CN103641667B - A kind of area synergist and preparation method thereof - Google Patents
A kind of area synergist and preparation method thereof Download PDFInfo
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- CN103641667B CN103641667B CN201310582614.0A CN201310582614A CN103641667B CN 103641667 B CN103641667 B CN 103641667B CN 201310582614 A CN201310582614 A CN 201310582614A CN 103641667 B CN103641667 B CN 103641667B
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- 238000002360 preparation method Methods 0.000 title claims abstract description 11
- 239000000843 powder Substances 0.000 claims abstract description 36
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical class O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 claims abstract description 13
- 239000002994 raw material Substances 0.000 claims abstract description 7
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 claims abstract description 4
- APUPEJJSWDHEBO-UHFFFAOYSA-P ammonium molybdate Chemical compound [NH4+].[NH4+].[O-][Mo]([O-])(=O)=O APUPEJJSWDHEBO-UHFFFAOYSA-P 0.000 claims abstract description 4
- 235000018660 ammonium molybdate Nutrition 0.000 claims abstract description 4
- 239000011609 ammonium molybdate Substances 0.000 claims abstract description 4
- 229940010552 ammonium molybdate Drugs 0.000 claims abstract description 4
- BFNBIHQBYMNNAN-UHFFFAOYSA-N ammonium sulfate Chemical compound N.N.OS(O)(=O)=O BFNBIHQBYMNNAN-UHFFFAOYSA-N 0.000 claims abstract description 4
- 229910052921 ammonium sulfate Inorganic materials 0.000 claims abstract description 4
- 235000011130 ammonium sulphate Nutrition 0.000 claims abstract description 4
- KGBXLFKZBHKPEV-UHFFFAOYSA-N boric acid Chemical compound OB(O)O KGBXLFKZBHKPEV-UHFFFAOYSA-N 0.000 claims abstract description 4
- 239000004327 boric acid Substances 0.000 claims abstract description 4
- GVPFVAHMJGGAJG-UHFFFAOYSA-L cobalt dichloride Chemical compound [Cl-].[Cl-].[Co+2] GVPFVAHMJGGAJG-UHFFFAOYSA-L 0.000 claims abstract description 4
- -1 compound sodium nitrophenolate Chemical class 0.000 claims abstract description 4
- 229910000402 monopotassium phosphate Inorganic materials 0.000 claims abstract description 4
- 235000019796 monopotassium phosphate Nutrition 0.000 claims abstract description 4
- LGQLOGILCSXPEA-UHFFFAOYSA-L nickel sulfate Chemical compound [Ni+2].[O-]S([O-])(=O)=O LGQLOGILCSXPEA-UHFFFAOYSA-L 0.000 claims abstract description 4
- 229910000363 nickel(II) sulfate Inorganic materials 0.000 claims abstract description 4
- PJNZPQUBCPKICU-UHFFFAOYSA-N phosphoric acid;potassium Chemical compound [K].OP(O)(O)=O PJNZPQUBCPKICU-UHFFFAOYSA-N 0.000 claims abstract description 4
- 239000011591 potassium Substances 0.000 claims abstract description 4
- 229910052700 potassium Inorganic materials 0.000 claims abstract description 4
- NWONKYPBYAMBJT-UHFFFAOYSA-L zinc sulfate Chemical compound [Zn+2].[O-]S([O-])(=O)=O NWONKYPBYAMBJT-UHFFFAOYSA-L 0.000 claims abstract description 4
- 229910000368 zinc sulfate Inorganic materials 0.000 claims abstract description 4
- 229960001763 zinc sulfate Drugs 0.000 claims abstract description 4
- ZGTMUACCHSMWAC-UHFFFAOYSA-L EDTA disodium salt (anhydrous) Chemical compound [Na+].[Na+].OC(=O)CN(CC([O-])=O)CCN(CC(O)=O)CC([O-])=O ZGTMUACCHSMWAC-UHFFFAOYSA-L 0.000 claims abstract description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 10
- 239000000203 mixture Substances 0.000 claims description 8
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 6
- 229910021536 Zeolite Inorganic materials 0.000 claims description 6
- 239000010457 zeolite Substances 0.000 claims description 6
- 235000017166 Bambusa arundinacea Nutrition 0.000 claims description 3
- 235000017491 Bambusa tulda Nutrition 0.000 claims description 3
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 3
- 229920002134 Carboxymethyl cellulose Polymers 0.000 claims description 3
- 241001312402 Helvella corium Species 0.000 claims description 3
- 240000000233 Melia azedarach Species 0.000 claims description 3
- 244000062730 Melissa officinalis Species 0.000 claims description 3
- 235000010654 Melissa officinalis Nutrition 0.000 claims description 3
- 244000082204 Phyllostachys viridis Species 0.000 claims description 3
- 235000015334 Phyllostachys viridis Nutrition 0.000 claims description 3
- 244000294611 Punica granatum Species 0.000 claims description 3
