CN103655908B - FUFANG EJIAO JIANG and preparation technology thereof - Google Patents
FUFANG EJIAO JIANG and preparation technology thereof Download PDFInfo
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- CN103655908B CN103655908B CN201310600819.7A CN201310600819A CN103655908B CN 103655908 B CN103655908 B CN 103655908B CN 201310600819 A CN201310600819 A CN 201310600819A CN 103655908 B CN103655908 B CN 103655908B
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Abstract
The present invention relates to a kind of FUFANG EJIAO JIANG and preparation technology thereof.Existing ass glue oral liquid uncomfortable yin-deficiency constitution crowd take.For this reason, this FUFANG EJIAO JIANG is made up according to new technology of the raw materials such as Colla Corii Asini, Radix Ginseng, Radix Scrophulariae, Radix Rehmanniae Preparata, Radix Codonopsis and Fructus Ponciri Trifoliatae (Fructus Ponciri Trifoliatae Immaturus).Radix Ginseng, Radix Scrophulariae are first immersed ethanol and then add in high-pressure alcohol extraction tank by this FUFANG EJIAO JIANG preparation technology, and then to inflating pressure to 8 in high-pressure alcohol extraction tank ~ 10kgf/cm
2, soak 2 hours, then put into the tank body of new medicine extractor.Preferentially adopt film condensing device to concentrate during concentration of liquid medicine simultaneously.FUFANG EJIAO JIANG of the present invention has YIN nourishing and QI supplementing, nourishing blood function, patient and the weakness of the spleen and stomach person of yin-deficiency constitution also can take, be applicable to various crowd to take, be particularly suitable for women to take, its preparation technology takes height-normal pressure alcohol extraction/water extraction mixed extraction new technology to medicine juice raw material, and the effective ingredient of each component is not run off.
Description
Technical field
The present invention relates to a kind of FUFANG EJIAO JIANG and preparation technology thereof.
Background technology
FUFANG EJIAO JIANG has the effect of qi and blood tonifying, and successful, the clinical practice history of existing more than 30 year, but the patient of some yin-deficiency constitution takes and easily occurs that epistaxis etc. is got angry outward manifestation afterwards, and part weakness of the spleen and stomach person also there will be the symptoms such as anorexia.
Summary of the invention
The technical problem to be solved in the present invention is the above-mentioned defect how overcoming existing product prescription technology, provides a kind of long-term taking not easily to occur xerostomia, dry pharynx etc., and has the FUFANG EJIAO JIANG of strengthening the spleen and stomach effect.
For solving the problems of the technologies described above, this FUFANG EJIAO JIANG raw material comprise 125-130 kilogram Colla Corii Asini, the Radix Ginseng of 30-50 kilogram, the Radix Scrophulariae of 30-50 kilogram, the Radix Rehmanniae Preparata of 410-430 kilogram, the Radix Codonopsis of 410-430 kilogram, the Fructus Crataegi of 170-190 kilogram and the sucrose of 110-130 kilogram.
1. this FUFANG EJIAO JIANG preparation technology comprise the steps:. after taking the Radix Scrophulariae section of the Radix Ginseng of 30-50 kilogram, 30-50 kilogram, immerse 45% ethanol of 60 ~ 80 kilograms, then add in high-pressure alcohol extraction tank, then by air pump to inflating pressure 8 ~ 10kgf/cm in high-pressure alcohol extraction tank
2, soak 2 hours; Wherein high-pressure alcohol extraction tank top is provided with closed charging aperture, Pressure gauge and intake valve, and is furnished with air pump;
2.. by aforesaid weight ratio, take the Fructus Crataegi of the Radix Rehmanniae Preparata of 410-430 kilogram, the Radix Codonopsis of 410-430 kilogram, 170-190 kilogram, add in the tank body of new medicine extractor, then 5000 kilograms are added water, soak 0.5-2.0 hour, after closed tank, pass into Steam Heating, medical material after immersion is boiled, opens the circulation waterway of tank body evaporator overhead condenser simultaneously, then the material in high-pressure alcohol extraction tank is put into fast the tank body of new medicine extractor, continue heated and boiled, after being greater than 1.04 to medicine juice proportion, release first time medicine juice, stand-by;
Wherein new medicine extractor comprises tank body, and tank body top is provided with condenser, and tank wall is provided with vapour jacket, and tank base is provided with slag notch, and its top is provided with closed charging aperture; Described high-pressure alcohol extraction pot bottom is communicated with tank body by baiting valve;
3.. then second time adds water 3000 kilograms, heated and boiled, when being greater than 1.01 to medicine juice proportion, releases second time medicine juice, stand-by;
