CN103613408A - Low-temperature rose-red glaze ceramic product and manufacturing method thereof - Google Patents
Low-temperature rose-red glaze ceramic product and manufacturing method thereof Download PDFInfo
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- CN103613408A CN103613408A CN201310584382.2A CN201310584382A CN103613408A CN 103613408 A CN103613408 A CN 103613408A CN 201310584382 A CN201310584382 A CN 201310584382A CN 103613408 A CN103613408 A CN 103613408A
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Abstract
The invention relates to a ceramic product and a manufacturing method thereof, and specifically relates to a low-temperature rose-red glaze ceramic product and a manufacturing method thereof. The low-temperature rose-red glaze ceramic product is prepared by the following steps: applying red slurry on the surface of a ceramic blank in a glazing way, carrying out high-temperature biscuiting after the red slurry is dried, wherein the biscuiting temperature is 1150 DEG C-1200 DEG C; and applying rose-red glaze for the ceramic blank piece by adopting a glazing method after high-temperature biscuiting, carrying out low-temperature glaze firing after the rose-red glaze is dried, adopting roller kiln oxidizing flame firing at a firing temperature of 850 DEG C-950 DEG C, and discharging out of the kiln after firing. The low-temperature rose-red glaze ceramic product provided by the invention adopts a firing process of high-temperature biscuiting and low-temperature glaze firing, so that the product has high strength and high compactness and avoids pin holes, glaze shrinkage, orange glaze and blank blistering; and moreover, glaze color is full of third dimension and ceramics fired in different batches are stable in color.
Description
Technical field
The present invention relates to a kind of ceramic and manufacture method thereof, be specially low temperature rose red glaze ceramic products and manufacture method thereof.
Background technology
Current conventional rose red glaze goods, generally on ceramic form, directly glazing is burnt till, firing temperature is generally more than 1000 ℃, because coexisting under hot conditions, glaze and ceramic form fire, easily produce the defects such as pin hole, contracting glaze, orange peel glaze, glaze colours be inhomogeneous, and each color of firing batch products has some difference.
Summary of the invention
In order to address the above problem, the invention provides a kind of quality better, the rose red glaze ceramic products of colour stable, concrete technical scheme is:
Low temperature rose red glaze ceramic products, by following steps system: to soak the mode of glaze, execute red slurry on ceramic body surface, after red slurry is dry, carry out high temperature biscuiting, biscuiting temperature is 1150 ℃~1200 ℃;
Adopt the method for soaking glaze to execute rhodo glaze the ceramic form after high temperature biscuiting again, low temperature sinter after dry, adopts roller kiln oxydizing flame to burn till, and firing temperature is 850 ℃~950 ℃, burns till kiln discharge.
Described redness slurry, take feldspar, Tu, Dehua, Suzhou china clay, frit, bright red pigment is raw material, its each red slurry raw material weight umber is: 6~8 parts of feldspars, 20~25 parts, Suzhou soil, 45~50 parts of Dehua china clay, 7~10 parts of frits, 13~18 parts of bright red pigments.
Above-mentioned red slurry raw material is entered to ball mill cylinder ball milling by weight ratio with ball, water, red slurry raw material: ball: water=1:1.6:1.6, through 15 hours ball millings, goes out cylinder and cross 120 mesh sieves and make red slurry.
Described rhodo glaze take that rhodo glaze frit, feldspar, Suzhou soil, bright red pigment, atom are red, zirconium iron pink, melanochrome are rhodo glaze raw material, its parts by weight are: 70~80 parts of rhodo glaze frits, these 6~8 parts of feldspars, 2~5 parts, Suzhou soil, 6~9 parts of bright red pigments, red 5~8 parts of atom, 3~5 parts of zirconium iron pinks, 0.3~0.6 part of melanochrome.
