CN103655898B - The FUFANG EJIAO JIANG of dysmenorrhea can be treated - Google Patents
The FUFANG EJIAO JIANG of dysmenorrhea can be treated Download PDFInfo
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- CN103655898B CN103655898B CN201310595990.3A CN201310595990A CN103655898B CN 103655898 B CN103655898 B CN 103655898B CN 201310595990 A CN201310595990 A CN 201310595990A CN 103655898 B CN103655898 B CN 103655898B
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Abstract
The present invention relates to a kind of FUFANG EJIAO JIANG for the treatment of dysmenorrhea.Existing FUFANG EJIAO JIANG curative mechanism, mainly to take good care of, to nourish, during treatment dysmenorrhea, takes effect slightly slowly aobvious.For solving the problems of the technologies described above, originally the FUFANG EJIAO JIANG raw material can treating dysmenorrhea comprises the Colla Corii Asini of 125-130 weight portion, the Radix Angelicae Sinensis of 30-50 weight portion, the Radix Rehmanniae Preparata of 380-390 weight portion, the Herba Leonuri of 430-450 weight portion, the Fructus Crataegi of 160-165 weight portion, the sucrose of 130-150 weight portion, make according to following step the FUFANG EJIAO JIANG that the present invention can treat dysmenorrhea and contain the rare Chinese medicines such as Colla Corii Asini, there are YIN nourishing and QI supplementing, nourishing blood function, treatment dysmenorrhea, instant effect is applicable to female friend and takes.
Description
Technical field
The present invention relates to a kind of FUFANG EJIAO JIANG for the treatment of dysmenorrhea.
Background technology
Colla Corii Asini is a kind of rare Chinese medicine, be usually used in enriching blood, FUFANG EJIAO JIANG is the bottled oral liquid of one of east, Shandong Donga Colla Corii Asini limited company exploitation, taking convenience, all have certain curative effect to various anemic disorders, its curative mechanism is mainly to take good care of, to nourish; When treating menalgia, take effect slightly slowly aobvious.
Summary of the invention
The technical problem to be solved in the present invention is the above-mentioned defect how overcoming prior art, provides one to enrich blood, takes good care of instant effect, can treat the FUFANG EJIAO JIANG of menalgia simultaneously.
For solving the problems of the technologies described above, originally the FUFANG EJIAO JIANG raw material can treating dysmenorrhea comprises the Colla Corii Asini of 125-130 weight portion, the Radix Ginseng of 55-65 weight portion, the Radix Angelicae Sinensis of 30-50 weight portion, the Herba Leonuri of 430-450 weight portion, the Radix Rehmanniae Preparata of 380-390 weight portion, the Fructus Crataegi of 160-165 weight portion, the sucrose of 130-150 weight portion, makes according to following step.
The present invention can treat the FUFANG EJIAO JIANG preparation technology of dysmenorrhea, comprises the steps:
1.. take the Radix Ginseng of 55-65 weight portion, after section, immerse 45% ethanol of 60 ~ 80 weight portions, then add in high-pressure alcohol extraction tank, then by air pump to inflating pressure 8 ~ 10kgf/cm in high-pressure alcohol extraction tank
2, soak 2 hours; Wherein high-pressure alcohol extraction tank top is provided with closed charging aperture, Pressure gauge and intake valve, and is furnished with air pump;
2.. by aforesaid weight ratio, take the Radix Angelicae Sinensis of 30-50 weight portion, the Herba Leonuri of 430-450 weight portion, the Radix Rehmanniae Preparata of 410-430 weight portion, the Radix Codonopsis of 410-430 weight portion, the Fructus Crataegi of 170-190 weight portion, add in the tank body of new medicine extractor, then 5000 kilograms are added water, soak 0.5-2.0 hour, after closed tank, pass into Steam Heating, medical material after immersion is boiled, open the circulation waterway of tank body evaporator overhead condenser simultaneously, again the material in high-pressure alcohol extraction tank is put into fast the tank body of new medicine extractor, continue heated and boiled, after being greater than 1.04 to medicine juice proportion, release first time medicine juice, stand-by,
Wherein new medicine extractor comprises tank body, and tank body top is provided with condenser, and tank wall is provided with vapour jacket, and tank base is provided with slag notch, and its top is provided with closed charging aperture; Described high-pressure alcohol extraction pot bottom is communicated with tank body by baiting valve;
3.. then second time adds water 3000 kilograms, heated and boiled, when being greater than 1.01 to medicine juice proportion, releases second time medicine juice, stand-by;
4.. then third time adds water 1800 kilograms, heated and boiled, reaches after more than 1.005 to medicine juice proportion, releases third time medicine juice;