4.. then third time adds water 1800 kilograms, heated and boiled, reaches after more than 1.005 to medicine juice proportion, releases third time medicine juice;
5.. three medicine juice pumps are squeezed into seperator together and is separated, obtain hybrid separation liquid, before being separated, medicine juice funnel adds a gauze layer, and separating rate must not be greater than 16 kg/min, 30 minutes row's primary slags;
6.. open vacuum, when triple effect vacuum reaches 0.06MPa, hybrid separation liquid vacuum is sucked in triple effect evaporator and evaporates, be evaporated to medicine juice proportion and reach after between 1.05-1.06, release stand-by, obtain medicine juice;
7.. get the Colla Corii Asini of 125-130 kilogram and the water of 5 times of Colla Corii Asini weight, add in jacketed pan, after being heated to boil, Colla Corii Asini is added in pot and constantly stirs, make it to dissolve uniformly after glue, turn glue foam and impurity defecation with foam, then the sucrose adding 110-130 kilogram dissolves completely, make its proportion be greater than 1.12, obtain gum sugar liquid;
8.. 6. walk gained medicine juice and the by the and 7. walk gained gum sugar liquid, squeezing into pump has in the settling box of heating function, slowly adds sodium carbonate liquor, pH value is adjusted to 5.5-6.5, heated and boiled 15-20 minute, leave standstill more than 16 hours, be then separated by the mixed liquor seperator after precipitation, every 30 minutes deslagginves once, mixed liquor enters turnover barrel after being separated, carry out fine straining, pressure is no more than 0.1MPa, and the medicine juice after fine straining enters liquid receiver;
9.. the medicine juice of liquid receiver is concentrated into relative density more than 1.085, slowly adds sodium carbonate liquor, pH value is adjusted to 4.5-6.5, be heated to boil, 100 DEG C are boiled 15 minutes; Finally squeezed into by medicine juice pump in the finished product liquid receiver of band 100 mesh sieve, covered and enclosed, is no more than 6 hours standing time, fill, sterilizing and get final product.
Design like this, after Radix Ginseng, unit's participation ethanol put into high-pressure alcohol extraction tank together, under High Pressure, ethanol fully infiltrates in each cell of Radix Ginseng, after in the tank body adding new medicine extractor fast, pressure reduces suddenly, meets again the medicine juice of high temperature, Radix Ginseng, the intracellular ethanol of Radix Scrophulariae break through ginseng-cell wall, are brought in medicine juice by effective ingredient in Radix Ginseng, Radix Scrophulariae.
As optimization, the when 9. step is concentrated, by vacuum by the medicine juice suction concentration pan of liquid receiver, carries out concentrating under reduced pressure.
As optimization, the when 9. step is concentrated, adopt film condensing device, concentrate, by the clear water of film condensing device, give over to 2., 3., 4. step to add water use, gained concentrated solution through boiling, airtight fill, sterilizing is FUFANG EJIAO JIANG.Film condensing device is usually used in desalinization, and for people during desalinization is water by semipermeable membrane, is blocked in the high concentration saline before semipermeable membrane and is given it up; And present invention utilizes the high concentration medicine juice before being blocked in semipermeable membrane, also do not wasted by the water of semipermeable membrane simultaneously.Design like this, energy consumption is low, survivable medicament effective component.
As optimization, 1. the walk: 45% ethanol of Radix Ginseng, Radix Scrophulariae section immersion 60 ~ 80 kilograms, pulls out, put into plodder, then put back to together with residue in ethanol by juice, finally add in high-pressure alcohol extraction tank more together after 2 hours.Design like this, Radix Ginseng, Radix Scrophulariae cell suck after ethanol, then use plodder, contribute to squeeze crack Radix Ginseng, Radix Scrophulariae cell wall, are convenient to the and 2. walk ethanol and break through Radix Ginseng, Radix Scrophulariae cell wall, discharge the active ingredient in Radix Ginseng better.
FUFANG EJIAO JIANG of the present invention contains the rare Chinese medicines such as Colla Corii Asini, Radix Ginseng, Radix Scrophulariae, there are YIN nourishing and QI supplementing, nourishing blood function, patient and the weakness of the spleen and stomach person of yin-deficiency constitution take, also there will not be the malaise symptoms such as dry mouth and parching tongue, anorexia, be applicable to various crowd to take, be particularly suitable for women to take, its preparation technology is fully extracted the effective ingredient of the rare Chinese medicines such as Colla Corii Asini, Radix Ginseng, Radix Scrophulariae, has played the drug effect of rare Chinese medicine to greatest extent.
