CN103610974B - Sugar-free compound colla corii asini pulp and preparation technology thereof - Google Patents
Sugar-free compound colla corii asini pulp and preparation technology thereof Download PDFInfo
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- CN103610974B CN103610974B CN201310600686.3A CN201310600686A CN103610974B CN 103610974 B CN103610974 B CN 103610974B CN 201310600686 A CN201310600686 A CN 201310600686A CN 103610974 B CN103610974 B CN 103610974B
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Abstract
The present invention relates to a kind of sugar-free compound colla corii asini pulp and preparation technology thereof.Existing FUFANG EJIAO JIANG includes sucrose, is not suitable for hyperglycemia and diabetics is taken.Sugar-free compound colla corii asini pulp of the present invention is made up according to new technology of the raw materials such as Colla Corii Asini, Radix Ginseng, Radix Rehmanniae Preparata, Radix Codonopsis and Stevia rebaudiana (Bertoni) Hemsl extract and lemon grass extract.Radix Ginseng is first immersed 45% ethanol by this sugar-free compound colla corii asini pulp preparation technology, then adds in high-pressure alcohol extraction tank, and then to inflating pressure to 8 in high-pressure alcohol extraction tank ~ 10kgf/cm
2, soak 2 hours, then put into the tank body of new medicine extractor.Preferentially adopt film condensing device to concentrate during concentration of liquid medicine simultaneously.Sugar-free compound colla corii asini pulp of the present invention is applicable to hyperglycemia population and diabetic to take, and its preparation technology takes height-normal pressure alcohol extraction/water extraction mixed extraction new technology to medicine juice raw material, at utmost extracts the active ingredients such as Radix Ginseng, the effective ingredient of each component is not run off.
Description
Technical field
The present invention relates to a kind of sugar-free compound colla corii asini pulp and preparation technology thereof.
Background technology
April 5 calendar year 2001 bulletin, notification number is the preparation method that the Chinese invention patent of CN1064849C discloses a kind of medicament of enriching blood, this medicament of enriching blood is Be very effective enriching blood, in QI invigorating, but containing sucrose in its prescription, hyperglycemia and diabetics cannot be applied, limit the scope that it is suitable for colony.
Summary of the invention
The technical problem to be solved in the present invention is the above-mentioned defect how overcoming prior art, provides a kind of sugar-free compound colla corii asini pulp and preparation technology thereof.
For solving the problems of the technologies described above, sugar-free compound colla corii asini pulp of the present invention is prepared from according to shown weight ratio by following component:
Design like this, the middle-aged and elderly people that sugar-free compound colla corii asini pulp of the present invention is applicable to diabetes patient and hyperglycemia is taken.
Sugar-free compound colla corii asini pulp preparation technology of the present invention, comprises the steps:
1.. take the Radix Ginseng of 55-65 weight portion, after section, immerse 45% ethanol of 60 ~ 80 weight portions, then add in high-pressure alcohol extraction tank, then by air pump to inflating pressure 8 ~ 10kgf/cm in high-pressure alcohol extraction tank
2, soak 2 hours; Wherein high-pressure alcohol extraction tank top is provided with closed charging aperture, Pressure gauge and intake valve, and is furnished with air pump;
2.. by aforesaid weight ratio, take the Radix Rehmanniae Preparata of 410-430 weight portion, the Radix Codonopsis of 410-430 weight portion, the Fructus Crataegi of 170-190 weight portion, add in the tank body of new medicine extractor, then add water 5000 weight portions, soak 0.5-2.0 hour, after closed tank, pass into Steam Heating, medical material after immersion is boiled, opens the circulation waterway of tank body evaporator overhead condenser simultaneously, then the material in high-pressure alcohol extraction tank is put into fast the tank body of new medicine extractor, continue heated and boiled, after being greater than 1.04 to medicine juice proportion, release first time medicine juice, stand-by;
Wherein new medicine extractor comprises tank body, and tank body top is provided with condenser, and tank wall is provided with vapour jacket, and tank base is provided with slag notch, and its top is provided with closed charging aperture; Described high-pressure alcohol extraction pot bottom is communicated with tank body by baiting valve;
3.. then add water 3000 weight portions for the second time, and heated and boiled, when being greater than 1.01 to medicine juice proportion, releases second time medicine juice, stand-by;
