CN108715508A - A kind of pig farm excrement object inorganic agent and preparation method thereof - Google Patents
A kind of pig farm excrement object inorganic agent and preparation method thereof Download PDFInfo
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- CN108715508A CN108715508A CN201810697653.8A CN201810697653A CN108715508A CN 108715508 A CN108715508 A CN 108715508A CN 201810697653 A CN201810697653 A CN 201810697653A CN 108715508 A CN108715508 A CN 108715508A
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F11/00—Treatment of sludge; Devices therefor
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/28—Treatment of water, waste water, or sewage by sorption
- C02F1/281—Treatment of water, waste water, or sewage by sorption using inorganic sorbents
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/50—Treatment of water, waste water, or sewage by addition or application of a germicide or by oligodynamic treatment
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/52—Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities
- C02F1/5236—Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities using inorganic agents
- C02F1/5245—Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities using inorganic agents using basic salts, e.g. of aluminium and iron
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/52—Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities
- C02F1/54—Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities using organic material
- C02F1/56—Macromolecular compounds
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/72—Treatment of water, waste water, or sewage by oxidation
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F11/00—Treatment of sludge; Devices therefor
- C02F11/06—Treatment of sludge; Devices therefor by oxidation
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F11/00—Treatment of sludge; Devices therefor
- C02F11/12—Treatment of sludge; Devices therefor by de-watering, drying or thickening
- C02F11/14—Treatment of sludge; Devices therefor by de-watering, drying or thickening with addition of chemical agents
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F2103/00—Nature of the water, waste water, sewage or sludge to be treated
- C02F2103/20—Nature of the water, waste water, sewage or sludge to be treated from animal husbandry
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F2303/00—Specific treatment goals
- C02F2303/02—Odour removal or prevention of malodour
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F2303/00—Specific treatment goals
- C02F2303/04—Disinfection
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F2305/00—Use of specific compounds during water treatment
- C02F2305/04—Surfactants, used as part of a formulation or alone
Abstract
The invention discloses a kind of pig farm excrement object inorganic agents and preparation method thereof, which be formulated by the raw material of following weight：2-8 parts of ammonium persulfate, 3-15 parts of bodied ferric sulfate, 0.5-3 parts of sodium hydrogensulfite, 5-20 parts of polyaluminium sulfate, 0.3-1.8 parts of sodium acetate, 2-6 parts of laminated crystal of sodium disilicate, 1-3.5 parts of neopelex, 1.5-5.5 parts of polyacrylamide, 2-6 parts of antimony trichloride, 1-5 parts of atlapulgite, 0.5-3 parts of high polymer composite synergistic activator, 45-95 parts of deionized water.Pig farm excrement object inorganic agent produced by the present invention can effectively kill the harmful substances such as germ, worm's ovum in swine manure, and can quickly and efficiently remove the stink in swine manure, and effectively can carry out purified treatment to pig farm fecaluria waste water.
Description
Technical field
The invention belongs to technical field of pig cultivation, and in particular to a kind of pig farm excrement object inorganic agent and preparation method thereof.
Background technology
Swine manure is a kind of environmental hazard substance, and is that one kind can be using living resources, can if realizing harmless treatment
The effect for largely playing the resources such as swine manure biomass energy, waste nutrition, realizes the recycling of waste resource.
The stink that swine manure distributes can pollute air, and pig farm fecaluria can go deep into soil, and then can be polluted to soil, and deeply
The pig farm fecaluria of soil flows into river meeting polluted source with underground water or surface water, and contains germ and worm in swine manure
Ovum, therefore untreated swine manure cannot be directly as the fertilizer of crops.
It to pig farm excrement substance treating method is handled by mechanical filter in the prior art, liquid dung is detached, processing routine is multiple
Miscellaneous, efficiency is low, and processing cost is high, and requires the healthy prevention in processing procedure also high.
Invention content
A kind of pig farm excrement object inorganic agent of present invention offer and preparation method thereof, pig farm excrement object inorganic agent obtained can have
Effect kills the harmful substances such as germ, the worm's ovum in swine manure, and can quickly and efficiently remove the stink in swine manure, and
Can purified treatment effectively be carried out to pig farm fecaluria waste water.
