CN105906006A - Preparation method of domestic sewage treatment agent - Google Patents

Preparation method of domestic sewage treatment agent Download PDF

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Publication number
CN105906006A
CN105906006A CN201510667943.4A CN201510667943A CN105906006A CN 105906006 A CN105906006 A CN 105906006A CN 201510667943 A CN201510667943 A CN 201510667943A CN 105906006 A CN105906006 A CN 105906006A
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powder
preparation
biological raw
life
raw material
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CN105906006B (en
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阎华�
李云捷
于博
汤尚文
黄升谋
林淦
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Dongguan Lanshen environmental protection Co., Ltd
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Hubei University of Arts and Science
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Abstract

The invention discloses a preparation method of a domestic sewage treatment agent. Through treatment on a plurality of biological raw materials and then mixing of the biological raw materials and other auxiliary agents, the domestic sewage treatment agent is prepared. The preparation method can be operated simply. The domestic sewage treatment agent has a low cost and good effects and is suitable for large scale production. The domestic sewage treatment agent has a domestic sewage suspension removal ratio of 95% or more, a BOD removal ratio of 90% or more and a COD removal ratio of 90% or more.

Description

The preparation method of one way of life drainge treating agent
Technical field
The present invention relates to living drainage processing technology field, particularly relate to the preparation method of one way of life drainge treating agent.
Background technology
The sewage produced during human lives, is one of the primary pollution source of water body.Mainly feces and wash water.Containing large amount of organic in sanitary sewage, such as cellulose, starch, saccharide and fat protein etc.;The most often contain pathogen, virus and parasitic ovum;The chloride of inorganic salts, sulfate, phosphate, bicarbonate and sodium, potassium, calcium, magnesium etc..Total feature is nitrogenous, sulfur-bearing and phosphorous height, under anaerobic bacteria effect, easily gives birth to odorant.Existing sanitary sewage disposal material has, bodied ferric sulfate, is a kind of inorganic polymer coagulant water-purifying material developed on the basis of aluminium salt and iron salt coagulation Hydrolytic Mechanism.According to Synergistic principle, add the new and effective coagulant of one that fe ion or ferric oxide are composited with other iron containing compounds.Aluminum sulfate, not easy-weathering and lose water of crystallization, more stable, heating can dehydration, high temperature can be decomposed into aluminium oxide and sulfur oxide.Aluminium hydroxide is generated after hydrolysis.Aqueous solution seethes with excitement for a long time and can generate basic aluminium sulphate.Industrial goods are canescence lamellar, granular or block, because of the band light green containing low iron salt, make surface turn to be yellow because low price iron salt is oxidized again.Crude product is canescence aplitic texture cellular thing.Nontoxic, dust can stimulate eyes.Aluminium polychlorid, sewage disposal aluminium polychlorid special increase temperature extends the response time, make whole Molecularly Imprinted Polymer structure the hugest, crane span structure distribution is the most reasonable, so that having higher absorption affinity and cohesiveness, being the first-selection of medicament used by Industrial Wastewater Treatment, it can decline to a great extent cost of water treatment.Polyacrylamide, on the premise of reaching equal water quality, polyacrylamide as flocculation aid and other flocculant (the most inorganic or organic coagulants) with the use of, the usage amount of flocculant can be substantially reduced.Improve water quality.In the processing procedure of drinking water treatment and industrial wastewater, polyacrylamide uses with inorganic coagulant, can obviously improve effluent quality.These inorganic agents, can only Cucumber in single treatment sewage owing to using monistic chemical substance, it is difficult to reach the purpose of integrated treatment, it is also difficult to remove the float in sanitary sewage, BOD and COD simultaneously.
Summary of the invention
The purpose of the present invention is aiming at the defect of above-mentioned existence and provides the preparation method of one way of life drainge treating agent.Multiple biological raw material is prepared as living drainage inorganic agent, effective, low cost, it is suitable for large-scale production.
1. the present invention provides the preparation method of one way of life drainge treating agent, and step is as follows:
(1) being uniformly mixed with water by multiple biological raw material, every 1g biological raw material mixing 5g water, filter after stirring 20-30 minute under 100-200rpm, filter screen is 80-100 mesh;
(2) filtrate in step (1) being added concentration is the hydrochloric acid of 10%, and regulation pH is 2-4, is simultaneously introduced potassium permanganate solid, and the addition quality of potassium permanganate solid accounts for after addition the 3% of always solution quality.Stir 20-30 minute under the conditions of 100-200rpm, be centrifuged 10 minutes under 3000rpm;
(3) by the solid matter being centrifugally separating to obtain in step (2) and silicon dioxide, calcium hypochlorite, calcium carbonate, enter granulator granulation after the mixing of sodium acetate, polyacrylamide, acrylamide, EDTA, bentonite;The solid matter being centrifugally separating to obtain in every 80-90g step (2) mixes with 10-15g silicon dioxide, 10-20g calcium hypochlorite, 5-10g calcium carbonate, 5-10g sodium acetate, 10-20g polyacrylamide, 10-20g acrylamide, 5-10gEDTA, 10-15g bentonite.