4.. then add water 1800 weight portions for the third time, and heated and boiled, reaches after more than 1.005 to medicine juice proportion, releases third time medicine juice;
5.. three medicine juice pumps are squeezed into seperator together and is separated, obtain hybrid separation liquid, before being separated, medicine juice funnel adds a gauze layer, and separating rate must not be greater than 16 kg/min, 30 minutes row's primary slags;
6.. open vacuum, when triple effect vacuum reaches 0.06MPa, hybrid separation liquid vacuum is sucked in triple effect evaporator and evaporates, be evaporated to medicine juice proportion and reach after between 1.05-1.06, release stand-by, obtain medicine juice;
7.. get the Colla Corii Asini of 125-130 weight portion and the water of 5 times of Colla Corii Asini weight, add in jacketed pan, after being heated to boil, Colla Corii Asini is added in pot and constantly stirs, make it to dissolve uniformly after glue, turn glue foam and impurity defecation with foam, then add the Stevia rebaudiana (Bertoni) Hemsl extract of 20-30 weight portion and the lemon grass extract of 10-20 weight portion, obtain the glue that proportion is greater than 1.12;
8.. 6. walk gained medicine juice and the by the and 7. walk gained glue, squeezing into pump has in the settling box of heating function, slowly adds sodium carbonate liquor, pH value is adjusted to 5.5-6.5, heated and boiled 15-20 minute, leave standstill more than 16 hours, be then separated by the mixed liquor seperator after precipitation, every 30 minutes deslagginves once, mixed liquor enters turnover barrel after being separated, carry out fine straining, pressure is no more than 0.1MPa, and the medicine juice after fine straining enters liquid receiver;
9.. the medicine juice of liquid receiver is concentrated into relative density more than 1.085, slowly adds sodium carbonate liquor, pH value is adjusted to 4.5-6.5, be heated to boil, 100 DEG C are boiled 15 minutes; Finally squeezed into by medicine juice pump in the finished product liquid receiver of band 100 mesh sieve, covered and enclosed, is no more than 6 hours standing time, fill, sterilizing and get final product.
Design like this, people participates in after ethanol puts into high-pressure alcohol extraction tank together, under High Pressure, ethanol fully infiltrates in each cell of Radix Ginseng, after in the tank body adding new medicine extractor fast, pressure reduces suddenly, meets again the medicine juice of high temperature, ethanol in ginseng-cell breaks through ginseng-cell wall, is brought in medicine juice by effective ingredient in Radix Ginseng.
As optimization, the when 9. step is concentrated, by vacuum by the medicine juice suction concentration pan of liquid receiver, carries out concentrating under reduced pressure.
As optimization, the when 9. step is concentrated, adopt film condensing device, concentrate, by the clear water of film condensing device, give over to 2., 3., 4. step to add water use, gained concentrated solution through boiling, airtight fill, sterilizing is finished product sugar-free compound colla corii asini pulp.Film condensing device is usually used in desalinization, and for people during desalinization is water by semipermeable membrane, is blocked in the high concentration saline before semipermeable membrane and is given it up; And present invention utilizes the high concentration medicine juice before being blocked in semipermeable membrane, also do not wasted by the water of semipermeable membrane simultaneously.Design like this, energy consumption is low, survivable medicament effective component.
As optimization, 1. the walk: 45% ethanol of Radix Ginseng section immersion 60 ~ 80 weight portion, pulls out, put into plodder, then put back to together with residue in ethanol by juice, finally add in high-pressure alcohol extraction tank more together after 2 hours.Design like this, ginseng-cell sucks after ethanol, then uses plodder, contributes to squeeze crack ginseng-cell wall, is convenient to the and 2. walks ethanol and break through ginseng-cell wall, discharge the active ingredient in Radix Ginseng better.
Sugar-free compound colla corii asini pulp of the present invention is applicable to hyperglycemia population and diabetic to take, its preparation technology takes the mixed extraction new technology of height-normal pressure alcohol extraction/water extraction to famous and precious raw material, at utmost extract the active ingredients such as Radix Ginseng, the effective ingredient of each raw material components is not run off.
Accompanying drawing explanation
Below in conjunction with accompanying drawing, the equipment that the present invention uses is described further:
Fig. 1 is the structural representation of high-pressure alcohol extraction tank and new medicine extractor.