In order to solve the above-mentioned technical problem, the present invention adopts the following technical scheme that：
A kind of pig farm excrement object inorganic agent, it is formulated by the raw material of following weight：2-8 parts of ammonium persulfate gathers
Close 3-15 parts of ferric sulfate, 0.5-3 parts of sodium hydrogensulfite, 5-20 parts of polyaluminium sulfate, 0.3-1.8 parts of sodium acetate, laminated crystalline two
2-6 parts of sodium metasilicate, 1-3.5 parts of neopelex, 1.5-5.5 parts of polyacrylamide, 2-6 parts of antimony trichloride, activity are white
1-5 parts native, 0.5-3 parts of high polymer composite synergistic activator, 45-95 parts of deionized water.
Further, the weight of each raw material is：2 parts of ammonium persulfate, 3 parts of bodied ferric sulfate, sodium hydrogensulfite 0.5
Part, 5 parts of polyaluminium sulfate, 0.3 part of sodium acetate, 2 parts of laminated crystal of sodium disilicate, 1 part of neopelex, polyacrylamide
1.5 parts of amine, 2 parts of antimony trichloride, 1 part of atlapulgite, 0.5 part of high polymer composite synergistic activator, 45 parts of deionized water.
Further, the weight of each raw material is：5 parts of ammonium persulfate, 9 parts of bodied ferric sulfate, sodium hydrogensulfite 1.7
Part, 12 parts of polyaluminium sulfate, 1.1 parts of sodium acetate, 4 parts of laminated crystal of sodium disilicate, 2.2 parts of neopelex, poly- third
3.5 parts of acrylamide, 4 parts of antimony trichloride, 3 parts of atlapulgite, 1.8 parts of high polymer composite synergistic activator, 70 parts of deionized water.
Further, the weight of each raw material is：8 parts of ammonium persulfate, 15 parts of bodied ferric sulfate, sodium hydrogensulfite 3
Part, 20 parts of polyaluminium sulfate, 1.8 parts of sodium acetate, 6 parts of laminated crystal of sodium disilicate, 3.5 parts of neopelex, poly- third
5.5 parts of acrylamide, 6 parts of antimony trichloride, 5 parts of atlapulgite, 3 parts of high polymer composite synergistic activator, 95 parts of deionized water.
The preparation method of pig farm excrement object inorganic agent, includes the following steps：
（1）It is weighed respectively by the proportional quantity except polyaluminium sulfate, laminated crystal of sodium disilicate, atlapulgite and macromolecule are compound
Various raw materials other than synergistic activator, and the various raw materials claimed are contained in respectively in corresponding container, then respectively to Sheng
Add deionized water in the container of the corresponding raw material of dress and dissolve by heating, and stir evenly, and then the water-soluble of corresponding raw material is respectively prepared
Liquid, i.e. ammonium persulfate aqueous solution, polyaluminum sulfate water solution, aqueous solution of sodium bisulfite, aqueous sodium acetate solution, detergent alkylate
Sulfonic acid sodium water solution, polyacrylamide solution, antimony trichloride aqueous solution, wherein into the container for containing corresponding raw material plus go from
It is degree that the amount of sub- water is all dissolved into solution state with corresponding raw material, and the corresponding dissolving heating temperature range of each raw material is distinguished
For：30-40 DEG C of ammonium persulfate, 25-35 DEG C of bodied ferric sulfate, 80-100 DEG C of sodium hydrogensulfite, 25-35 DEG C of sodium acetate, dodecane
80-90 DEG C of base benzene sulfonic acid sodium salt, 30-40 DEG C of polyacrylamide, 75-80 DEG C of antimony trichloride；
（2）By step（1）In ammonium persulfate aqueous solution obtained, polyaluminum sulfate water solution, aqueous solution of sodium bisulfite, second
Acid sodium aqueous solution, sodium dodecyl benzene sulfonate aqueous solution, polyacrylamide solution, antimony trichloride aqueous solution are stirred
It is even, first material is obtained, weighs polyaluminium sulfate by the proportioning, and the polyaluminium sulfate claimed is added in first material simultaneously
It is uniformly mixed, obtains second material, then by the stratiform knot for matching and weighing laminated crystal of sodium disilicate and claiming
Brilliant sodium disilicate grind into powder, and the laminated crystal of sodium disilicate being ground into powder is added in second material and is stirred mixed
It closes uniformly, obtains third material, then atlapulgite is weighed by the proportioning, and the atlapulgite claimed is added in third material
And be uniformly mixed, obtain 4 materials, then high polymer composite synergistic activator is weighed by the proportioning, and by the high score of title
Sub- composite synergistic activator is added in 4 materials and is uniformly mixed, and obtains the 5th material, finally adds by the proportional quantity
Sufficient deionized water, and be uniformly mixed, obtain pig farm excrement object inorganic agent.