5.. three medicine juice pumps are squeezed into seperator together and is separated, obtain hybrid separation liquid, before being separated, medicine juice funnel adds a gauze layer, and separating rate must not be greater than 16 kg/min, 30 minutes row's primary slags;
6.. open vacuum, when triple effect vacuum reaches 0.06MPa, hybrid separation liquid vacuum is sucked in triple effect evaporator and evaporates, be evaporated to medicine juice proportion and reach after between 1.05-1.06, release stand-by, obtain medicine juice;
7.. get the Colla Corii Asini of 125-130 weight portion and the water of 5 times of Colla Corii Asini weight, add in jacketed pan, after being heated to boil, Colla Corii Asini is added in pot and constantly stirs, make it to dissolve uniformly after glue, turn glue foam and impurity defecation with foam, then the sucrose adding 110-130 weight portion dissolves completely, make its proportion be greater than 1.12, obtain gum sugar liquid;
8.. 6. walk gained medicine juice and the by the and 7. walk gained gum sugar liquid, squeezing into pump has in the settling box of heating function, slowly adds sodium carbonate liquor, pH value is adjusted to 5.5-6.5, heated and boiled 15-20 minute, leave standstill more than 16 hours, be then separated by the mixed liquor seperator after precipitation, every 30 minutes deslagginves once, mixed liquor enters turnover barrel after being separated, carry out fine straining, pressure is no more than 0.1MPa, and the medicine juice after fine straining enters liquid receiver;
9.. the medicine juice of liquid receiver is concentrated into relative density more than 1.085, slowly adds sodium carbonate liquor, pH value is adjusted to 4.5-6.5, be heated to boil, 100 DEG C are boiled 15 minutes; Finally squeezed into by medicine juice pump in the finished product liquid receiver of band 100 mesh sieve, covered and enclosed, is no more than 6 hours standing time, fill, sterilizing and get final product.
Design like this, people participates in after 45% ethanol puts into high-pressure alcohol extraction tank together, under High Pressure, 45% ethanol fully infiltrates in each cell of Radix Ginseng, after in the tank body adding new medicine extractor fast, pressure reduces suddenly, meets again the medicine juice of high temperature, 45% ethanol in ginseng-cell breaks through ginseng-cell wall, is brought in medicine juice by the effective ingredient in Radix Ginseng.
As optimization, the when 9. step is concentrated, by vacuum by the medicine juice suction concentration pan of liquid receiver, carries out concentrating under reduced pressure.
As optimization, the when 9. step is concentrated, adopt film condensing device, concentrate, by the clear water of film condensing device, give over to 2., 3., 4. step to add water use, gained concentrated solution through boiling, airtight fill, sterilizing is finished product FUFANG EJIAO JIANG.Film condensing device is usually used in desalinization, and for people during desalinization is water by semipermeable membrane, is blocked in the high concentration saline before semipermeable membrane and is given it up; And present invention utilizes the high concentration medicine juice before being blocked in semipermeable membrane, also do not wasted by the water of semipermeable membrane simultaneously.Design like this, energy consumption is low, survivable medicament effective component.
As optimization, 1. the walk: 45% ethanol of Radix Ginseng section immersion 60 ~ 80 weight portion, pulls out, put into plodder, then put back to together with residue in ethanol by juice, finally add in high-pressure alcohol extraction tank more together after 2 hours.Design like this, ginseng-cell sucks after ethanol, then uses plodder, contributes to squeeze crack ginseng-cell wall, is convenient to the and 2. walks ethanol and break through ginseng-cell wall, discharge the active ingredient in Radix Ginseng better.
The FUFANG EJIAO JIANG that the present invention can treat dysmenorrhea contains the rare Chinese medicines such as Colla Corii Asini, has YIN nourishing and QI supplementing, nourishing blood function, and treatment dysmenorrhea, instant effect is applicable to female friend and takes.
Accompanying drawing explanation
Below in conjunction with accompanying drawing, the equipment that the present invention uses is described further:
Fig. 1 is the structural representation of high-pressure alcohol extraction tank and new medicine extractor.
Fig. 2 is the schematic diagram utilizing film condensing device concentrated medicament.
In figure: 1 be high-pressure alcohol extraction tank, 2 be visor, 3 be closed charging aperture, 4 be Pressure gauge, 5 be intake valve, 6 be tank body, 7 be condenser, 8 be vapour jacket, 9 be slag notch, 10 be baiting valve, 11 be film condensing device, 12 be medicine juice feed pipe, 13 be outlet pipe, 15 be piston pump for medicine juice discharge nozzle, 14 after concentrated.