Fig. 2 is the schematic diagram utilizing film condensing device concentrated medicament.
In figure: 1 be high-pressure alcohol extraction tank, 2 be visor, 3 be closed charging aperture, 4 be Pressure gauge, 5 be intake valve, 6 be tank body, 7 be condenser, 8 be vapour jacket, 9 be slag notch, 10 be baiting valve, 11 be film condensing device, 12 be medicine juice feed pipe, 13 be outlet pipe, 15 be piston pump for medicine juice discharge nozzle, 14 after concentrated.
Detailed description of the invention
Embodiment 1: embodiment 1: 1.. take the Radix Ginseng of 55kg, after section, immerse 45% ethanol (namely volumetric concentration is the ethanol water of 45%) of 60kg, then add in high-pressure alcohol extraction tank 1, then to be pressurizeed 10kgf/cm to inflated with nitrogen in high-pressure alcohol extraction tank 1 by air pump
2, soak 2 hours; Wherein high-pressure alcohol extraction tank 1 top is provided with closed charging aperture 3, Pressure gauge 4 and intake valve 5, and is furnished with air pump (not shown), as shown in Figure 1.
2.. by aforesaid weight ratio, take the Radix Rehmanniae Preparata of 410kg, the Radix Codonopsis of 420kg, the Fructus Crataegi of 190kg, add in the tank body of new medicine extractor, then add water 5000kg, soak 1.5 hours, after closed tank, pass into Steam Heating, medical material after immersion is boiled, open the circulation waterway of tank body evaporator overhead condenser simultaneously, again the material in high-pressure alcohol extraction tank 1 is put into fast the tank body 6 of new medicine extractor, high-pressure alcohol extraction tank 1 side is provided with visor 2, observed by this visor 2, material in high-pressure alcohol extraction tank 1 only can be put into the tank body 6 of new medicine extractor by operator, prevent because nitrogen enters tank body 6, the pressure in tank body 6 is caused to raise, continue heated and boiled, after being greater than 1.04 to medicine juice proportion, release first time medicine juice, stand-by,
Wherein new medicine extractor comprises tank body 6, and tank body 6 top is provided with condenser 7, and tank body 6 sidewall is provided with vapour jacket 8, is provided with slag notch 9 bottom tank body 6, and its top is provided with closed charging aperture 3; Communicated with tank body 6 by baiting valve 10 bottom described high-pressure alcohol extraction tank 1, as shown in Figure 1.
3.. then add water 3000kg for the second time, and heated and boiled, when being greater than 1.01 to medicine juice proportion, releases second time medicine juice, stand-by;
4.. then add water 1800kg for the third time, and heated and boiled, reaches after more than 1.005 to medicine juice proportion, releases third time medicine juice;
5.. three medicine juice pumps are squeezed into seperator together and is separated, obtain hybrid separation liquid, before being separated, medicine juice funnel adds a gauze layer, and separating rate must not be greater than 16 kg/min, 30 minutes row's primary slags;
6.. open vacuum, when triple effect vacuum reaches 0.06MPa, hybrid separation liquid vacuum is sucked in triple effect evaporator and evaporates, be evaporated to medicine juice proportion and reach after between 1.05-1.06, release stand-by, obtain medicine juice;
7.. get the Colla Corii Asini of 125kg and the water of 5 times of Colla Corii Asini weight, add in jacketed pan, after being heated to boil, Colla Corii Asini is added in pot and constantly stirs, make it to dissolve uniformly after glue, turn glue foam and impurity defecation with foam, then add the Stevia rebaudiana (Bertoni) Hemsl extract of 25kg and the lemon grass extract of 20kg, obtain the glue that proportion is greater than 1.12;
8.. 6. walk gained medicine juice and the by the and 7. walk gained gum sugar liquid, squeezing into pump has in the settling box of heating function, slowly adds sodium carbonate liquor, pH value is adjusted to 5.5-6.5, heated and boiled 15-20 minute, leave standstill more than 16 hours, be then separated by the mixed liquor seperator after precipitation, every 30 minutes deslagginves once, mixed liquor enters turnover barrel after being separated, carry out fine straining, pressure is no more than 0.1MPa, and the medicine juice after fine straining enters liquid receiver;
9.. the medicine juice of liquid receiver is concentrated into relative density more than 1.085, slowly adds sodium carbonate liquor, pH value is adjusted to 4.5-6.5, be heated to boil, 100 DEG C are boiled 15 minutes; Finally squeezed into by medicine juice pump in the finished product liquid receiver of band 100 mesh sieve, covered and enclosed, be no more than 6 hours standing time, fill, namely sterilizing obtains sugar-free compound colla corii asini pulp A.