Compared with the existing technology, beneficial effects of the present invention are：
The function of each raw material used in excrement object inorganic agent in pig farm produced by the present invention is respectively：
Ammonium persulfate：With strong oxidizing property, it can be hydrolyzed into ammonium hydrogen sulfate and hydrogen peroxide in aqueous solution, be used as oxidant, drift
White agent, disinfectant etc.；
Bodied ferric sulfate：It is a kind of inorganic polymer coagulant of superior performance, be widely used in drinking water, industrial water,
The purified treatment of various industrial wastewaters, municipal sewage, sludge dewatering etc., turbidity removal, de-oiling, degerming, deodorization, remove algae, removal at decoloration
COD, BOD and heavy metal ion and other effects are notable in water；
Sodium hydrogensulfite：Its aqueous solution is used for the bleaching of cotton fabric, in dyestuff, papermaking, process hides, chemical synthesis etc. in acidity
It is used as reducing agent in industry, also acts as preservative, antioxidant etc.；
Polyaluminium sulfate：It is composite polymer polymer, and molecular structure is huge, and adsorption capacity is strong, and purifying water effect is better than institute
There is traditional inorganic water purification agent, it is big to be put into the floccule body formed after raw water, and settling velocity is fast, activity is high, filterability is good, and
It is adaptable to various raw waters, minimum on the influence of the pH value of water, no matter raw water turbidity height, Wastewater Pollutant concentration are big
Small, its clean-up effect is all very notable, and it is small to the corrosivity of equipment；
Sodium acetate：Its aqueous solution can be used as buffer, PH conditioning agents etc. in alkalinity；
Laminated crystal of sodium disilicate：Its softening outlet capacity is strong, its exchange capacity with calcium and magnesium ion reaches 300mg CaCO3/
G and 400mg MgCO3/g or more, and very thoroughly, quickly to the softening of water, its alkaline buffer ability is strong, and active ingredient is high,
With higher active alkalinity, PH buffer capacities are strong, to being impregnated with of greasy dirt, emulsify and dispersion performance is excellent, and with independent
Dirt-removing power has good suspension to dirt, and deflocculation, antiredeposition ability are strong；
Neopelex：Alkali, diluted acid, hard water chemical property are stablized, are anion surfactants, is had good
Surface-active, hydrophily is stronger, can effectively reduce the tension of oil-water interface, reaches emulsion dispersion effect；
Polyacrylamide：It is macromolecule organic synthesis flocculant, its amide groups can, absorption affine with many substances and formed
Hydrogen bond, high molecular weight polyacrylamide form " bridging " between the particle adsorbed, generate floc sedimentation, are conducive to particle sinking, gather
Acrylamide flocculating agent adapts to a variety of flocculation phenomenons, and dosage is small, efficient, and the body refuse of generation is few, and easy post-processing can
Chemistry in water treatment medicament as industries such as original sub-block, municipal sewage treatment and Industrial Wastewater Treatments；
Antimony trichloride：It can be used as catalyst；
Atlapulgite：Its absorption property is very strong, can adsorb coloring matter, organic substance, has good absorption odor function,
It can be used as catalyst, adsorbent, flocculant for treating waste water etc.；
High polymer composite synergistic activator：It is formulated by a variety of polymer substances, containing surfactant emulsifies object, can be reduced
The surface tension of liquid changes the property of boundary material, and immiscible substance can be prevented mutually exclusive, has in wet treatment molten
The effects that solution, wetting, infiltration, diffusion, emulsification, washing, and there is good compounding capacity, and also it is stable and reliable for performance, and
The pH value of solution can be adjusted；
Deionized water：It is bordering on pure water obtained from being the impurity in ionized state removed as ion exchange resin in water.
