrifugally separating to obtain in step (2) and silicon dioxide, sodium chloride, magnesium sulfate, sodium peroxydisulfate, polyacrylamide, acrylamide, enter granulator granulation after the mixing of calcium phosphate, bentonite;
Solid matter and silicon dioxide, sodium chloride in step (3), magnesium sulfate, sodium peroxydisulfate, polyacrylamide, acrylamide, calcium phosphate, bentonite be by weight:
Solid matter 75 weight portion
Silica 12 weight portion
Sodium chloride 12 weight portion
Magnesium sulfate 8 weight portion
Sodium peroxydisulfate 8 weight portion
Polyacrylamide 12 weight portion
Acrylamide 15 weight portion
Calcium phosphate 8 weight portion
Bentonite 12 weight portion.
In step (1), mixing speed is 150rpm, and mixing time is 25 minutes, and the filter screen filtered is 80 mesh.
The total solution weight percentage ratio adding potassium permanganate solid in step (2) is 8%.
In step (2), mixing speed is 150rpm, and mixing time is 25 minutes.Centrifugal speed is 3000rpm, and centrifugation time is 10 minutes.
Multiple biological raw material includes rice meal, Carnis Gallus domesticus powder, fish powder, flour, Rhizoma Dioscoreae powder, dry scallop powder, peanut powder.Multiple biological raw material weight ratio is rice meal 5 parts, Carnis Gallus domesticus powder 3 parts, fish powder 5 parts, 5 parts of flour, Rhizoma Dioscoreae powder 5 parts, 1 part of dry scallop powder, peanut powder 5 parts.
Trade effluent cleaning agent prepared by the inventive method, processes postindustrial wastewater suspended substance clearance and reaches 95%, and BOD clearance is 93%, and COD clearance is 94%.
Embodiment 3
The preparation method of a kind of trade effluent cleaning agent is as follows:
(1) multiple biological raw material is uniformly mixed with water weight ratio 1:8, filters;
(2) filtrate in step (1) being added concentration is the acetic acid of 10%, and regulation pH is 4, is simultaneously introduced potassium permanganate solid, after stirring, centrifugation;
(3) by the solid matter being centrifugally separating to obtain in step (2) and silicon dioxide, sodium chloride, magnesium sulfate, sodium peroxydisulfate, polyacrylamide, acrylamide, enter granulator granulation after the mixing of calcium phosphate, bentonite;
Solid matter and silicon dioxide, sodium chloride in step (3), magnesium sulfate, sodium peroxydisulfate, polyacrylamide, acrylamide, calcium phosphate, bentonite be by weight:
Solid matter 80 weight portion
Silica 15 weight portion
Sodium chloride 15 weight portion
Magnesium sulfate 10 weight portion
Sodium peroxydisulfate 10 weight portion
Polyacrylamide 15 weight portion
Acrylamide 20 weight portion
Calcium phosphate 10 weight portion
Bentonite 15 weight portion.
In step (1), mixing speed is 200rpm, and mixing time is 30 minutes, and the filter screen filtered is 100 mesh.
The total solution weight percentage ratio adding potassium permanganate solid in step (2) is 8%.Centrifugal speed is 3000rpm, and centrifugation time is 10 minutes.
In step (2), mixing speed is 200rpm, and mixing time is 30 minutes.
Multiple biological raw material includes rice meal, Carnis Gallus domesticus powder, fish powder, flour, Rhizoma Dioscoreae powder, dry scallop powder, peanut powder.Multiple biological raw material weight ratio is rice meal 5 parts, Carnis Gallus domesticus powder 3 parts, fish powder 5 parts, 5 parts of flour, Rhizoma Dioscoreae powder 5 parts, 1 part of dry scallop powder, peanut powder 5 parts.
Trade effluent cleaning agent prepared by the inventive method, processes postindustrial wastewater suspended substance clearance and reaches 96%, and BOD clearance is 94%, and COD clearance is 93%.

