CN106335989B - A kind of preparation method of sanitary sewage detergent - Google Patents
A kind of preparation method of sanitary sewage detergent Download PDFInfo
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- CN106335989B CN106335989B CN201511011325.0A CN201511011325A CN106335989B CN 106335989 B CN106335989 B CN 106335989B CN 201511011325 A CN201511011325 A CN 201511011325A CN 106335989 B CN106335989 B CN 106335989B
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Classifications
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/52—Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities
- C02F1/54—Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities using organic material
- C02F1/56—Macromolecular compounds
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/52—Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities
- C02F1/5236—Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities using inorganic agents
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/52—Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities
- C02F1/5263—Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities using natural chemical compounds
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/52—Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities
- C02F1/54—Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities using organic material
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Hydrology & Water Resources (AREA)
- Engineering & Computer Science (AREA)
- Environmental & Geological Engineering (AREA)
- Water Supply & Treatment (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Detergent Compositions (AREA)
- Separation Of Suspended Particles By Flocculating Agents (AREA)
Abstract
The invention discloses a kind of preparation methods of sanitary sewage detergent to prepare sanitary sewage detergent by mixing again with other auxiliary agents after being handled a variety of biological raw materials, it is easy to operate, the sanitary sewage detergent prepared is at low cost, and effect is good, is suitble to large-scale production.The sanitary sewage detergent of the method for the present invention preparation, it be 95% or more, COD removal rate is 95% or more that sanitary sewage removal efficiency, which reaches 96% or more, BOD removal rate, after processing.
Description
Technical field
The present invention relates to sanitary sewage disposal technical fields, more particularly to a kind of preparation side of sanitary sewage detergent
Method.
Background technique
The sewage generated during human lives, is one of primary pollution source of water body.Mainly excrement and wash water.
Contain large amount of organic, such as cellulose, starch, carbohydrate and fat protein in sanitary sewage;Also often contain pathogen, virus
And parasitic ovum;Chloride, sulfate, phosphate, bicarbonate and the sodium of inorganic salts, potassium, calcium, magnesium etc..Total feature is
Nitrogenous, sulfur-bearing and phosphorous height, under anaerobic bacteria effect, easily raw odorant.Existing sanitary sewage disposal substance has, polymerised sulphur
Sour iron is a kind of inorganic polymer coagulant water purification material that developed on the basis of aluminium salt and molysite coagulation Hydrolytic Mechanism
Material.According to synergistic principle, it is new that one kind that simple substance iron ion or ferric oxide and other iron containing compounds are combined is added
Type coagulant.Aluminum sulfate, not easy-weathering and lose the crystallization water, it is more stable, heating can dehydration, high temperature can be decomposed into oxidation
Aluminium and sulfur oxide.Aluminium hydroxide is generated after hydrolysis.Aqueous solution boils for a long time produces basic aluminium sulphate.Industrial goods are ash
It is white plates, granular or blocky, so that surface is turned to be yellow with light green, and due to low price molysite is oxidized due to containing low molysite.Crude product
For canescence aplitic texture cellular object.Nontoxic, dust can stimulate eyes.Aluminium polychloride, sewage treatment aluminium polychloride
Special increase temperature extends the reaction time, so that entire Molecularly Imprinted Polymer structure is more huge, gantry distribution is more reasonable, so that
There are stronger adsorption capacity and cohesiveness, be the first choice of medicament used in Industrial Wastewater Treatment, it can decline to a great extent cost of water treatment.It is poly-
Acrylamide, under the premise of reaching same water quality, polyacrylamide as flocculation aid and other flocculants (it is mainly inorganic or
Person's organic coagulants) it is used cooperatively, the usage amount of flocculant can be substantially reduced.Improve water quality.In drinking water treatment and Industry Waste
In the treatment process of water, polyacrylamide and inorganic coagulant are used, and can obviously improve effluent quality.These detergents are due to adopting
It, can only Cucumber in single treatment sewage with monistic chemical substance, it is difficult to achieve the purpose that integrated treatment, it is also difficult to
The suspended matter in sanitary sewage, BOD and COD are removed simultaneously.
Summary of the invention
A kind of preparation method of sanitary sewage detergent is provided the purpose of the present invention is to above-mentioned defect.