Pig farm excrement object inorganic agent has been made using above-mentioned each raw material in the present invention, and above-mentioned each raw material can make each original after combining
The effect of material, generates synergistic effect, and then can effectively kill the harmful substances such as germ, worm's ovum in swine manure, and can be quickly high
Stink in effect ground removal swine manure, and can purified treatment effectively be carried out to pig farm fecaluria waste water；In raw material of the present invention
Ammonium persulfate have strong oxidizing property, ammonium hydrogen sulfate and hydrogen peroxide, ammonium persulfate energy and pig farm can be hydrolyzed into aqueous solution
Redox reaction occurs for the hydrogen sulfide gas in excrement object, and then removes hydrogen sulfide gas, the stink of removal of hydrogen sulfide gas, and
Ammonium persulfate can kill the harmful substances such as germ, the worm's ovum in swine manure as disinfectant；Polymerised sulphur in raw material of the present invention
Sour iron is a kind of inorganic polymer coagulant of superior performance, can effectively to pig farm fecaluria waste water carry out purified treatment, turbidity removal,
Decoloration, de-oiling, degerming, deodorization, except algae, remove in water removal COD, BOD and other effects significantly；Polyaluminium sulfate in raw material of the present invention is
Composite polymer polymer, molecular structure is huge, and adsorption capacity is strong, is put into the floccule body formed after the fecaluria waste water of pig farm
Greatly, the settling velocity of the floccule body formed in this way is fast, activity is high, filterability is good, and it is to the adaptable of pig farm fecaluria waste water,
It is minimum on the influence of the pH value of pig farm fecaluria waste water, no matter the pollutant of the turbidity height of pig farm fecaluria waste water, pig farm fecaluria waste water
Concentration, its clean-up effect is all very notable, and it is small to the corrosivity of equipment；Sodium acetate in raw material of the present invention is used as slow
Electuary and PH conditioning agents；Neopelex in raw material of the present invention stablizes alkali, diluted acid, hard water chemical property, is cloudy
Ionic surface active agent has good surface-active, and hydrophily is stronger, can effectively reduce the tension of oil-water interface, reaches breast
Change peptizaiton；Polyacrylamide in raw material of the present invention is macromolecule organic synthesis flocculant, its amide groups can be with many
Substance is affine, adsorbs and forms hydrogen bond, and high molecular weight polyacrylamide forms " bridging " between the particle adsorbed, generates wadding
Group is conducive to particle sinking in this way, and polyacrylamide flocculant adapts to a variety of flocculation phenomenons, and dosage is small, efficient, generates
Body refuse it is few, easy post-processing can carry out to pig farm fecaluria waste water high-efficiency and rapidly purified treatment；Three in raw material of the present invention
Antimony chloride is used as catalyst；The absorption property of atlapulgite in raw material of the present invention is very strong, can adsorb coloring matter, organic matter
Matter has good absorption odor function, and then can remove the peculiar smell of pig farm excrement object, and as catalyst, adsorbent, pig farm excrement
Urinate flocculant for treating waste water；High polymer composite synergistic activator in raw material of the present invention is formulated by a variety of polymer substances,
Containing surfactant emulsifies object, the surface tension of pig farm excrement object inorganic agent can be reduced, changes the property of boundary material, in turn
Immiscible substance can be prevented mutually exclusive, have when handling pig farm excrement object dissolving, wetting, infiltration, diffusion, emulsification,
The effects that washing, and there is good compounding capacity, and also it is stable and reliable for performance, and pig farm excrement object inorganic agent can be adjusted
PH value；The present invention prepares pig farm excrement object inorganic agent using deionized water, can effectively avoid in this way calcium in tap water from
Son, magnesium ion etc. enter in the excrement object inorganic agent of pig farm, can thus neopelex be made farthest to play it
Effect；Laminated crystal of sodium disilicate in raw material of the present invention has independent dirt-removing power, has good suspension to dirt,
Deflocculation, antiredeposition ability are strong.