Specific embodiment
Embodiment one: 1.. take the Radix Ginseng of 55kg, after section, immerse 45% ethanol (namely volumetric concentration is the ethanol water of 45%) of 60kg, then add in high-pressure alcohol extraction tank, then by air pump to inflating pressure 8 ~ 10kgf/cm in high-pressure alcohol extraction tank
2, soak 2 hours; Wherein high-pressure alcohol extraction tank top is provided with closed charging aperture, Pressure gauge and intake valve, and is furnished with air pump;
2.. by aforesaid weight ratio, take the Radix Angelicae Sinensis of 30kg, the Herba Leonuri of 440kg, the Radix Rehmanniae Preparata of 410kg, the Radix Codonopsis of 420kg, the Fructus Crataegi of 190kg, add in the tank body of new medicine extractor, then 5000 kilograms are added water, soak 0.5-2.0 hour, after closed tank, pass into Steam Heating, medical material after immersion is boiled, opens the circulation waterway of tank body evaporator overhead condenser simultaneously, then the material in high-pressure alcohol extraction tank is put into fast the tank body of new medicine extractor, continue heated and boiled, after being greater than 1.04 to medicine juice proportion, release first time medicine juice, stand-by;
Wherein new medicine extractor comprises tank body, and tank body top is provided with condenser, and tank wall is provided with vapour jacket, and tank base is provided with slag notch, and its top is provided with closed charging aperture; Described high-pressure alcohol extraction pot bottom is communicated with tank body by baiting valve;
3.. then second time adds water 3000 kilograms, heated and boiled, when being greater than 1.01 to medicine juice proportion, releases second time medicine juice, stand-by;
4.. then third time adds water 1800 kilograms, heated and boiled, reaches after more than 1.005 to medicine juice proportion, releases third time medicine juice;
5.. three medicine juice pumps are squeezed into seperator together and is separated, obtain hybrid separation liquid, before being separated, medicine juice funnel adds a gauze layer, and separating rate must not be greater than 16 kg/min, 30 minutes row's primary slags;
6.. open vacuum, when triple effect vacuum reaches 0.06MPa, hybrid separation liquid vacuum is sucked in triple effect evaporator and evaporates, be evaporated to medicine juice proportion and reach after between 1.05-1.06, release stand-by, obtain medicine juice;
7.. get the Colla Corii Asini of 125kg and the water of 5 times of Colla Corii Asini weight, add in jacketed pan, after being heated to boil, Colla Corii Asini is added in pot and constantly stirs, make it to dissolve uniformly after glue, turn glue foam and impurity defecation with foam, then the sucrose adding 120kg dissolves completely, make its proportion be greater than 1.12, obtain gum sugar liquid;
8.. 6. walk gained medicine juice and the by the and 7. walk gained gum sugar liquid, squeezing into pump has in the settling box of heating function, slowly adds sodium carbonate liquor, pH value is adjusted to 5.5-6.5, heated and boiled 15-20 minute, leave standstill more than 16 hours, be then separated by the mixed liquor seperator after precipitation, every 30 minutes deslagginves once, mixed liquor enters turnover barrel after being separated, carry out fine straining, pressure is no more than 0.1MPa, and the medicine juice after fine straining enters liquid receiver;
9.. the medicine juice of liquid receiver is concentrated into relative density more than 1.085, slowly adds sodium carbonate liquor, pH value is adjusted to 4.5-6.5, be heated to boil, 100 DEG C are boiled 15 minutes; Finally squeezed into by medicine juice pump in the finished product liquid receiver of band 100 mesh sieve, covered and enclosed, is no more than 6 hours standing time, fill, and namely sterilizing obtains the FUFANG EJIAO JIANG A that can treat dysmenorrhea.
The sucrose of the Herba Leonuri of the Radix Ginseng of the Colla Corii Asini of embodiment 2: raw material is changed into: 127.5kg, 45% ethanol of 70kg, 60kg, the Radix Angelicae Sinensis of 40kg, 450kg, the Radix Rehmanniae Preparata of 420kg, the Radix Codonopsis of 430kg, the Fructus Crataegi of 170kg and 130kg, the when 9. step is concentrated, adopt film condensing device, concentrate, as shown in Figure 2, by the clear water of film condensing device 11, give over to and 2., 3., 4. walk the use that adds water, gained concentrated solution through boiling, airtight fill, sterilizing is the FUFANG EJIAO JIANG B that finished product can treat dysmenorrhea, all the other techniques as described in Example 1, are omited.