The most kinds of biological raw materials include rice meal, beef powder, Semen phaseoli radiati powder, flour, tapioca flour, dry scallop powder, peanut powder.Multiple biological raw material proportioning is: every 10g rice meal, and with beef powder 3g, Semen phaseoli radiati powder 10g, flour 10g, tapioca flour 5g, dry scallop powder 8g, peanut powder 10g mix.
The invention have the benefit that the present invention is by mixing with other auxiliary agents after being processed by multiple biological raw material again, prepare living drainage inorganic agent, living drainage inorganic agent low cost simple to operate, that prepare, the effect flocculating the impurity in waste water is notable.Living drainage inorganic agent prepared by the inventive method, after process, living drainage removal efficiency reaches more than 95%, and BOD clearance is more than 90%, and COD clearance is more than 90%.
Detailed description of the invention:
In order to be more fully understood that the present invention, describe technical scheme in detail with instantiation below, but the invention is not limited in this.
Embodiment 1
1. the present invention provides the preparation method of one way of life drainge treating agent, and step is as follows:
(1) being uniformly mixed with water by multiple biological raw material, every 1g biological raw material mixing 5g water, stirring was filtered after 20 minutes at 100 rpm, and filter screen is 80 mesh;
(2) filtrate in step (1) being added concentration is the hydrochloric acid of 10%, and regulation pH is 2, is simultaneously introduced potassium permanganate solid, and the additions quality of potassium permanganate solid accounts for after addition the 3% of always solution quality.Stirring 20 minutes at 100 rpm, are centrifuged 10 minutes under 3000rpm;
(3) by the solid matter being centrifugally separating to obtain in step (2) and silicon dioxide, calcium hypochlorite, calcium carbonate, enter granulator granulation after the mixing of sodium acetate, polyacrylamide, acrylamide, EDTA, bentonite;The solid matter being centrifugally separating to obtain in every 80g step (2) mixes with 10g silicon dioxide, 10g calcium hypochlorite, 5g calcium carbonate, 5g sodium acetate, 10g polyacrylamide, 10g acrylamide, 5gEDTA, 10g bentonite.
The most kinds of biological raw materials include rice meal, beef powder, Semen phaseoli radiati powder, flour, tapioca flour, dry scallop powder, peanut powder.Multiple biological raw material proportioning is: every 10g rice meal, and with beef powder 3g, Semen phaseoli radiati powder 10g, flour 10g, tapioca flour 5g, dry scallop powder 8g, peanut powder 10g mix.
Living drainage inorganic agent prepared by the inventive method, after process, living drainage removal efficiency reaches 95%, and BOD clearance is 90%, and COD clearance is 90%.
Embodiment 2
1. the present invention provides the preparation method of one way of life drainge treating agent, and step is as follows:
(1) being uniformly mixed with water by multiple biological raw material, every 1g biological raw material mixing 5g water, filter after stirring 25 minutes under 150rpm, filter screen is 90 mesh;
(2) filtrate in step (1) being added concentration is the hydrochloric acid of 10%, and regulation pH is 3, is simultaneously introduced potassium permanganate solid, and the additions quality of potassium permanganate solid accounts for after addition the 3% of always solution quality.Stir 25 minutes under the conditions of 150rpm, be centrifuged 10 minutes under 3000rpm;
(3) by the solid matter being centrifugally separating to obtain in step (2) and silicon dioxide, calcium hypochlorite, calcium carbonate, enter granulator granulation after the mixing of sodium acetate, polyacrylamide, acrylamide, EDTA, bentonite;The solid matter being centrifugally separating to obtain in every 85g step (2) mixes with 12g silicon dioxide, 15g calcium hypochlorite, 8g calcium carbonate, 8g sodium acetate, 15g polyacrylamide, 15g acrylamide, 8gEDTA, 12g bentonite.
The most kinds of biological raw materials include rice meal, beef powder, Semen phaseoli radiati powder, flour, tapioca flour, dry scallop powder, peanut powder.Multiple biological raw material proportioning is: every 10g rice meal, and with beef powder 3g, Semen phaseoli radiati powder 10g, flour 10g, tapioca flour 5g, dry scallop powder 8g, peanut powder 10g mix.
Living drainage inorganic agent prepared by the inventive method, after process, living drainage removal efficiency reaches 96%, and BOD clearance is 91%, and COD clearance is 91%.
Embodiment 3
1. the present invention provides the preparation method of one way of life drainge treating agent, and step is as follows:
(1) being uniformly mixed with water by multiple biological raw material, every 1g biological raw material mixing 5g water, stirring was filtered after 30 minutes at 200 rpm, and filter screen is 100 mesh;
(2) filtrate in step (1) being added concentration is the hydrochloric acid of 10%, and regulation pH is 4, is simultaneously introduced potassium permanganate solid, and the additions quality of potassium permanganate solid accounts for after addition the 3% of always solution quality.Stir 30 minutes under the conditions of 200rpm, be centrifuged 10 minutes under 3000rpm;
(3) by the solid matter being centrifugally separating to obtain in step (2) and silicon dioxide, calcium hypochlorite, calcium carbonate, enter granulator granulation after the mixing of sodium acetate, polyacrylamide, acrylamide, EDTA, bentonite;The solid matter being centrifugally separating to obtain in every 90g step (2) mixes with 15g silicon dioxide, 20g calcium hypochlorite, 10g calcium carbonate, 10g sodium acetate, 20g polyacrylamide, 20g acrylamide, 10gEDTA, 15g bentonite.
The most kinds of biological raw materials include rice meal, beef powder, Semen phaseoli radiati powder, flour, tapioca flour, dry scallop powder, peanut powder.Multiple biological raw material proportioning is: every 10g rice meal, and with beef powder 3g, Semen phaseoli radiati powder 10g, flour 10g, tapioca flour 5g, dry scallop powder 8g, peanut powder 10g mix.
Living drainage inorganic agent prepared by the inventive method, after process, living drainage removal efficiency reaches 97%, and BOD clearance is 92%, and COD clearance is 92%.