The use of excrement object inorganic agent in pig farm produced by the present invention：Directly by the pig farm excrement object inorganic agent according to excrement per ton
Water is spread with 5 ~ 7% ratio and is scattered in liquid dung collecting pit, by the chemical reaction of pig farm the excrement object inorganic agent and excrement object, can be incited somebody to action
Fecaluria is sterilized, is flocculated, is precipitated, and is then detached, and excrement slag uses after being collected directly as fertilizer after precipitation, not to soil
It pollutes, the urine water after separation is also used as a kind of Liquid Fertilizer, and for pouring kind of a plant after collection, disease is not also caused to kind of a plant
Evil.
Specific implementation mode
Embodiment 1
A kind of pig farm excrement object inorganic agent, it is formulated by the raw material of following weight：2 parts of ammonium persulfate, polymerization
3 parts of ferric sulfate, 0.5 part of sodium hydrogensulfite, 5 parts of polyaluminium sulfate, 0.3 part of sodium acetate, 2 parts of laminated crystal of sodium disilicate, 12
1 part of sodium alkyl benzene sulfonate, 1.5 parts of polyacrylamide, 2 parts of antimony trichloride, 1 part of atlapulgite, high polymer composite synergistic activator
0.5 part, 45 parts of deionized water.
The preparation method of pig farm excrement object inorganic agent, includes the following steps：
（1）It is weighed respectively by the proportional quantity except polyaluminium sulfate, laminated crystal of sodium disilicate, atlapulgite and macromolecule are compound
Various raw materials other than synergistic activator, and the various raw materials claimed are contained in respectively in corresponding container, then respectively to Sheng
Add deionized water in the container of the corresponding raw material of dress and dissolve by heating, and stir evenly, and then the water-soluble of corresponding raw material is respectively prepared
Liquid, i.e. ammonium persulfate aqueous solution, polyaluminum sulfate water solution, aqueous solution of sodium bisulfite, aqueous sodium acetate solution, detergent alkylate
Sulfonic acid sodium water solution, polyacrylamide solution, antimony trichloride aqueous solution, wherein into the container for containing corresponding raw material plus go from
It is degree that the amount of sub- water is all dissolved into solution state with corresponding raw material, and the corresponding dissolving heating temperature range of each raw material is distinguished
For：30 DEG C of ammonium persulfate, 25 DEG C of bodied ferric sulfate, 80 DEG C of sodium hydrogensulfite, 25 DEG C of sodium acetate, neopelex 80
DEG C, 30 DEG C of polyacrylamide, 75 DEG C of antimony trichloride；
（2）By step（1）In ammonium persulfate aqueous solution obtained, polyaluminum sulfate water solution, aqueous solution of sodium bisulfite, second
Acid sodium aqueous solution, sodium dodecyl benzene sulfonate aqueous solution, polyacrylamide solution, antimony trichloride aqueous solution are stirred
It is even, first material is obtained, weighs polyaluminium sulfate by the proportioning, and the polyaluminium sulfate claimed is added in first material simultaneously
It is uniformly mixed, obtains second material, then by the stratiform knot for matching and weighing laminated crystal of sodium disilicate and claiming
Brilliant sodium disilicate grind into powder, and the laminated crystal of sodium disilicate being ground into powder is added in second material and is stirred mixed
It closes uniformly, obtains third material, then atlapulgite is weighed by the proportioning, and the atlapulgite claimed is added in third material
And be uniformly mixed, obtain 4 materials, then high polymer composite synergistic activator is weighed by the proportioning, and by the high score of title
Sub- composite synergistic activator is added in 4 materials and is uniformly mixed, and obtains the 5th material, finally adds by the proportional quantity
Sufficient deionized water, and be uniformly mixed, obtain pig farm excrement object inorganic agent.
Embodiment 2
A kind of pig farm excrement object inorganic agent, it is formulated by the raw material of following weight：5 parts of ammonium persulfate, polymerization
9 parts of ferric sulfate, 1.7 parts of sodium hydrogensulfite, 12 parts of polyaluminium sulfate, 1.1 parts of sodium acetate, 4 parts of laminated crystal of sodium disilicate, 12
2.2 parts of sodium alkyl benzene sulfonate, 3.5 parts of polyacrylamide, 4 parts of antimony trichloride, 3 parts of atlapulgite, high polymer composite synergistic activity
1.8 parts of agent, 70 parts of deionized water.