Accompanying drawing explanation
Below in conjunction with accompanying drawing, the equipment that the present invention uses is described further:
Fig. 1 is the structural representation of high-pressure alcohol extraction tank and new medicine extractor.
Fig. 2 is the schematic diagram utilizing film condensing device concentrated medicament.
In figure: 1 be high-pressure alcohol extraction tank, 2 be visor, 3 be closed charging aperture, 4 be Pressure gauge, 5 be intake valve, 6 be tank body, 7 be condenser, 8 be vapour jacket, 9 be slag notch, 10 be baiting valve, 11 be film condensing device, 12 be medicine juice feed pipe, 13 be outlet pipe, 15 be piston pump for medicine juice discharge nozzle, 14 after concentrated.
Detailed description of the invention
Embodiment 1: 1.. take 30kg Radix Ginseng, 40kg Radix Scrophulariae, after section, immerse 45% ethanol (namely volumetric concentration is the ethanol water of 45%) of 60kg, then add in high-pressure alcohol extraction tank 1, then to be pressurizeed 10kgf/cm to inflated with nitrogen in high-pressure alcohol extraction tank 1 by air pump
2, soak 2 hours; Wherein high-pressure alcohol extraction tank 1 top is provided with closed charging aperture 3, Pressure gauge 4 and intake valve 5, and is furnished with air pump (not shown), as shown in Figure 1.
2.. by aforesaid weight ratio, take the Radix Rehmanniae Preparata of 410kg, the Radix Codonopsis of 420kg, the Fructus Crataegi of 190kg, add in the tank body of new medicine extractor, then 5000 kilograms are added water, soak 1.5 hours, after closed tank, pass into Steam Heating, medical material after immersion is boiled, open the circulation waterway of tank body evaporator overhead condenser simultaneously, again the material in high-pressure alcohol extraction tank 1 is put into fast the tank body 6 of new medicine extractor, high-pressure alcohol extraction tank 1 side is provided with visor 2, observed by this visor 2, material in high-pressure alcohol extraction tank 1 only can be put into the tank body 6 of new medicine extractor by operator, prevent because nitrogen enters tank body 6, the pressure in tank body 6 is caused to raise, continue heated and boiled, after being greater than 1.04 to medicine juice proportion, release first time medicine juice, stand-by,
Wherein new medicine extractor comprises tank body 6, and tank body 6 top is provided with condenser 7, and tank body 6 sidewall is provided with vapour jacket 8, is provided with slag notch 9 bottom tank body 6, and its top is provided with closed charging aperture 3; Communicated with tank body 6 by baiting valve 10 bottom described high-pressure alcohol extraction tank 1, as shown in Figure 1.
3.. then second time adds water 3000 kilograms, heated and boiled, when being greater than 1.01 to medicine juice proportion, releases second time medicine juice, stand-by;
4.. then third time adds water 1800 kilograms, heated and boiled, reaches after more than 1.005 to medicine juice proportion, releases third time medicine juice;
5.. three medicine juice pumps are squeezed into seperator together and is separated, obtain hybrid separation liquid, before being separated, medicine juice funnel adds a gauze layer, and separating rate must not be greater than 16 kg/min, 30 minutes row's primary slags;
6.. open vacuum, when triple effect vacuum reaches 0.06MPa, hybrid separation liquid vacuum is sucked in triple effect evaporator and evaporates, be evaporated to medicine juice proportion and reach after between 1.05-1.06, release stand-by, obtain medicine juice;
7.. get the Colla Corii Asini of 125kg and the water of 5 times of Colla Corii Asini weight, add in jacketed pan, after being heated to boil, Colla Corii Asini is added in pot and constantly stirs, make it to dissolve uniformly after glue, turn glue foam and impurity defecation with foam, then the sucrose adding 120kg dissolves completely, make its proportion be greater than 1.12, obtain gum sugar liquid;
8.. 6. walk gained medicine juice and the by the and 7. walk gained gum sugar liquid, squeezing into pump has in the settling box of heating function, slowly adds sodium carbonate liquor, pH value is adjusted to 5.5-6.5, heated and boiled 15-20 minute, leave standstill more than 16 hours, be then separated by the mixed liquor seperator after precipitation, every 30 minutes deslagginves once, mixed liquor enters turnover barrel after being separated, carry out fine straining, pressure is no more than 0.1MPa, and the medicine juice after fine straining enters liquid receiver;
9.. the medicine juice of liquid receiver is concentrated into relative density more than 1.085, slowly adds sodium carbonate liquor, pH value is adjusted to 4.5-6.5, be heated to boil, 100 DEG C are boiled 15 minutes; Finally squeezed into by medicine juice pump in the finished product liquid receiver of band 100 mesh sieve, covered and enclosed, be no more than 6 hours standing time, fill, namely sterilizing obtains FUFANG EJIAO JIANG A.