- 235000014360 Punica granatum Nutrition 0.000 claims description 3
- 244000269722 Thea sinensis Species 0.000 claims description 3
- 240000001866 Vernicia fordii Species 0.000 claims description 3
- 229960000892 attapulgite Drugs 0.000 claims description 3
- 239000011425 bamboo Substances 0.000 claims description 3
- 238000010009 beating Methods 0.000 claims description 3
- VSGNNIFQASZAOI-UHFFFAOYSA-L calcium acetate Chemical compound [Ca+2].CC([O-])=O.CC([O-])=O VSGNNIFQASZAOI-UHFFFAOYSA-L 0.000 claims description 3
- 239000001639 calcium acetate Substances 0.000 claims description 3
- 235000011092 calcium acetate Nutrition 0.000 claims description 3
- 229960005147 calcium acetate Drugs 0.000 claims description 3
- 229910052799 carbon Inorganic materials 0.000 claims description 3
- 239000001768 carboxy methyl cellulose Substances 0.000 claims description 3
- 235000010948 carboxy methyl cellulose Nutrition 0.000 claims description 3
- 239000008112 carboxymethyl-cellulose Substances 0.000 claims description 3
- 239000012153 distilled water Substances 0.000 claims description 3
- 238000001914 filtration Methods 0.000 claims description 3
- 238000009472 formulation Methods 0.000 claims description 3
- 238000010438 heat treatment Methods 0.000 claims description 3
- 238000009413 insulation Methods 0.000 claims description 3
- 239000010977 jade Substances 0.000 claims description 3
- 239000000865 liniment Substances 0.000 claims description 3
- 239000002105 nanoparticle Substances 0.000 claims description 3
- 229910052625 palygorskite Inorganic materials 0.000 claims description 3
- 108010064470 polyaspartate Proteins 0.000 claims description 3
- 239000001267 polyvinylpyrrolidone Substances 0.000 claims description 3
- 229920000036 polyvinylpyrrolidone Polymers 0.000 claims description 3
- 235000013855 polyvinylpyrrolidone Nutrition 0.000 claims description 3
- 238000007873 sieving Methods 0.000 claims description 3
- 235000019832 sodium triphosphate Nutrition 0.000 claims description 3
- 239000007787 solid Substances 0.000 claims description 3
- 239000007921 spray Substances 0.000 claims description 3
- 238000003756 stirring Methods 0.000 claims description 3
- 239000000052 vinegar Substances 0.000 claims description 3
- 235000021419 vinegar Nutrition 0.000 claims description 3
- 238000001354 calcination Methods 0.000 claims description 2
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 abstract description 28
- 239000004202 carbamide Substances 0.000 abstract description 14
- 235000013877 carbamide Nutrition 0.000 abstract description 14
- 239000003337 fertilizer Substances 0.000 abstract description 7
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 abstract description 6
- 229910052757 nitrogen Inorganic materials 0.000 abstract description 3
- 201000010099 disease Diseases 0.000 abstract description 2
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 abstract description 2
- 241001122767 Theaceae Species 0.000 abstract 1
- 239000002689 soil Substances 0.000 description 6
- WCUXLLCKKVVCTQ-UHFFFAOYSA-M Potassium chloride Chemical compound [Cl-].[K+] WCUXLLCKKVVCTQ-UHFFFAOYSA-M 0.000 description 4
- 240000007594 Oryza sativa Species 0.000 description 3
- 235000007164 Oryza sativa Nutrition 0.000 description 3
- 230000014075 nitrogen utilization Effects 0.000 description 3
- 235000009566 rice Nutrition 0.000 description 3
- PNNCWTXUWKENPE-UHFFFAOYSA-N [N].NC(N)=O Chemical compound [N].NC(N)=O PNNCWTXUWKENPE-UHFFFAOYSA-N 0.000 description 2
- 239000008280 blood Substances 0.000 description 2
- 210000004369 blood Anatomy 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 239000001103 potassium chloride Substances 0.000 description 2
- 235000011164 potassium chloride Nutrition 0.000 description 2
- 238000001179 sorption measurement Methods 0.000 description 2
- 238000012271 agricultural production Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 235000019994 cava Nutrition 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000000618 nitrogen fertilizer Substances 0.000 description 1
- 235000015097 nutrients Nutrition 0.000 description 1
- 230000008635 plant growth Effects 0.000 description 1
- 238000010298 pulverizing process Methods 0.000 description 1