Claims (5)

1. the preparation method of a trade effluent cleaning agent, it is characterised in that step is as follows:
(1) multiple biological raw material is uniformly mixed with water weight ratio 1:8, filters;
(2) filtrate in step (1) being added concentration is the acetic acid of 10%, and regulation pH is 1-4, is simultaneously introduced potassium permanganate solid, after stirring, centrifugation;
(3) by the solid matter being centrifugally separating to obtain in step (2) and silicon dioxide, sodium chloride, magnesium sulfate, sodium peroxydisulfate, polyacrylamide, acrylamide, enter granulator granulation after the mixing of calcium phosphate, bentonite;
Solid matter and silicon dioxide, sodium chloride in step (3), magnesium sulfate, sodium peroxydisulfate, polyacrylamide, acrylamide, calcium phosphate, bentonite be by weight:
Solid matter 70-80 weight portion
Silica 1 0-15 weight portion
Sodium chloride 10-15 weight portion
Magnesium sulfate 5-10 weight portion
Sodium peroxydisulfate 5-10 weight portion
Polyacrylamide 10-15 weight portion
Acrylamide 10-20 weight portion
Calcium phosphate 5-10 weight portion
Bentonite 10-15 weight portion.
The preparation method of a kind of trade effluent cleaning agent the most according to claim 1, it is characterised in that in step (1), mixing speed is 100-200rpm, and mixing time is 20-30 minute, and the filter screen filtered is 50-100 mesh.
The preparation method of a kind of trade effluent cleaning agent the most according to claim 1, it is characterised in that the total solution weight percentage ratio adding potassium permanganate in step (2) is 8%.
The preparation method of a kind of trade effluent cleaning agent the most according to claim 1, it is characterised in that in step (2), mixing speed is 100-200rpm, mixing time is 20-30 minute, and centrifugal speed is 3000rpm, and centrifugation time is 10 minutes.
The preparation method of a kind of trade effluent cleaning agent the most according to claim 1, it is characterised in that multiple biological raw material includes rice meal, Carnis Gallus domesticus powder, fish powder, flour, Rhizoma Dioscoreae powder, dry scallop powder, peanut powder, multiple biological raw material weight ratio is rice meal 5 parts, Carnis Gallus domesticus powder 3 parts, fish powder 5 parts, 5 parts of flour, Rhizoma Dioscoreae powder 5 parts, 1 part of dry scallop powder, peanut powder 5 parts.
CN201511011326.5A 2015-12-30 2015-12-30 A kind of preparation method of trade effluent detergent Expired - Fee Related CN106256769B (en)

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Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201511011326.5A CN106256769B (en) 2015-12-30 2015-12-30 A kind of preparation method of trade effluent detergent

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CN106256769A true CN106256769A (en) 2016-12-28
CN106256769B CN106256769B (en) 2019-05-03

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106495259A (en) * 2016-12-30 2017-03-15 余姚市哈特馒餐饮有限公司 A kind of efficient domestic sewage treating compound
CN111186890A (en) * 2019-11-08 2020-05-22 张如意 Preparation method of industrial cleaning agent

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103663652A (en) * 2013-12-11 2014-03-26 山东华亚环保科技有限公司 Preparation method of sewage treatment agent
CN103663651A (en) * 2013-12-11 2014-03-26 山东华亚环保科技有限公司 Preparation method of sewage flocculant

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103663652A (en) * 2013-12-11 2014-03-26 山东华亚环保科技有限公司 Preparation method of sewage treatment agent
CN103663651A (en) * 2013-12-11 2014-03-26 山东华亚环保科技有限公司 Preparation method of sewage flocculant

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106495259A (en) * 2016-12-30 2017-03-15 余姚市哈特馒餐饮有限公司 A kind of efficient domestic sewage treating compound
CN111186890A (en) * 2019-11-08 2020-05-22 张如意 Preparation method of industrial cleaning agent

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