The sorbic acid of the Radix Rehmanniae Preparata of the Colla Corii Asini of embodiment 2: raw material is changed into: 127.5kg, 45% ethanol of 70kg, 40kg Radix Ginseng, 50kg Radix Scrophulariae 420kg, the Radix Codonopsis of 430kg, the Fructus Crataegi of 170kg, the sucrose of 130kg and 2.2kg, the when 9. step is concentrated, adopt film condensing device, concentrate, as shown in Figure 2, by the clear water of film condensing device 11, give over to and 2., 3., 4. walk the use that adds water, gained concentrated solution through boiling, airtight fill, sterilizing is finished product FUFANG EJIAO JIANG B, all the other techniques as described in Example 1, are omited.
The sucrose of the Radix Scrophulariae of the Colla Corii Asini of embodiment 3: raw material is changed into: 130kg, 45% ethanol of 80kg, 50kg Radix Ginseng, 30kg, the Radix Rehmanniae Preparata of 430kg, the Radix Codonopsis of 410kg, the Fructus Crataegi of 180kg and 110kg, 1. the walk: 45% ethanol of Radix Ginseng, Radix Scrophulariae section immersion 60 ~ 80 amount part, pull out after 2 hours, put into the extruding of screw extruder (not shown), then juice is put back in ethanol together with residue, finally add together again in high-pressure alcohol extraction tank 1, all the other techniques as described in Example 1, obtain FUFANG EJIAO JIANG C.
Contrast experiment 1: choose same batch of ginseng raw material, be divided into four groups, respectively by technique and FUFANG EJIAO JIANG conventional fabrication process production FUFANG EJIAO JIANG described in embodiment 1,2,3, produces Radix Ginseng residue A, Radix Ginseng residue B, Radix Ginseng residue C, Radix Ginseng residue D respectively.Detect ginsenoside (Ginsenoside) content in above-mentioned four kinds of Radix Ginseng residues respectively, obtain following table
Upper table illustrates, the utilization rate of the present invention to Radix Ginseng is higher.
Contrast experiment: choose 300 volunteers respectively, be divided into 6 groups---A group, B group, C group, D group, E group and F group, often organizes 50 people,
A group people morning, noon and afternoon every day after meal, take a 20ml respectively and fill FUFANG EJIAO JIANG A;
B group people morning, noon and afternoon every day after meal, take a 20ml respectively and fill FUFANG EJIAO JIANG B;
C group people morning, noon and afternoon every day after meal, take a 20ml respectively and fill FUFANG EJIAO JIANG C;
D group people morning, noon and afternoon every day after meal, take a 20ml respectively and fill commercially available FUFANG EJIAO JIANG.
Result: after six months, in D group there is xerostomia, dry pharynx phenomenon in 32 people's reflections, and abdominal distention, inappetence phenomenon appear in 16 people's reflections, and 2 people have no adverse reaction.And there is not the bad phenomenon such as xerostomia, dry pharynx, inappetence per capita in A-F group.
Claims (4)
1. a preparation technology for FUFANG EJIAO JIANG, comprises the steps:
1.. after taking the Radix Scrophulariae section of the Radix Ginseng of 30-50 kilogram, 30-50 kilogram, immerse 45% ethanol of 60 ~ 80 kilograms, then add in high-pressure alcohol extraction tank, then by air pump to inflating pressure 8 ~ 10kgf/cm in high-pressure alcohol extraction tank
2, soak 2 hours; Wherein high-pressure alcohol extraction tank top is provided with closed charging aperture, Pressure gauge and intake valve, and is furnished with air pump;
2.. take the Fructus Crataegi of the Radix Rehmanniae Preparata of 410-430 kilogram, the Radix Codonopsis of 410-430 kilogram, 170-190 kilogram, add in the tank body of new medicine extractor, then 5000 kilograms are added water, soak 0.5-2.0 hour, after closed tank, pass into Steam Heating, medical material after immersion is boiled, open the circulation waterway of tank body evaporator overhead condenser simultaneously, again the material in high-pressure alcohol extraction tank is put into fast the tank body of new medicine extractor, continue heated and boiled, after being greater than 1.04 to medicine juice proportion, release first time medicine juice, stand-by;
Wherein new medicine extractor comprises tank body, and tank body top is provided with condenser, and tank wall is provided with vapour jacket, and tank base is provided with slag notch, and its top is provided with closed charging aperture; Described high-pressure alcohol extraction pot bottom is communicated with tank body by baiting valve;