- SRFKWQSWMOPVQK-UHFFFAOYSA-K sodium;2-[2-[bis(carboxylatomethyl)amino]ethyl-(carboxymethyl)amino]acetate;iron(2+) Chemical compound [Na+].[Fe+2].OC(=O)CN(CC([O-])=O)CCN(CC([O-])=O)CC([O-])=O SRFKWQSWMOPVQK-UHFFFAOYSA-K 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
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- Fertilizers (AREA)
Abstract
The invention discloses a kind of area synergist and preparation method thereof, it is made up of the raw material of following weight portion: ammonium sulfate 150-200, potassium dihydrogen phosphate 120-160, ammonium molybdate 10-15, boric acid 25-35, cobalt chloride 5-10, nickel sulfate 5-10, disodiumedetate 20-30, zinc sulfate 30-40, Entermorpha dry powder 20-30, potassium fulvate 10-15, volcanic ash 15-25, tea seed cake powder 10-15, modified zeolite powder 50-100, compound sodium nitrophenolate 3-6; Synergist of the present invention can significantly improve fertilizer efficiency and the nitrogen use efficiency of carbamide, extend the urea efficiency phase, promote crop fast-growth, improve drought resisting, anti-disease ability, notable volume increase and Crop Improvement quality, and consumption is few, province topdresses, saving of labor economizes fertilizer, reduce planting cost, improve the economic benefit of crop.
Description
Technical field
The present invention relates to a kind of area synergist and preparation method thereof, belong to technical field of agricultural fertilizers.
Background technology
Carbamide is the chemical nitrogen fertilizer that China is important, also it is affect crop yield and the most important nutrient of quality, carbamide is not easily by adsorption by soil, in soil, carbamide only has about 20 by adsorption by soil, and not firm, easily outflow with water, cause that the nitrogen utilization efficiency of carbamide is low, Total Nitrogen loss is serious, thus affecting plant growth and improving planting cost. Therefore, how to improve blood urea nitrogen utilization rate and fertilizer efficiency is problem demanding prompt solution in the agricultural production of current China.
Summary of the invention
Present invention aims to the deficiencies in the prior art, it is provided that a kind of area synergist and preparation method thereof, this synergist and carbamide composite application are remarkably improved blood urea nitrogen utilization rate and fertilizer efficiency.
For achieving the above object, the technical solution used in the present invention is as follows:
A kind of area synergist, is made up of the raw material of following weight portion: ammonium sulfate 150-200, potassium dihydrogen phosphate 120-160, ammonium molybdate 10-15, boric acid 25-35, cobalt chloride 5-10, nickel sulfate 5-10, sodium iron ethylenediaminetetraacetate 20-30, zinc sulfate 30-40, Entermorpha dry powder 20-30, potassium fulvate 10-15, volcanic ash 15-25, tea seed cake powder 10-15, modified zeolite powder 50-100, compound sodium nitrophenolate 3-6;
The preparation method of described modified zeolite powder is as follows: (a) takes calcining 2-3h at zeolite is placed in 640-680 DEG C, puts into micro-decoction 20-30min that boils in the hydrochloric acid solution that concentration is 10-15%, filter after being cooled to room temperature, filtering residue distilled water wash is clean, dry, pulverize, cross 100-150 mesh sieve; (b) sieve after zeolite powder add the Punica granatum L. corium farinosum of the offal of 3-5%, the Melia azedarach L. corium farinosum of 2-3%, the Herba Ocimi (Herba Ocimi Pilosi) leaf powder of 1-2%, the Aleurites fordii Hemsl. shell powder of 3-4% and 2-3%, mix homogeneously, then the serosity that solid content is 50-60% is made in water making beating, heating in water bath is to 80-90 DEG C, insulation 40-60min, add the Bamboo vinegar solution of the attapulgite of 5-10%, the nano-sized carbon of 3-5%, the calcium acetate of 2-3%, the sodium tripolyphosphate of 4-6%, the polyvinylpyrrolidone of 3-5%, the carboxymethyl cellulose of 1-2% and 2-3%, speed lapping 15-20min, is spray dried to powder;C () above-mentioned prepared powder adds the jade powder of poly-aspartate of 2-3%, the essential balm of 1-2% and 2-3%, stir, dry.
Preparation method: crushed respectively by above-mentioned raw materials by formulation ratio, crosses 100-150 mesh sieve, is then sent in blender by the powder after sieving and is sufficiently mixed uniformly, is re-fed in granulating disc pelletize, dries and is finished product.