The sucrose of the Herba Leonuri of the Radix Ginseng of the Colla Corii Asini of embodiment 3: raw material is changed into: 130kg, 45% ethanol of 80kg, 65kg, the Radix Angelicae Sinensis of 50kg, 430kg, the Radix Rehmanniae Preparata of 430kg, the Radix Codonopsis of 410kg, the Fructus Crataegi of 180kg and 110kg, 1. the walk: 45% ethanol of Radix Ginseng section immersion 60 ~ 80 amount part was pulled out after 2 hours, put into the extruding of screw extruder (not shown), then juice is put back in ethanol together with residue, finally add together again in high-pressure alcohol extraction tank 1, all the other techniques as described in Example 1, obtain the FUFANG EJIAO JIANG C that can treat dysmenorrhea.
Contrast experiment one: choose same batch of ginseng raw material, be divided into four groups, respectively by technique and FUFANG EJIAO JIANG conventional fabrication process production FUFANG EJIAO JIANG described in embodiment 1,2,3, produce Radix Ginseng residue A, Radix Ginseng residue B, Radix Ginseng residue C, Radix Ginseng residue D respectively.Detect ginsenoside (Ginsenoside) content in above-mentioned four kinds of Radix Ginseng residues respectively, obtain following table
Upper table illustrates, the utilization rate of the present invention to Radix Ginseng is higher.
Contrast experiment two: the volunteer choosing 48 dysmenorrheas respectively, are divided into 4 groups---A group, B group, C group and D group, often organize 12 people,
A group people morning, noon and afternoon every day after meal, take the FUFANG EJIAO JIANG A that a 20ml dress can treat dysmenorrhea respectively;
B group people morning, noon and afternoon every day after meal, take the FUFANG EJIAO JIANG B that a 20ml dress can treat dysmenorrhea respectively;
C group people morning, noon and afternoon every day after meal, take the FUFANG EJIAO JIANG C that a 20ml dress can treat dysmenorrhea respectively;
D group people morning, noon and afternoon every day after meal, take a 20ml respectively and fill commercially available FUFANG EJIAO JIANG.
Result: after six months, in D group, 5 people reflect that dysmenorrhea takes a turn for the better to some extent, and other three people reflect DeGrain, and after 1 year, 3 people cure, and 2 people's reflections take a turn for the better to some extent, and it is invalid that another people is reflected.
And after A-C group people takes three months, except D group one people reflect not obvious except, all the other volunteers all reflect that menstruation is gradually normal, and dysmenorrhea symptom alleviates greatly, all reflects dysmenorrhea transference cure after half a year.
Wherein in B group people, original 2 people have dysuria, constipation symptom before taking, since take can treat dysmenorrhea FUFANG EJIAO JIANG B after two months, symptom also disappears.
Claims (4)
1. treat a FUFANG EJIAO JIANG for dysmenorrhea, its preparation technology comprises the steps:
1.. take the Radix Ginseng of 55-65 kilogram, after section, immerse 45% ethanol of 60 ~ 80 kilograms, then add in high-pressure alcohol extraction tank, then by air pump to inflating pressure 8 ~ 10kgf/cm in high-pressure alcohol extraction tank
2, soak 2 hours; Wherein high-pressure alcohol extraction tank top is provided with closed charging aperture, Pressure gauge and intake valve, and is furnished with air pump;
2.. take the Radix Angelicae Sinensis of 30-50 kilogram, the Herba Leonuri of 430-450 kilogram, the Radix Rehmanniae Preparata of 410-430 kilogram, the Radix Codonopsis of 410-430 kilogram, the Fructus Crataegi of 170-190 kilogram, add in the tank body of new medicine extractor, then 5000 kilograms are added water, soak 0.5-2.0 hour, after closed tank, pass into Steam Heating, medical material after immersion is boiled, open the circulation waterway of tank body evaporator overhead condenser simultaneously, again the material in high-pressure alcohol extraction tank is put into fast the tank body of new medicine extractor, continue heated and boiled, after being greater than 1.04 to medicine juice proportion, release first time medicine juice, stand-by,
Wherein new medicine extractor comprises tank body, and tank body top is provided with condenser, and tank wall is provided with vapour jacket, and tank base is provided with slag notch, and its top is provided with closed charging aperture; Described high-pressure alcohol extraction pot bottom is communicated with tank body by baiting valve;
3.. then second time adds water 3000 kilograms, heated and boiled, when being greater than 1.01 to medicine juice proportion, releases second time medicine juice, stand-by;
4.. then third time adds water 1800 kilograms, heated and boiled, reaches after more than 1.005 to medicine juice proportion, releases third time medicine juice;