Wherein said rhodo glaze frit be take feldspar, quartz, hydrated alumina, boron oxide, calcite, strontium titanate, zinc oxide, sodium carbonate and is made frit as raw material, its parts by weight are: 16~20 parts of feldspars, quartzy 30~36 parts, 7~10 parts of hydrated alumina, 10~15 parts of boron oxides, 5~8 parts, calcite, 10~15 parts of strontium titanate, 6~8 parts, zinc oxide, 0.8~1.2 part, sodium carbonate.
Above-mentioned rhodo glaze raw material and ball, water enter ball mill cylinder ball milling by weight ratio, rhodo glaze raw material: ball: water=1:0.7:0.7, through 24 hours ball millings, goes out cylinder mistake 180 mesh sieves and make rhodo glaze.
Dehua china clay, i.e. Fujian mud, the feldspathic china clay of richness of producing for Dehua County, Fujian Province porcelain stone ore deposit.
Low temperature rose red glaze ceramic products provided by the invention adopts the firing process of high temperature biscuiting, low temperature sinter, by high temperature biscuiting, product approval is solidified, make the technical indicators such as shape of product, specification, volume, water-intake rate, bending strength meet client or specified requirement, avoid blank in sintering process organism volatilization and base, glaze when high temperature burns till at the same time combination reaction glaze is had a negative impact.The effect of red slurry is to adjust glaze colours together with the infrared glaze of rose, makes glaze colours keep stable, and ceramic form surface smoothness after the biscuiting of raising high temperature becomes, does not affect on ceramic form surface and execute other glaze again; Fill up the micro hole that ceramic form produces in sintering process; When the outer glaze of executing of next step burns till, due to what mill base produced, stablize pure layer, the fault defect of having blocked the alloying reaction of the trickle objectionable impurities of work in-process and low temperature glaze layer and having produced, make product there is the defects such as high strength, high compactness, free of pinholes, contracting glaze, orange peel glaze, base bubble, glaze colours is rich in stereoscopic sensation, the ceramic color stable that different batches is fired.
Embodiment
The specific embodiment of the present invention is described in conjunction with the embodiments.
embodiment 1
(1) the red slurry of system
By following red slurry raw material, according to parts by weight, formed 6 parts of feldspars, 23 parts, Suzhou soil, 50 parts of Dehua china clay, 8 parts of frits, 13 parts of bright red pigments;
Above-mentioned red slurry raw material is entered to ball mill cylinder ball milling by weight ratio with ball, water, red slurry raw material: ball: water=1:1.6:1.6, through 15 hours ball millings, goes out cylinder and cross 120 mesh sieves and make red slurry.
(2) rhodo glaze processed
First, rhodo glaze frit processed, rhodo glaze frit is comprised of according to parts by weight following, 16 parts of feldspars, quartzy 34 parts, 10 parts of hydrated alumina, 10 parts of boron oxides, 7 parts, calcite, 15 parts of strontium titanate, 6 parts, zinc oxide, 1.0 parts, sodium carbonate;
Secondly, enamel frit makeing material, rhodo glaze is comprised of according to parts by weight following rhodo glaze raw material, 75 parts of rhodo glaze frits, these 8 parts of feldspars, 2 parts, Suzhou soil, 8 parts of bright red pigments, red 8 parts of atom, 3 parts of zirconium iron pinks, 0.5 part of melanochrome;
Above-mentioned rhodo glaze raw material and ball, water enter ball mill cylinder ball milling by weight ratio, rhodo glaze raw material: ball: water=1:0.7:0.7, through 24 hours ball millings, goes out cylinder mistake 180 mesh sieves and make rhodo glaze.
(3) high temperature biscuiting
To soak the mode of glaze, execute red slurry on ceramic body surface, after red slurry is dry, carry out high temperature biscuiting, biscuiting temperature is 1150 ℃~1200 ℃.
(4) low temperature sinter
Adopt the method for soaking glaze to execute rhodo glaze the ceramic form after high temperature biscuiting again, low temperature sinter after dry, adopts roller kiln oxydizing flame to burn till, and firing temperature is 850 ℃~950 ℃, burns till kiln discharge.