The preparation method of pig farm excrement object inorganic agent, includes the following steps：
（1）It is weighed respectively by the proportional quantity except polyaluminium sulfate, laminated crystal of sodium disilicate, atlapulgite and macromolecule are compound
Various raw materials other than synergistic activator, and the various raw materials claimed are contained in respectively in corresponding container, then respectively to Sheng
Add deionized water in the container of the corresponding raw material of dress and dissolve by heating, and stir evenly, and then the water-soluble of corresponding raw material is respectively prepared
Liquid, i.e. ammonium persulfate aqueous solution, polyaluminum sulfate water solution, aqueous solution of sodium bisulfite, aqueous sodium acetate solution, detergent alkylate
Sulfonic acid sodium water solution, polyacrylamide solution, antimony trichloride aqueous solution, wherein into the container for containing corresponding raw material plus go from
It is degree that the amount of sub- water is all dissolved into solution state with corresponding raw material, and the corresponding dissolving heating temperature range of each raw material is distinguished
For：35 DEG C of ammonium persulfate, 30 DEG C of bodied ferric sulfate, 90 DEG C of sodium hydrogensulfite, 30 DEG C of sodium acetate, neopelex 85
DEG C, 35 DEG C of polyacrylamide, 77 DEG C of antimony trichloride；
（2）By step（1）In ammonium persulfate aqueous solution obtained, polyaluminum sulfate water solution, aqueous solution of sodium bisulfite, second
Acid sodium aqueous solution, sodium dodecyl benzene sulfonate aqueous solution, polyacrylamide solution, antimony trichloride aqueous solution are stirred
It is even, first material is obtained, weighs polyaluminium sulfate by the proportioning, and the polyaluminium sulfate claimed is added in first material simultaneously
It is uniformly mixed, obtains second material, then by the stratiform knot for matching and weighing laminated crystal of sodium disilicate and claiming
Brilliant sodium disilicate grind into powder, and the laminated crystal of sodium disilicate being ground into powder is added in second material and is stirred mixed
It closes uniformly, obtains third material, then atlapulgite is weighed by the proportioning, and the atlapulgite claimed is added in third material
And be uniformly mixed, obtain 4 materials, then high polymer composite synergistic activator is weighed by the proportioning, and by the high score of title
Sub- composite synergistic activator is added in 4 materials and is uniformly mixed, and obtains the 5th material, finally adds by the proportional quantity
Sufficient deionized water, and be uniformly mixed, obtain pig farm excrement object inorganic agent.
Embodiment 3
A kind of pig farm excrement object inorganic agent, it is formulated by the raw material of following weight：8 parts of ammonium persulfate, polymerization
15 parts of ferric sulfate, 3 parts of sodium hydrogensulfite, 20 parts of polyaluminium sulfate, 1.8 parts of sodium acetate, 6 parts of laminated crystal of sodium disilicate, 12
3.5 parts of sodium alkyl benzene sulfonate, 5.5 parts of polyacrylamide, 6 parts of antimony trichloride, 5 parts of atlapulgite, high polymer composite synergistic activity
3 parts of agent, 95 parts of deionized water.