A variety of biological raw materials are prepared into sanitary sewage detergent, effect is good, and it is at low cost, it is suitble to large-scale production.
A kind of preparation method technical solution of sanitary sewage detergent of the invention is that steps are as follows:
(1) a variety of biological raw materials and water weight ratio 1:7 are uniformly mixed, are filtered;
(2) phosphoric acid that concentration is 10% is added in the filtrate in step (1), adjusting pH is 1-3, while potassium permanganate is added
Solid, after mixing evenly, centrifuge separation;
(3) by the solid matter being centrifugally separating to obtain in step (2) and sulfur dioxide, calcium chloride, calcirm-fluoride, bicarbonate
Calcium, polyacrylamide, acrylamide enter pelletizer after sodium benzoate, bentonite mixing and are granulated;
Solid matter and sulfur dioxide, calcium chloride, calcirm-fluoride, calcium bicarbonate, polyacrylamide, acryloyl in step (3)
Amine, sodium benzoate, bentonite are by weight are as follows:
Solid matter 60-70 parts by weight
Sulfur dioxide 10-20 parts by weight
Calcium chloride 10-20 parts by weight
Calcirm-fluoride 10-20 parts by weight
Calcium bicarbonate 5-10 parts by weight
Polyacrylamide 5-10 parts by weight
Acrylamide 5-10 parts by weight
Sodium benzoate 5-10 parts by weight
Bentonite 10-15 parts by weight.
In step (1), mixing speed 100-200rpm, mixing time is 20-30 minutes, and the strainer of filtering is 100-
200 mesh.
The total solution weight percent that potassium permanganate is added in step (2) is 10%.
Mixing speed is 100-200rpm in step (2), and mixing time is 30-60 minutes, centrifugal speed 3000-
6000rpm, centrifugation time are 10 minutes.
A variety of biological raw materials include oatmeal, powder of pork, chicken meal, licorice powder, ginseng pulverate, laver powder, and peanut powder is more
Kind of biological raw material weight ratio is 5 parts of oatmeal, 15 parts of powder of pork, 30 parts of chicken meal, and 5 parts of licorice powder, 1 part of ginseng pulverate, laver powder
15 parts, 5 parts of peanut powder.
The invention has the benefit that the present invention with other auxiliary agents by carrying out again after handling a variety of biological raw materials
Mixing, prepares sanitary sewage detergent, easy to operate, the sanitary sewage detergent prepared is at low cost, to the impurity in waste water
Carry out flocculated significant effect.The sanitary sewage detergent of the method for the present invention preparation, sanitary sewage removal efficiency after processing
It is 95% or more that reach 96% or more, BOD removal rate, which be 95% or more, COD removal rate,.
Specific embodiment:
For a better understanding of the present invention, below with specific example come the technical solution that the present invention will be described in detail, but this
Invention is not limited thereto.
Embodiment 1
(1) a variety of biological raw materials and water weight ratio 1:7 are uniformly mixed, are filtered;
(2) phosphoric acid that concentration is 10% is added in the filtrate in step (1), adjusting pH is 1, while it is solid that potassium permanganate is added
Body, after mixing evenly, centrifuge separation;
(3) by the solid matter being centrifugally separating to obtain in step (2) and sulfur dioxide, calcium chloride, calcirm-fluoride, bicarbonate
Calcium, polyacrylamide, acrylamide enter pelletizer after sodium benzoate, bentonite mixing and are granulated;
Solid matter and sulfur dioxide, calcium chloride, calcirm-fluoride, calcium bicarbonate, polyacrylamide, acryloyl in step (3)
Amine, sodium benzoate, bentonite are by weight are as follows:
60 parts by weight of solid matter
10 parts by weight of sulfur dioxide
10 parts by weight of calcium chloride
10 parts by weight of calcirm-fluoride
5 parts by weight of calcium bicarbonate
5 parts by weight of polyacrylamide
5 parts by weight of acrylamide
5 parts by weight of sodium benzoate
10 parts by weight of bentonite.
In step (1), mixing speed 100rpm, mixing time is 20 minutes, and the strainer of filtering is 100 mesh.
The total solution weight percent that potassium permanganate is added in step (2) is 10%.