Using method: take the synergist of weight of urea 2-3% and mix thoroughly with carbamide, uniformly applies field, and ploughs under in earth and mix with soil.
Beneficial effects of the present invention:
Synergist of the present invention can significantly improve fertilizer efficiency and the nitrogen use efficiency of carbamide, extend the urea efficiency phase, promote crop fast-growth, improve drought resisting, anti-disease ability, notable volume increase and Crop Improvement quality, and consumption is few, province topdresses, saving of labor economizes fertilizer, reduce planting cost, improve the economic benefit of crop.
Detailed description of the invention
A kind of area synergist, is made up of the raw material of following weight (kg): ammonium sulfate 160, potassium dihydrogen phosphate 160, ammonium molybdate 10, boric acid 30, cobalt chloride 10, nickel sulfate 10, disodiumedetate 30, zinc sulfate 40, Entermorpha dry powder 25, potassium fulvate 10, volcanic ash 20, tea seed cake powder 15, modified zeolite powder 70, compound sodium nitrophenolate 5;
The preparation method of described modified zeolite powder is as follows: (a) takes zeolite and be placed at 660 DEG C and calcine 3h, puts into micro-decoction 20min that boils in the hydrochloric acid solution that concentration is 15%, filter after being cooled to room temperature, and filtering residue is clean with distilled water wash, dries, and 150 mesh sieves are crossed in pulverizing; (b) sieve after zeolite powder add 4% offal, 2% Melia azedarach L. corium farinosum, the Herba Ocimi (Herba Ocimi Pilosi) leaf powder of 1%, the Aleurites fordii Hemsl. shell powder of 3 and 3% Punica granatum L. corium farinosum, mix homogeneously, then the serosity that solid content is 55% is made in water making beating, heating in water bath is to 90 DEG C, insulation 50min, add 8% attapulgite, 4% nano-sized carbon, 2% calcium acetate, 5% sodium tripolyphosphate, the polyvinylpyrrolidone of 4%, the carboxymethyl cellulose of 1.5% and 2% Bamboo vinegar solution, speed lapping 15min, be spray dried to powder; (c) above-mentioned prepared powder add poly-aspartate of 3%, the essential balm of 2% and 2% jade powder, stir, dry.
Preparation method: crushed respectively by above-mentioned raw materials by formulation ratio, crosses 150 mesh sieves, is then sent in blender by the powder after sieving and is sufficiently mixed uniformly, is re-fed in granulating disc pelletize, dries and is finished product.
Field test:
Adopt great Qu matching type, set 2 process altogether. 1. trial zone: area 2000m2, May 10 in 2011 is whole when raking the soil level, and mu executes carbamide 12.5kg, diammonium 6.7kg, potassium chloride 3.3kg, synergist 2.8kg, and the later stage does not topdress. 2. check plot: area 2000m2, on May 10th, 2011 is whole when raking the soil level, and mu executes carbamide 17kg, diammonium 6.7kg, potassium chloride 3.3kg, and June 14 chased after carbamide 5kg/ mu. Rice varieties is excellent No. 1 of K two, and April 14 soaked seed, and April 20 was sowed, length of time rice seedlings grow 30d. Honda rice transplanting on May 20, row cave from 30cm*20cm,
Square metre 20 caves, every cave 3 post, field management is consistent. Result of the test is as shown in table 1:
Table 1
Claims (2)
1. an area synergist, it is characterized in that, be made up of the raw material of following weight portion: ammonium sulfate 150-200, potassium dihydrogen phosphate 120-160, ammonium molybdate 10-15, boric acid 25-35, cobalt chloride 5-10, nickel sulfate 5-10, disodiumedetate 20-30, zinc sulfate 30-40, Entermorpha dry powder 20-30, potassium fulvate 10-15, volcanic ash 15-25, tea seed cake powder 10-15, modified zeolite powder 50-100, compound sodium nitrophenolate 3-6;
The preparation method of described modified zeolite powder is as follows: (a) takes calcining 2-3h at zeolite is placed in 640-680 DEG C, puts into micro-decoction 20-30min that boils in the hydrochloric acid solution that concentration is 10-15%, filter after being cooled to room temperature, filtering residue distilled water wash is clean, dry, pulverize, cross 100-150 mesh sieve; (b) sieve after zeolite powder add the Punica granatum L. corium farinosum of the offal of 3-5%, the Melia azedarach L. corium farinosum of 2-3%, the Herba Ocimi (Herba Ocimi Pilosi) leaf powder of 1-2%, the Aleurites fordii Hemsl. shell powder of 3-4% and 2-3%, mix homogeneously, then the serosity that solid content is 50-60% is made in water making beating, heating in water bath is to 80-90 DEG C, insulation 40-60min, add the Bamboo vinegar solution of the attapulgite of 5-10%, the nano-sized carbon of 3-5%, the calcium acetate of 2-3%, the sodium tripolyphosphate of 4-6%, the polyvinylpyrrolidone of 3-5%, the carboxymethyl cellulose of 1-2% and 2-3%, speed lapping 15-20min, is spray dried to powder; C () above-mentioned prepared powder adds the jade powder of poly-aspartate of 2-3%, the essential balm of 1-2% and 2-3%, stir, dry.