The preparation method of pig farm excrement object inorganic agent, includes the following steps：
（1）It is weighed respectively by the proportional quantity except polyaluminium sulfate, laminated crystal of sodium disilicate, atlapulgite and macromolecule are compound
Various raw materials other than synergistic activator, and the various raw materials claimed are contained in respectively in corresponding container, then respectively to Sheng
Add deionized water in the container of the corresponding raw material of dress and dissolve by heating, and stir evenly, and then the water-soluble of corresponding raw material is respectively prepared
Liquid, i.e. ammonium persulfate aqueous solution, polyaluminum sulfate water solution, aqueous solution of sodium bisulfite, aqueous sodium acetate solution, detergent alkylate
Sulfonic acid sodium water solution, polyacrylamide solution, antimony trichloride aqueous solution, wherein into the container for containing corresponding raw material plus go from
It is degree that the amount of sub- water is all dissolved into solution state with corresponding raw material, and the corresponding dissolving heating temperature range of each raw material is distinguished
For：40 DEG C of ammonium persulfate, 35 DEG C of bodied ferric sulfate, 100 DEG C of sodium hydrogensulfite, 35 DEG C of sodium acetate, neopelex 90
DEG C, 40 DEG C of polyacrylamide, 80 DEG C of antimony trichloride；
（2）By step（1）In ammonium persulfate aqueous solution obtained, polyaluminum sulfate water solution, aqueous solution of sodium bisulfite, second
Acid sodium aqueous solution, sodium dodecyl benzene sulfonate aqueous solution, polyacrylamide solution, antimony trichloride aqueous solution are stirred
It is even, first material is obtained, weighs polyaluminium sulfate by the proportioning, and the polyaluminium sulfate claimed is added in first material simultaneously
It is uniformly mixed, obtains second material, then by the stratiform knot for matching and weighing laminated crystal of sodium disilicate and claiming
Brilliant sodium disilicate grind into powder, and the laminated crystal of sodium disilicate being ground into powder is added in second material and is stirred mixed
It closes uniformly, obtains third material, then atlapulgite is weighed by the proportioning, and the atlapulgite claimed is added in third material
And be uniformly mixed, obtain 4 materials, then high polymer composite synergistic activator is weighed by the proportioning, and by the high score of title
Sub- composite synergistic activator is added in 4 materials and is uniformly mixed, and obtains the 5th material, finally adds by the proportional quantity
Sufficient deionized water, and be uniformly mixed, obtain pig farm excrement object inorganic agent.
Claims (5)
1. a kind of pig farm excrement object inorganic agent, which is characterized in that it is formulated by the raw material of following weight：Over cure
Sour ammonium 2-8 parts, 3-15 parts of bodied ferric sulfate, 0.5-3 parts of sodium hydrogensulfite, 5-20 parts of polyaluminium sulfate, sodium acetate 0.3-1.8
Part, 2-6 parts of laminated crystal of sodium disilicate, 1-3.5 parts of neopelex, 1.5-5.5 parts of polyacrylamide, antimony trichloride
2-6 parts, 1-5 parts of atlapulgite, 0.5-3 parts of high polymer composite synergistic activator, 45-95 parts of deionized water.
2. excrement object inorganic agent in pig farm according to claim 1, which is characterized in that the weight of each raw material is：It crosses
2 parts of ammonium sulfate, 3 parts of bodied ferric sulfate, 0.5 part of sodium hydrogensulfite, 5 parts of polyaluminium sulfate, 0.3 part of sodium acetate, laminated crystalline two
2 parts of sodium metasilicate, 1 part of neopelex, 1.5 parts of polyacrylamide, 2 parts of antimony trichloride, 1 part of atlapulgite, macromolecule
0.5 part of composite synergistic activator, 45 parts of deionized water.
3. excrement object inorganic agent in pig farm according to claim 1, which is characterized in that the weight of each raw material is：It crosses
5 parts of ammonium sulfate, 9 parts of bodied ferric sulfate, 1.7 parts of sodium hydrogensulfite, 12 parts of polyaluminium sulfate, 1.1 parts of sodium acetate, laminated crystalline two
4 parts of sodium metasilicate, 2.2 parts of neopelex, 3.5 parts of polyacrylamide, 4 parts of antimony trichloride, 3 parts of atlapulgite, high score
1.8 parts of sub- composite synergistic activator, 70 parts of deionized water.
4. excrement object inorganic agent in pig farm according to claim 1, which is characterized in that the weight of each raw material is：It crosses
8 parts of ammonium sulfate, 15 parts of bodied ferric sulfate, 3 parts of sodium hydrogensulfite, 20 parts of polyaluminium sulfate, 1.8 parts of sodium acetate, laminated crystalline two
6 parts of sodium metasilicate, 3.5 parts of neopelex, 5.5 parts of polyacrylamide, 6 parts of antimony trichloride, 5 parts of atlapulgite, high score
3 parts of sub- composite synergistic activator, 95 parts of deionized water.