Just become after the assay was approved qualified product.
embodiment 2
(1) the red slurry of system
By following red slurry raw material, according to parts by weight, formed 8 parts of feldspars, 25 parts, Suzhou soil, 48 parts of Dehua china clay, 7 parts of frits, 16 parts of bright red pigments;
Above-mentioned red slurry raw material is entered to ball mill cylinder ball milling by weight ratio with ball, water, red slurry raw material: ball: water=1:1.6:1.6, through 15 hours ball millings, goes out cylinder and cross 120 mesh sieves and make red slurry.
(2) rhodo glaze processed
First, rhodo glaze frit processed, rhodo glaze frit is comprised of according to parts by weight following, 18 parts of feldspars, quartzy 36 parts, 7 parts of hydrated alumina, 13 parts of boron oxides, 8 parts, calcite, 10 parts of strontium titanate, 7 parts, zinc oxide, 1.2 parts, sodium carbonate;
Secondly, enamel frit makeing material, rhodo glaze is comprised of according to parts by weight following rhodo glaze raw material, 70 parts of rhodo glaze frits, these 7 parts of feldspars, 5 parts, Suzhou soil, 6 parts of bright red pigments, red 7 parts of atom, 5 parts of zirconium iron pinks, 0.3 part of melanochrome;
Above-mentioned rhodo glaze raw material and ball, water enter ball mill cylinder ball milling by weight ratio, rhodo glaze raw material: ball: water=1:0.7:0.7, through 24 hours ball millings, goes out cylinder mistake 180 mesh sieves and make rhodo glaze.
(3) high temperature biscuiting
To soak the mode of glaze, execute red slurry on ceramic body surface, after red slurry is dry, carry out high temperature biscuiting, biscuiting temperature is 1150 ℃~1200 ℃.
(4) low temperature sinter
Adopt the method for soaking glaze to execute rhodo glaze the ceramic form after high temperature biscuiting again, low temperature sinter after dry, adopts roller kiln oxydizing flame to burn till, and firing temperature is 850 ℃~950 ℃, burns till kiln discharge.
Just become after the assay was approved qualified product.
embodiment 3
(1) the red slurry of system
By following red slurry raw material, according to parts by weight, formed 7 parts of feldspars, 20 parts, Suzhou soil, 45 parts of Dehua china clay, 10 parts of frits, 18 parts of bright red pigments; Above-mentioned red slurry raw material is entered to ball mill cylinder ball milling by weight ratio with ball, water, red slurry raw material: ball: water=1:1.6:1.6, through 15 hours ball millings, goes out cylinder and cross 120 mesh sieves and make red slurry.
(2) rhodo glaze processed
First, rhodo glaze frit processed, rhodo glaze frit is comprised of according to parts by weight following, 20 parts of feldspars, quartzy 30 parts, 8 parts of hydrated alumina, 15 parts of boron oxides, 5 parts, calcite, 13 parts of strontium titanate, 8 parts, zinc oxide, 0.8 part, sodium carbonate;
Secondly, enamel frit makeing material, rhodo glaze is comprised of according to parts by weight following rhodo glaze raw material, 80 parts of rhodo glaze frits, these 6 parts of feldspars, 4 parts, Suzhou soil, 9 parts of bright red pigments, red 5 parts of atom, 4 parts of zirconium iron pinks, 0.6 part of melanochrome;
Above-mentioned rhodo glaze raw material and ball, water enter ball mill cylinder ball milling by weight ratio, rhodo glaze raw material: ball: water=1:0.7:0.7, through 24 hours ball millings, goes out cylinder mistake 180 mesh sieves and make rhodo glaze.
(3) high temperature biscuiting
To soak the mode of glaze, execute red slurry on ceramic body surface, after red slurry is dry, carry out high temperature biscuiting, biscuiting temperature is 1150 ℃~1200 ℃.
(4) low temperature sinter
Adopt the method for soaking glaze to execute rhodo glaze the ceramic form after high temperature biscuiting again, low temperature sinter after dry, adopts roller kiln oxydizing flame to burn till, and firing temperature is 850 ℃~950 ℃, burns till kiln discharge.