Mixing speed is 100rpm in step (2), and mixing time is 30 minutes, centrifugal speed 3000rpm, centrifugation time
It is 10 minutes.
A variety of biological raw materials include oatmeal, powder of pork, chicken meal, licorice powder, ginseng pulverate, laver powder, and peanut powder is more
Kind of biological raw material weight ratio is 5 parts of oatmeal, 15 parts of powder of pork, 30 parts of chicken meal, and 5 parts of licorice powder, 1 part of ginseng pulverate, laver powder
15 parts, 5 parts of peanut powder.
The sanitary sewage detergent of the method for the present invention preparation, sanitary sewage removal efficiency reaches 96%, BOD after processing
Removal rate is that 95%, COD removal rate is 95%.
Embodiment 2
A kind of preparation method technical solution of sanitary sewage detergent of the invention is that steps are as follows:
(1) a variety of biological raw materials and water weight ratio 1:7 are uniformly mixed, are filtered;
(2) phosphoric acid that concentration is 10% is added in the filtrate in step (1), adjusting pH is 2, while it is solid that potassium permanganate is added
Body, after mixing evenly, centrifuge separation;
(3) by the solid matter being centrifugally separating to obtain in step (2) and sulfur dioxide, calcium chloride, calcirm-fluoride, bicarbonate
Calcium, polyacrylamide, acrylamide enter pelletizer after sodium benzoate, bentonite mixing and are granulated;
Solid matter and sulfur dioxide, calcium chloride, calcirm-fluoride, calcium bicarbonate, polyacrylamide, acryloyl in step (3)
Amine, sodium benzoate, bentonite are by weight are as follows:
65 parts by weight of solid matter
15 parts by weight of sulfur dioxide
15 parts by weight of calcium chloride
15 parts by weight of calcirm-fluoride
8 parts by weight of calcium bicarbonate
8 parts by weight of polyacrylamide
8 parts by weight of acrylamide
8 parts by weight of sodium benzoate
12 parts by weight of bentonite.
In step (1), mixing speed 150rpm, mixing time is 25 minutes, and the strainer of filtering is 150 mesh.
The total solution weight percent that potassium permanganate is added in step (2) is 10%.
Mixing speed is 150rpm in step (2), and mixing time is 45 minutes, centrifugal speed 5000rpm, centrifugation time
It is 10 minutes.
A variety of biological raw materials include oatmeal, powder of pork, chicken meal, licorice powder, ginseng pulverate, laver powder, and peanut powder is more
Kind of biological raw material weight ratio is 5 parts of oatmeal, 15 parts of powder of pork, 30 parts of chicken meal, and 5 parts of licorice powder, 1 part of ginseng pulverate, laver powder
15 parts, 5 parts of peanut powder.
The sanitary sewage detergent of the method for the present invention preparation, sanitary sewage removal efficiency reaches 97%, BOD after processing
Removal rate is that 97%, COD removal rate is 97%.
Embodiment 3
A kind of preparation method technical solution of sanitary sewage detergent of the invention is that steps are as follows:
(1) a variety of biological raw materials and water weight ratio 1:7 are uniformly mixed, are filtered;
(2) phosphoric acid that concentration is 10% is added in the filtrate in step (1), adjusting pH is 3, while it is solid that potassium permanganate is added
Body, after mixing evenly, centrifuge separation;
(3) by the solid matter being centrifugally separating to obtain in step (2) and sulfur dioxide, calcium chloride, calcirm-fluoride, bicarbonate
Calcium, polyacrylamide, acrylamide enter pelletizer after sodium benzoate, bentonite mixing and are granulated;
Solid matter and sulfur dioxide, calcium chloride, calcirm-fluoride, calcium bicarbonate, polyacrylamide, acryloyl in step (3)
Amine, sodium benzoate, bentonite are by weight are as follows:
70 parts by weight of solid matter
20 parts by weight of sulfur dioxide
20 parts by weight of calcium chloride
20 parts by weight of calcirm-fluoride
10 parts by weight of calcium bicarbonate
10 parts by weight of polyacrylamide
10 parts by weight of acrylamide
10 parts by weight of sodium benzoate
15 parts by weight of bentonite.
In step (1), mixing speed 200rpm, mixing time is 30 minutes, and the strainer of filtering is 200 mesh.