5. according to the preparation method of claim 1-4 any one of them pig farm excrement object inorganic agent, it is characterised in that including with
Lower step：
（1）It is weighed respectively by the proportional quantity except polyaluminium sulfate, laminated crystal of sodium disilicate, atlapulgite and macromolecule are compound
Various raw materials other than synergistic activator, and the various raw materials claimed are contained in respectively in corresponding container, then respectively to Sheng
Add deionized water in the container of the corresponding raw material of dress and dissolve by heating, and stir evenly, and then the water-soluble of corresponding raw material is respectively prepared
Liquid, i.e. ammonium persulfate aqueous solution, polyaluminum sulfate water solution, aqueous solution of sodium bisulfite, aqueous sodium acetate solution, detergent alkylate
Sulfonic acid sodium water solution, polyacrylamide solution, antimony trichloride aqueous solution, wherein into the container for containing corresponding raw material plus go from
It is degree that the amount of sub- water is all dissolved into solution state with corresponding raw material, and the corresponding dissolving heating temperature range of each raw material is distinguished
For：30-40 DEG C of ammonium persulfate, 25-35 DEG C of bodied ferric sulfate, 80-100 DEG C of sodium hydrogensulfite, 25-35 DEG C of sodium acetate, dodecane
80-90 DEG C of base benzene sulfonic acid sodium salt, 30-40 DEG C of polyacrylamide, 75-80 DEG C of antimony trichloride；
（2）By step（1）In ammonium persulfate aqueous solution obtained, polyaluminum sulfate water solution, aqueous solution of sodium bisulfite, second
Acid sodium aqueous solution, sodium dodecyl benzene sulfonate aqueous solution, polyacrylamide solution, antimony trichloride aqueous solution are stirred
It is even, first material is obtained, weighs polyaluminium sulfate by the proportioning, and the polyaluminium sulfate claimed is added in first material simultaneously
It is uniformly mixed, obtains second material, then by the stratiform knot for matching and weighing laminated crystal of sodium disilicate and claiming
Brilliant sodium disilicate grind into powder, and the laminated crystal of sodium disilicate being ground into powder is added in second material and is stirred mixed
It closes uniformly, obtains third material, then atlapulgite is weighed by the proportioning, and the atlapulgite claimed is added in third material
And be uniformly mixed, obtain 4 materials, then high polymer composite synergistic activator is weighed by the proportioning, and by the high score of title
Sub- composite synergistic activator is added in 4 materials and is uniformly mixed, and obtains the 5th material, finally adds by the proportional quantity
Sufficient deionized water, and be uniformly mixed, obtain pig farm excrement object inorganic agent.
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN110885120A (en) * | 2019-12-05 | 2020-03-17 | 常州市振邦化工制造有限公司 | Efficient composite flocculant for papermaking sewage treatment |
| CN112979123A (en) * | 2021-04-01 | 2021-06-18 | 福州大学 | Method for removing sludge odor and harmful substances by reduction-oxidation and deodorized sludge |
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| CN105967261A (en) * | 2016-05-26 | 2016-09-28 | 许婷 | Sewage treatment agent special for printing and dyeing wastewater and preparation method of sewage treatment agent |
| CN106745350A (en) * | 2016-11-11 | 2017-05-31 | 广西新六合环保有限责任公司 | A kind of Industrial waste water treatment agent |
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| CN101817596A (en) * | 2010-01-25 | 2010-09-01 | 夏光甫 | Environmental-friendly spunlace nonwoven circulating water treating liquid and preparation method thereof |
| CN105967261A (en) * | 2016-05-26 | 2016-09-28 | 许婷 | Sewage treatment agent special for printing and dyeing wastewater and preparation method of sewage treatment agent |
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| CN110885120A (en) * | 2019-12-05 | 2020-03-17 | 常州市振邦化工制造有限公司 | Efficient composite flocculant for papermaking sewage treatment |
| CN112979123A (en) * | 2021-04-01 | 2021-06-18 | 福州大学 | Method for removing sludge odor and harmful substances by reduction-oxidation and deodorized sludge |
| CN112979123B (en) * | 2021-04-01 | 2022-03-29 | 福州大学 | Method for removing sludge odor and harmful substances by reduction-oxidation and deodorized sludge |
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Application publication date: 20181030 |