The Fructus Crataegi of the Radix Ginseng of the Colla Corii Asini of embodiment 2: raw material is changed into: 127.5kg, 45% ethanol of 70kg, 60kg, the Radix Rehmanniae Preparata of 420kg, the Radix Codonopsis of 430kg and 170kg, add the Stevia rebaudiana (Bertoni) Hemsl extract of 30kg and the lemon grass extract of 10kg again, obtain the glue that proportion is greater than 1.12; The when 9. step is concentrated, adopts film condensing device, concentrates, as shown in Figure 2, by the clear water of film condensing device 11, give over to 2., 3., 4. step to add water use, gained concentrated solution through boiling, airtight fill, sterilizing is finished product sugar-free compound colla corii asini pulp B, and all the other techniques as described in Example 1, are omited.
The Radix Ginseng of the Colla Corii Asini of embodiment 3: raw material is changed into: 130kg, 45% ethanol of 80kg, 65kg, the Radix Rehmanniae Preparata of 430kg, the Radix Codonopsis of 410kg, the Fructus Crataegi of 180kg, add the Stevia rebaudiana (Bertoni) Hemsl extract of 20kg and the lemon grass extract of 15kg again, obtain the glue that proportion is greater than 1.12; 1. the walk: Radix Ginseng section immersion 45% ethanol was pulled out after 2 hours, put into the extruding of screw extruder (not shown), then juice is put back in ethanol together with residue, finally add in high-pressure alcohol extraction tank 1 more together, all the other techniques as described in Example 1, obtain sugar-free compound colla corii asini pulp C.
Contrast experiment: choose same batch of ginseng raw material, be divided into four groups, respectively by technique and FUFANG EJIAO JIANG conventional fabrication process production FUFANG EJIAO JIANG described in embodiment 1,2,3, produces Radix Ginseng residue A, Radix Ginseng residue B, Radix Ginseng residue C, Radix Ginseng residue D respectively.Detect ginsenoside (Ginsenoside) total content in above-mentioned four kinds of Radix Ginseng residues respectively, obtain following table.
Upper table illustrates, the utilization rate of the present invention to Radix Ginseng is higher.
Claims (4)
1. a preparation technology for sugar-free compound colla corii asini pulp, comprises the steps:
1.. take the Radix Ginseng of 55-65 weight portion, after section, immerse 45% ethanol of 60 ~ 80 weight portions, then add in high-pressure alcohol extraction tank, then by air pump to inflating pressure 8 ~ 10kgf/cm in high-pressure alcohol extraction tank
2, soak 2 hours; Wherein high-pressure alcohol extraction tank top is provided with closed charging aperture, Pressure gauge and intake valve, and is furnished with air pump;
2.. by aforesaid weight ratio, take the Radix Rehmanniae Preparata of 410-430 weight portion, the Radix Codonopsis of 410-430 weight portion, the Fructus Crataegi of 170-190 weight portion, add in the tank body of new medicine extractor, then add water 5000 weight portions, soak 0.5-2.0 hour, after closed tank, pass into Steam Heating, medical material after immersion is boiled, opens the circulation waterway of tank body evaporator overhead condenser simultaneously, then the material in high-pressure alcohol extraction tank is put into fast the tank body of new medicine extractor, continue heated and boiled, after being greater than 1.04 to medicine juice proportion, release first time medicine juice, stand-by;
Wherein new medicine extractor comprises tank body, and tank body top is provided with condenser, and tank wall is provided with vapour jacket, and tank base is provided with slag notch, and its top is provided with closed charging aperture; Described high-pressure alcohol extraction pot bottom is communicated with tank body by baiting valve;
3.. then add water 3000 weight portions for the second time, and heated and boiled, when being greater than 1.01 to medicine juice proportion, releases second time medicine juice, stand-by;
4.. then add water 1800 weight portions for the third time, and heated and boiled, reaches after more than 1.005 to medicine juice proportion, releases third time medicine juice;
5.. three medicine juice pumps are squeezed into seperator together and is separated, obtain hybrid separation liquid, before being separated, medicine juice funnel adds a gauze layer, and separating rate must not be greater than 16 kg/min, 30 minutes row's primary slags;