3.. then second time adds water 3000 kilograms, heated and boiled, when being greater than 1.01 to medicine juice proportion, releases second time medicine juice, stand-by;
4.. then third time adds water 1800 kilograms, heated and boiled, reaches after more than 1.005 to medicine juice proportion, releases third time medicine juice;
5.. three medicine juice pumps are squeezed into seperator together and is separated, obtain hybrid separation liquid, before being separated, medicine juice funnel adds a gauze layer, and separating rate must not be greater than 16 kg/min, 30 minutes row's primary slags;
6.. open vacuum, when triple effect vacuum reaches 0.06MPa, hybrid separation liquid vacuum is sucked in triple effect evaporator and evaporates, be evaporated to medicine juice proportion and reach after between 1.05-1.06, release stand-by, obtain medicine juice;
7.. get the Colla Corii Asini of 125-130 kilogram and the water of 5 times of Colla Corii Asini weight, add in jacketed pan, after being heated to boil, Colla Corii Asini is added in pot and constantly stirs, make it to dissolve uniformly after glue, turn glue foam and impurity defecation with foam, then the sucrose adding 110-130 kilogram dissolves completely, make its proportion be greater than 1.12, obtain gum sugar liquid;
8.. 6. walk gained medicine juice and the by the and 7. walk gained gum sugar liquid, squeezing into pump has in the settling box of heating function, slowly adds sodium carbonate liquor, pH value is adjusted to 5.5-6.5, heated and boiled 15-20 minute, leave standstill more than 16 hours, be then separated by the mixed liquor seperator after precipitation, every 30 minutes deslagginves once, mixed liquor enters turnover barrel after being separated, carry out fine straining, pressure is no more than 0.1MPa, and the medicine juice after fine straining enters liquid receiver;
9.. the medicine juice of liquid receiver is concentrated into relative density more than 1.085, slowly adds sodium carbonate liquor, pH value is adjusted to 4.5-6.5, be heated to boil, 100 DEG C are boiled 15 minutes; Finally squeezed into by medicine juice pump in the finished product liquid receiver of band 100 mesh sieve, covered and enclosed, is no more than 6 hours standing time, fill, sterilizing and get final product.
2. the preparation technology of FUFANG EJIAO JIANG according to claim 1, is characterized in that: the when 9. step is concentrated, by vacuum by the medicine juice suction concentration pan of liquid receiver, carries out concentrating under reduced pressure.
3. the preparation technology of FUFANG EJIAO JIANG according to claim 1, it is characterized in that: the when 9. step is concentrated, adopt film condensing device, concentrate, by the clear water of film condensing device, give over to 2., 3., 4. step to add water use, gained concentrated solution through boiling, airtight fill, sterilizing is FUFANG EJIAO JIANG.
4. the preparation technology of FUFANG EJIAO JIANG according to claim 1 or 2 or 3, it is characterized in that: 1. the walk: 45% ethanol of Radix Ginseng, Radix Scrophulariae section immersion 60 ~ 80 kilograms, pull out after 2 hours, put into plodder, then juice is put back in ethanol together with residue, finally add in high-pressure alcohol extraction tank more together.
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| CN105168676B (en) * | 2015-09-25 | 2019-12-03 | 湖北穆兰同大科技有限公司 | Safe bacteriostatic gel of Ms and preparation method thereof |
| CN105213359B (en) * | 2015-09-25 | 2018-05-18 | 湖北穆兰同大科技有限公司 | Women secret conditioning liquid and preparation method thereof |
| CN113813640A (en) * | 2021-10-14 | 2021-12-21 | 丽江英煌集生物工程有限公司 | Purified macamide activity refining device and method |
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| CN1168805A (en) * | 1997-06-20 | 1997-12-31 | 山东东阿阿胶股份有限公司 | Medicine for enriching the blood |
| CN101879248A (en) * | 2010-05-21 | 2010-11-10 | 郭景龙 | Medicine composition with blood tonification effect |
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| JP2004083449A (en) * | 2002-08-26 | 2004-03-18 | Kinji Ishida | Orally administrative composition for stress relaxation |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1168805A (en) * | 1997-06-20 | 1997-12-31 | 山东东阿阿胶股份有限公司 | Medicine for enriching the blood |
| CN101879248A (en) * | 2010-05-21 | 2010-11-10 | 郭景龙 | Medicine composition with blood tonification effect |
Non-Patent Citations (1)
| Title |
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| 康复春口服液质量标准研究;彭善贵等;《中国当代医药》;20100831;第17卷(第24期);第47-48、50页，第47页左栏最后1段，右栏最后1段，第48页图2 * |
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