5.. three medicine juice pumps are squeezed into seperator together and is separated, obtain hybrid separation liquid, before being separated, medicine juice funnel adds a gauze layer, and separating rate must not be greater than 16 kg/min, 30 minutes row's primary slags;
6.. open vacuum, when triple effect vacuum reaches 0.06MPa, hybrid separation liquid vacuum is sucked in triple effect evaporator and evaporates, be evaporated to medicine juice proportion and reach after between 1.05-1.06, release stand-by, obtain medicine juice;
7.. get the Colla Corii Asini of 125-130 kilogram and the water of 5 times of Colla Corii Asini weight, add in jacketed pan, after being heated to boil, Colla Corii Asini is added in pot and constantly stirs, make it to dissolve uniformly after glue, turn glue foam and impurity defecation with foam, then the sucrose adding 110-130 kilogram dissolves completely, make its proportion be greater than 1.12, obtain gum sugar liquid;
8.. 6. walk gained medicine juice and the by the and 7. walk gained gum sugar liquid, squeezing into pump has in the settling box of heating function, slowly adds sodium carbonate liquor, pH value is adjusted to 5.5-6.5, heated and boiled 15-20 minute, leave standstill more than 16 hours, be then separated by the mixed liquor seperator after precipitation, every 30 minutes deslagginves once, mixed liquor enters turnover barrel after being separated, carry out fine straining, pressure is no more than 0.1MPa, and the medicine juice after fine straining enters liquid receiver;
9.. the medicine juice of liquid receiver is concentrated into relative density more than 1.085, slowly adds sodium carbonate liquor, pH value is adjusted to 4.5-6.5, be heated to boil, 100 DEG C are boiled 15 minutes; Finally squeezed into by medicine juice pump in the finished product liquid receiver of band 100 mesh sieve, covered and enclosed, is no more than 6 hours standing time, fill, sterilizing and get final product.
2. treat the FUFANG EJIAO JIANG of dysmenorrhea according to claim 1, it is characterized in that: the when 9. step is concentrated, by vacuum by the medicine juice suction concentration pan of liquid receiver, carries out concentrating under reduced pressure.
3. treat the FUFANG EJIAO JIANG of dysmenorrhea according to claim 1, it is characterized in that: the when 9. step is concentrated, adopt film condensing device, concentrate, by the clear water of film condensing device, give over to 2., 3., 4. step to add water use, gained concentrated solution through boiling, airtight fill, sterilizing is finished product FUFANG EJIAO JIANG.
4. according to claim 1 or 2 or 3, treat the FUFANG EJIAO JIANG of dysmenorrhea, it is characterized in that: 1. the walk: 45% ethanol of Radix Ginseng section immersion 60 ~ 80 kilograms, pull out after 2 hours, put into plodder, then juice is put back in ethanol together with residue, finally add in high-pressure alcohol extraction tank more together.
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| CN108283312A (en) * | 2017-12-28 | 2018-07-17 | 湖州品创孵化器有限公司 | A kind of Herba Leonuri granule and its preparation process with health maintenance effect |
| CN114848723A (en) * | 2022-06-16 | 2022-08-05 | 苏州华葆药业股份有限公司 | Production process of oral liquid for tonifying qi and blood |
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| CN1168805A (en) * | 1997-06-20 | 1997-12-31 | 山东东阿阿胶股份有限公司 | Medicine for enriching the blood |
| CN1824013A (en) * | 2005-12-15 | 2006-08-30 | 北京阜康仁生物制药科技有限公司 | Four material leenurus preparation and its new preparing method |
| CN1872202A (en) * | 2006-05-09 | 2006-12-06 | 株洲千金药业股份有限公司 | Method for preparing medication of replenishing qi and the blood |
| CN101879248A (en) * | 2010-05-21 | 2010-11-10 | 郭景龙 | Medicine composition with blood tonification effect |
| CN102100798A (en) * | 2011-01-19 | 2011-06-22 | 黄素荣 | Chinese medicine decoction for treating menoxenia of women |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2002275086A (en) * | 2001-03-15 | 2002-09-25 | Fancl Corp | Composition for improving valetudinarianish |
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Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1168805A (en) * | 1997-06-20 | 1997-12-31 | 山东东阿阿胶股份有限公司 | Medicine for enriching the blood |
| CN1824013A (en) * | 2005-12-15 | 2006-08-30 | 北京阜康仁生物制药科技有限公司 | Four material leenurus preparation and its new preparing method |
| CN1872202A (en) * | 2006-05-09 | 2006-12-06 | 株洲千金药业股份有限公司 | Method for preparing medication of replenishing qi and the blood |
| CN101879248A (en) * | 2010-05-21 | 2010-11-10 | 郭景龙 | Medicine composition with blood tonification effect |
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