2. the preparation method of an area synergist as claimed in claim 1; it is characterized in that comprising the following steps: crushed respectively by above-mentioned raw materials by formulation ratio; cross 100-150 mesh sieve; then being sent into by the powder after sieving is sufficiently mixed uniformly in blender; it is re-fed in granulating disc pelletize, dries and be finished product.
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| CN103641667B true CN103641667B (en) | 2016-06-08 |
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| CN105175137A (en) * | 2015-09-16 | 2015-12-23 | 安徽盛农农业集团有限公司 | Grape planting fertilizer capable of adsorbing microorganisms and preparation method thereof |
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| CN105175136A (en) * | 2015-09-16 | 2015-12-23 | 安徽盛农农业集团有限公司 | Adsorption nitrogen fertilizer with modified natural zeolite and preparation method thereof |
| CN105198576A (en) * | 2015-09-16 | 2015-12-30 | 安徽盛农农业集团有限公司 | Modified ammoniacal nitrogen fertilizer for rice in seedling breeding period and preparation method thereof |
| CN105175139A (en) * | 2015-09-16 | 2015-12-23 | 安徽盛农农业集团有限公司 | Environment-friendly fertilizer applied in tomato seedling stage and preparation method thereof |
| CN105198577A (en) * | 2015-09-16 | 2015-12-30 | 安徽盛农农业集团有限公司 | Efficient enzyme environment-friendly fertilizer and preparation method thereof |
| CN105237174A (en) * | 2015-09-16 | 2016-01-13 | 安徽盛农农业集团有限公司 | Efficient nitrogen fertilizer obtained through cracking of straw powder and preparation method thereof |
| CN105237292A (en) * | 2015-09-16 | 2016-01-13 | 安徽盛农农业集团有限公司 | Efficient microbial fertilizer applied to plant corn and preparation method thereof |
| CN105175185A (en) * | 2015-09-16 | 2015-12-23 | 安徽盛农农业集团有限公司 | Grape planting soil improving fertilizer and preparation method thereof |
| CN105237176A (en) * | 2015-09-16 | 2016-01-13 | 安徽盛农农业集团有限公司 | Rice seedling-stage growth-assissting ammonium nitrogen fertilizer and preparation method thereof |
| CN105237313A (en) * | 2015-09-16 | 2016-01-13 | 安徽盛农农业集团有限公司 | Natural mineral-powder environment-friendly type fertilizer and preparation method thereof |
| CN105198679A (en) * | 2015-09-16 | 2015-12-30 | 安徽盛农农业集团有限公司 | Pustulation period corn sugar increasing environment-friendly fertilizer and preparation method thereof |
| CN108329151B (en) * | 2018-04-24 | 2021-05-28 | 武汉皓达农业科技有限公司 | Fertilizer synergist, preparation method and application thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN1064943C (en) * | 1997-03-28 | 2001-04-25 | 寇庆德 | Urea synergist |
| CN101391928B (en) * | 2008-11-12 | 2011-07-20 | 秦皇岛领先科技发展有限公司 | Fertilizer composition and use thereof |
| CN101638349A (en) * | 2009-08-30 | 2010-02-03 | 张永茂 | Novel slow-release drought-resisting nitrogenous fertilizer |
| CN102503737A (en) * | 2011-12-02 | 2012-06-20 | 青岛丰泰海洋生物科技有限公司 | Preparation method of synergistic nitrogen fertilizer |
| CN102515968A (en) * | 2012-01-04 | 2012-06-27 | 广西新方向化学工业有限公司 | Multifunctional synergistic nitrogen fertilizer and preparation method thereof |
| CN102936168A (en) * | 2012-10-30 | 2013-02-20 | 安徽省文胜肥业有限责任公司 | Ecological nitrogenous fertilizer and preparation method thereof |
| CN102936167B (en) * | 2012-10-30 | 2014-04-16 | 安徽省文胜肥业有限责任公司 | Polymorphic nitrogenous fertilizer and preparation method thereof |
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