6.. open vacuum, when triple effect vacuum reaches 0.06MPa, hybrid separation liquid vacuum is sucked in triple effect evaporator and evaporates, be evaporated to medicine juice proportion and reach after between 1.05-1.06, release stand-by, obtain medicine juice;
7.. get the Colla Corii Asini of 125-130 weight portion and the water of 5 times of Colla Corii Asini weight, add in jacketed pan, after being heated to boil, Colla Corii Asini is added in pot and constantly stirs, make it to dissolve uniformly after glue, turn glue foam and impurity defecation with foam, then add the Stevia rebaudiana (Bertoni) Hemsl extract of 20-30 weight portion and the lemon grass extract of 10-20 weight portion, obtain the glue that proportion is greater than 1.12;
8.. 6. walk gained medicine juice and the by the and 7. walk gained glue, squeezing into pump has in the settling box of heating function, slowly adds sodium carbonate liquor, pH value is adjusted to 5.5-6.5, heated and boiled 15-20 minute, leave standstill more than 16 hours, be then separated by the mixed liquor seperator after precipitation, every 30 minutes deslagginves once, mixed liquor enters turnover barrel after being separated, carry out fine straining, pressure is no more than 0.1MPa, and the medicine juice after fine straining enters liquid receiver;
9.. the medicine juice of liquid receiver is concentrated into relative density more than 1.085, slowly adds sodium carbonate liquor, pH value is adjusted to 4.5-6.5, be heated to boil, 100 DEG C are boiled 15 minutes; Finally squeezed into by medicine juice pump in the finished product liquid receiver of band 100 mesh sieve, covered and enclosed, is no more than 6 hours standing time, fill, sterilizing and get final product.
2. the preparation technology of sugar-free compound colla corii asini pulp according to claim 1, is characterized in that: the when 9. step is concentrated, by vacuum by the medicine juice suction concentration pan of liquid receiver, carries out concentrating under reduced pressure.
3. the preparation technology of sugar-free compound colla corii asini pulp according to claim 1, it is characterized in that: the when 9. step is concentrated, adopt film condensing device, concentrate, by the clear water of film condensing device, give over to 2., 3., 4. step to add water use, gained concentrated solution through boiling, airtight fill, sterilizing is finished product sugar-free compound colla corii asini pulp.
4. the preparation technology of sugar-free compound colla corii asini pulp according to claim 1 or 2 or 3, it is characterized in that: 1. the walk: 45% ethanol of Radix Ginseng section immersion 60 ~ 80 weight portion, pull out after 2 hours, put into plodder, then juice is put back in ethanol together with residue, finally add in high-pressure alcohol extraction tank more together.
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| CN105395888A (en) * | 2015-12-16 | 2016-03-16 | 湖南东健药业有限公司 | Preparation method for compound donkey-hide gelatin syrup |
| CN106333039A (en) * | 2016-08-24 | 2017-01-18 | 湖北康源药业有限公司 | Chocolate-containing instant donkey-hide gelatin food and preparation method thereof |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1168805A (en) * | 1997-06-20 | 1997-12-31 | 山东东阿阿胶股份有限公司 | Medicine for enriching the blood |
| CN1682978A (en) * | 2005-02-07 | 2005-10-19 | 贵州三力制药有限责任公司 | Compound ass-hide gelatin soft capsule and its preparing method |
| CN101112448A (en) * | 2007-08-03 | 2008-01-30 | 司家勇 | Donkey-hide gelatin composition having immunity improving effect and method of making the same |
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Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1168805A (en) * | 1997-06-20 | 1997-12-31 | 山东东阿阿胶股份有限公司 | Medicine for enriching the blood |
| CN1682978A (en) * | 2005-02-07 | 2005-10-19 | 贵州三力制药有限责任公司 | Compound ass-hide gelatin soft capsule and its preparing method |
| CN101112448A (en) * | 2007-08-03 | 2008-01-30 | 司家勇 | Donkey-hide gelatin composition having immunity improving effect and method of making the same |
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