The total solution weight percent that potassium permanganate is added in step (2) is 10%.
Mixing speed is 200rpm in step (2), and mixing time is 60 minutes, centrifugal speed 6000rpm, centrifugation time
It is 10 minutes.
A variety of biological raw materials include oatmeal, powder of pork, chicken meal, licorice powder, ginseng pulverate, laver powder, and peanut powder is more
Kind of biological raw material weight ratio is 5 parts of oatmeal, 15 parts of powder of pork, 30 parts of chicken meal, and 5 parts of licorice powder, 1 part of ginseng pulverate, laver powder
15 parts, 5 parts of peanut powder.
The sanitary sewage detergent of the method for the present invention preparation, sanitary sewage removal efficiency reaches 97%, BOD after processing
Removal rate is that 98%, COD removal rate is 98%.
Claims (4)
1. a kind of preparation method of sanitary sewage detergent, which is characterized in that steps are as follows:
(1) a variety of biological raw materials and water weight ratio 1:7 are uniformly mixed, are filtered;
(2) phosphoric acid that concentration is 10% being added in the filtrate in step (1), adjusting pH is 1-3, while potassium permanganate solid is added,
After mixing evenly, it is centrifugated;
(3) by the solid matter being centrifugally separating to obtain in step (2) and sulfur dioxide, calcium chloride, calcirm-fluoride is calcium bicarbonate, poly-
Acrylamide, acrylamide enter pelletizer after sodium benzoate, bentonite mixing and are granulated;
Solid matter and sulfur dioxide, calcium chloride, calcirm-fluoride, calcium bicarbonate, polyacrylamide, acrylamide, benzene in step (3)
Sodium formate, bentonite are by weight are as follows:
Solid matter 60-70 parts by weight;
Sulfur dioxide 10-20 parts by weight;
Calcium chloride 10-20 parts by weight;
Calcirm-fluoride 10-20 parts by weight;
Calcium bicarbonate 5-10 parts by weight;
Polyacrylamide 5-10 parts by weight;
Acrylamide 5-10 parts by weight;
Sodium benzoate 5-10 parts by weight;
Bentonite 10-15 parts by weight;
A variety of biological raw materials include oatmeal, powder of pork, chicken meal, licorice powder, ginseng pulverate, laver powder, and peanut powder is more
Kind of biological raw material weight ratio is 5 parts of oatmeal, 15 parts of powder of pork, 30 parts of chicken meal, and 5 parts of licorice powder, 1 part of ginseng pulverate, laver powder
15 parts, 5 parts of peanut powder.
2. a kind of preparation method of sanitary sewage detergent according to claim 1, which is characterized in that in step (1), stir
Mixing speed is 100-200rpm, and mixing time is 20-30 minutes, and the strainer of filtering is 100-200 mesh.
3. a kind of preparation method of sanitary sewage detergent according to claim 1, which is characterized in that add in step (2)
The total solution weight percent for entering potassium permanganate is 10%.
4. a kind of preparation method of sanitary sewage detergent according to claim 1, which is characterized in that step is stirred in (2)
Mixing speed is 100-200rpm, and mixing time is 30-60 minutes, centrifugal speed 3000-6000rpm, and centrifugation time is 10 points
Clock.
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Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
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CN103663651A (en) * | 2013-12-11 | 2014-03-26 | 山东华亚环保科技有限公司 | Preparation method of sewage flocculant |
CN103663652A (en) * | 2013-12-11 | 2014-03-26 | 山东华亚环保科技有限公司 | Preparation method of sewage treatment agent |
CN104815623A (en) * | 2015-04-10 | 2015-08-05 | 合肥环照高分子材料厂 | Rice husk-based heavy metal adsorbent and preparation method thereof |
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Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103663651A (en) * | 2013-12-11 | 2014-03-26 | 山东华亚环保科技有限公司 | Preparation method of sewage flocculant |
CN103663652A (en) * | 2013-12-11 | 2014-03-26 | 山东华亚环保科技有限公司 | Preparation method of sewage treatment agent |
CN104815623A (en) * | 2015-04-10 | 2015-08-05 | 合肥环照高分子材料厂 | Rice husk-based heavy metal adsorbent and preparation method thereof |
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