Claims (5)

1. the preparation method of one way of life drainge treating agent, step is as follows:
(1) multiple biological raw material is uniformly mixed with water, every 1g biological raw material mixing 5g water, filters;
(2) filtrate in step (1) being added concentration is the hydrochloric acid of 10%, and regulation pH is 2-4, is simultaneously introduced potassium permanganate solid, after stirring, centrifugation;
(3) granulator granulation is entered with silicon dioxide, calcium hypochlorite, calcium carbonate, sodium acetate, polyacrylamide, acrylamide, EDTA, bentonite after being mixed by the solid matter being centrifugally separating to obtain in step (2);The solid matter being centrifugally separating to obtain in every 80-90g step (2) mixes with 10-15g silicon dioxide, 10-20g calcium hypochlorite, 5-10g calcium carbonate, 5-10g sodium acetate, 10-20g polyacrylamide, 10-20g acrylamide, 5-10gEDTA, 10-15g bentonite.
The preparation method of one way of life drainge treating agent the most according to claim 1, it is characterised in that in step (1), mixing speed is 100-200rpm, and mixing time is 20-30 minute, and the filter screen filtered is 80-100 mesh.
The preparation method of one way of life drainge treating agent the most according to claim 1, it is characterised in that add after potassium permanganate quality accounts for addition the 3% of total solution quality in step (2).
The preparation method of one way of life drainge treating agent the most according to claim 1, it is characterised in that in step (2), mixing speed is 100-200rpm, mixing time is 20-30 minute, and centrifugal speed is 3000rpm, 10 minutes.
The preparation method of one way of life drainge treating agent the most according to claim 1, it is characterised in that multiple biological raw material includes rice meal, beef powder, Semen phaseoli radiati powder, flour, tapioca flour, dry scallop powder, peanut powder, multiple biological raw material proportioning is: every 10g rice meal, with beef powder 3g, Semen phaseoli radiati powder 10g, flour 10g, tapioca flour 5g, dry scallop powder 8g, peanut powder 10g mix.
CN201510667943.4A 2015-10-16 2015-10-16 A kind of preparation method of living drainage inorganic agent Active CN105906006B (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110540277A (en) * 2019-02-27 2019-12-06 湖北文理学院 Preparation method of domestic wastewater treatment agent
CN110563111A (en) * 2019-02-27 2019-12-13 湖北文理学院 preparation method of industrial wastewater composite treating agent

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101585571A (en) * 2009-06-25 2009-11-25 哈尔滨工业大学 Method for treating wastewater through compounding modified starch flocculant and tourmaline
CN102659229A (en) * 2012-06-08 2012-09-12 蒋涛 Environment-friendly composite flocculant
CN102701348A (en) * 2012-06-12 2012-10-03 徐梁冰 Preparation method for environment-friendly composite flocculant
CN103663652A (en) * 2013-12-11 2014-03-26 山东华亚环保科技有限公司 Preparation method of sewage treatment agent

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101585571A (en) * 2009-06-25 2009-11-25 哈尔滨工业大学 Method for treating wastewater through compounding modified starch flocculant and tourmaline
CN102659229A (en) * 2012-06-08 2012-09-12 蒋涛 Environment-friendly composite flocculant
CN102701348A (en) * 2012-06-12 2012-10-03 徐梁冰 Preparation method for environment-friendly composite flocculant
CN103663652A (en) * 2013-12-11 2014-03-26 山东华亚环保科技有限公司 Preparation method of sewage treatment agent

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110540277A (en) * 2019-02-27 2019-12-06 湖北文理学院 Preparation method of domestic wastewater treatment agent
CN110563111A (en) * 2019-02-27 2019-12-13 湖北文理学院 preparation method of industrial wastewater composite treating agent

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Effective date of registration: 20191030

Address after: No.1, upper side of Jiuqu bridge, Mazhou group, Beiyong village, Daojiao Town, Dongguan City, Guangdong Province

Patentee after: Dongguan Lanshen environmental protection Co., Ltd

Address before: Research at the 441053 Xiangfan city of Hubei province Xiangcheng District Long Road No. 296 Hubei liberal arts college

Patentee before: Hubei University of Arts and Science