Just become after the assay was approved qualified product.
Claims (4)
1. low temperature rose red glaze ceramic products, is characterized in that: by following steps system, to soak the mode of glaze, on ceramic body surface, execute red slurry, after red slurry is dry, carry out high temperature biscuiting, biscuiting temperature is 1150 ℃~1200 ℃;
Adopt the method for soaking glaze to execute rhodo glaze the ceramic form after high temperature biscuiting again, low temperature sinter after dry, adopts roller kiln oxydizing flame to burn till, and firing temperature is 850 ℃~950 ℃, burns till kiln discharge.
2. low temperature rose red glaze ceramic products according to claim 1, is characterized in that: described redness is starched, by following red slurry raw material, according to parts by weight, formed,
6~8 parts of feldspars,
20~25 parts, Suzhou soil,
45~50 parts of Dehua china clay,
7~10 parts of frits,
13~18 parts of bright red pigments;
Above-mentioned red slurry raw material is entered to ball mill cylinder ball milling by weight ratio with ball, water, red slurry raw material: ball: water=1:1.6:1.6, through 15 hours ball millings, goes out cylinder and cross 120 mesh sieves and make red slurry.
3. low temperature rose red glaze ceramic products according to claim 1, is characterized in that: described rhodo glaze is comprised of according to parts by weight following rhodo glaze raw material,
70~80 parts of rhodo glaze frits,
These 6~8 parts of feldspars,
2~5 parts, Suzhou soil,
6~9 parts of bright red pigments,
Red 5~8 parts of atom,
3~5 parts of zirconium iron pinks,
0.3~0.6 part of melanochrome;
Above-mentioned rhodo glaze raw material and ball, water enter ball mill cylinder ball milling by weight ratio, rhodo glaze raw material: ball: water=1:0.7:0.7, through 24 hours ball millings, goes out cylinder mistake 180 mesh sieves and make rhodo glaze.
4. low temperature rose red glaze ceramic products according to claim 3, is characterized in that: described rhodo glaze frit is comprised of according to parts by weight following,
16~20 parts of feldspars,
Quartzy 30~36 parts,
7~10 parts of hydrated alumina,
10~15 parts of boron oxides,
5~8 parts, calcite,
10~15 parts of strontium titanate,
6~8 parts, zinc oxide,
0.8~1.2 part, sodium carbonate.
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
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CN104193416A (en) * | 2014-09-03 | 2014-12-10 | 江苏省宜兴彩陶工艺厂 | Fast firing method for black aventurine glaze ceramic product in roller kiln |
CN104496554A (en) * | 2014-12-03 | 2015-04-08 | 张幼兰 | Jun red glaze and preparation method thereof |
Citations (2)
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CN102101794A (en) * | 2011-01-20 | 2011-06-22 | 潮州市波士发陶瓷制作有限公司 | Glazed low-temperature bright-red glaze and production process for ceramic products thereof |
CN102863259A (en) * | 2012-10-11 | 2013-01-09 | 江苏省宜兴彩陶工艺厂 | Low-temperature-glaze ceramic manufacturing method |
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Patent Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
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CN102101794A (en) * | 2011-01-20 | 2011-06-22 | 潮州市波士发陶瓷制作有限公司 | Glazed low-temperature bright-red glaze and production process for ceramic products thereof |
CN102863259A (en) * | 2012-10-11 | 2013-01-09 | 江苏省宜兴彩陶工艺厂 | Low-temperature-glaze ceramic manufacturing method |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
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CN104193416A (en) * | 2014-09-03 | 2014-12-10 | 江苏省宜兴彩陶工艺厂 | Fast firing method for black aventurine glaze ceramic product in roller kiln |
CN104193416B (en) * | 2014-09-03 | 2015-11-11 | 江苏省宜兴彩陶工艺厂 | The fast firing method of dark fund star glaze ceramic roller kiln |
CN104496554A (en) * | 2014-12-03 | 2015-04-08 | 张幼兰 | Jun red glaze and preparation method thereof |
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Application publication date: 20140305 |