CN103609561B - Rice blast prevention and control insecticide - Google Patents

Rice blast prevention and control insecticide Download PDF

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CN103609561B
CN103609561B CN201310656375.9A CN201310656375A CN103609561B CN 103609561 B CN103609561 B CN 103609561B CN 201310656375 A CN201310656375 A CN 201310656375A CN 103609561 B CN103609561 B CN 103609561B
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pesticide control
kasugarnycin
rice blast
portugal
control
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CN103609561A (en
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郭红甫
李政道
曹筠慧
陈建芳
孙艳敏
许国震
高洪泽
孙刚强
岳振国
白怀瑾
王留梅
秦海英
胡玉香
胡占菊
周娟丽
亓晓光
陈禄廷
刘晓帆
郭慧
赵平
寿永前
高爱旗
郭宁宁
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Abstract

The invention relates to a rice blast prevention and control insecticide, which consists of the following effective components in parts by weight: 0.1 to 55.0 parts of kasugamycin and 0.1 to 25.0 parts of glucan. According to the rice blast prevention and control insecticide, the synergistic effects of sterilization activity of kasugamycin and resistance induction of glucan are used for preventing and controlling the occurrence and development of rice blast, the insecticide has both prevention and control effects, and remarkable prevention and control effects can be achieved whenever the insecticide is used before or after the occurrence of the rice blast.

Description

A kind of pesticide control of rice blast
Technical field
The present invention relates to a kind of pesticide control of rice blast.
Background technology
Rice blast is also known as rice blast, and be one of the most serious three large diseases of hazard rice, can cause the paddy rice significantly underproduction, underproduction 40%-50% time serious, even No kernels or seeds are gathered, as in a year of scarcity.Rice blast all has generation throughout the country, occurs as many with leaf portion, joint portion, and main Types has seedling pest, leaf pest, joint pest, panicle blast and grain acne.
Rice blast pathogen is survived the winter on sick paddy, sick grass with conidium and mycelium, sprouts and produces conidium, propagate by means of air-flow, belong to polycyclic disease under good growing weather condition.Method for integrated control is taked, to eliminate premised on bacterium source of surviving the winter, to select centered by disease-resistant variety, and based on Healthy culture, chemical control is auxiliary Comprehensive Control Strategy, under normal circumstances to select disease-resistant variety and chemical control to attach most importance to.
In rice blast chemical control, be bacillus amyloliquefaciens, bacillus subtilis by the biological control medicament of national agriculture chemical registration at present, chemical control medicament is tricyclazole, kasugarnycin, cytosintetidemycin, fenoxanil, propiconazole, Isoprothiolane, carbendazim, prochloraz, tolelofos-methyl, chlorine nalidixic bacterium ester, own azoles alcohol, Tebuconazole, jinggangmeisu, Difenoconazole, cyprodinil, triazolone, iprobenfos, thiophanate-methyl, sulphur, prochloraz-manganese chloride complex, edifenphos, phosethyl-Al, olefin conversion, S-Ethyl ethylthio sulfonate, tmtd, oxime bacterium ester, pungent bacterium amine acetate, polyoxin, this thiazole of Western-style pastry, the single dose of tpn etc. or complex preparation.Biological control weak effect, takes effect slow, can not meet the needs of agricultural production; The good medicament of chemical control preventive effect is tricyclazole, and the good medicament of result for the treatment of is kasugarnycin.
At present by the single dose of national agriculture chemical registration kasugarnycin, be mainly used in preventing and treating rice blast, fusarium wilt, leaf mold, angular leaf spot, wildfire; Relevant complex preparation, as the complex preparation with chlorobromide isocyanuric acid, sulphur, Isoprothiolane, for preventing and treating rice blast; Composite with carbendazim, for preventing and treating anthracnose; With the complex preparation of prochloraz-manganese chloride complex, for preventing and treating rust; With the complex preparation of Cupravit, be used for the treatment of canker, downy mildew, leaf mold, peronospora tabacina.But on the whole, in rice blast is prevented and treated, the good medicament of integrated control effect is the complex preparation of tricyclazole and kasugarnycin, and control efficiency is 70%-80%.
CN200710085999.4(publication number is CN101258851A) disclose a kind of by amino-oligosaccharide-kasugarnycin and nutritive element form the production technology of soluble powder.Its ratio of components is: amino-oligosaccharide 0.2%-12%, kasugarnycin 1-20%, nutritive element 98.8-68%, and described nutritive element is mineral salt and the chelates thereof such as B, Zn, Mn, Fe, Mo.
For this reason, the rice blast pesticide control that a kind of prevention and therapy better effects if is provided is necessary.
Summary of the invention
The object of this invention is to provide a kind of rice blast pesticide control.
The pesticide control of a kind of rice blast of the present invention, its active component contains kasugarnycin and Portugal's polyene sugar.
Concrete, the active component of described pesticide control contains following parts by weight ingredient: kasugarnycin 0.1-55.0 part and Portugal's polyene sugar 0.1-25.0 part.
Preferably, the active component of described pesticide control contains following parts by weight ingredient: kasugarnycin 0.1-50.0 part and Portugal's polyene sugar 0.1-20.0 part.
Also soluble filler is comprised in pesticide control provided by the invention, described soluble filler is the various soluble filler that this area is commonly used, according to the common practise of those skilled in the art, mineral salt preferably containing plant nutrient ingredient or organic matter, as the mineral salt containing potassium, phosphorus, magnesium, calcium, manganese, copper, zinc, ammonium etc. or organic salt, urea etc. containing nitrogen, is specially calcium chloride, potassium chloride, manganese chloride, magnesium chloride, ammonium chloride, urea, ferrous sulfate, zinc sulphate, copper sulphate, ammonium sulfate, magnesium sulfate, calcium acetate or potassium dihydrogen phosphate.
In above-mentioned pesticide control:
Described weight portion can be the known unit of weights of pesticide field such as μ g, mg, g, kg, also can be above-mentioned known unit of weight multiple, as 10 times, 100 times, 1/10th, one of percentage.
Pesticide control provided by the invention is preparation well known in the art, preferred solvable pulvis and aqua.
Present invention also offers the preparation method of above-mentioned pesticide control, the method comprises the following steps: take each composition according to proportioning, mix, to obtain final product.
Present invention also offers the application of above-mentioned pesticide control in the agricultural chemicals of preparation control rice blast.
Pesticide control provided by the invention generally adopts foliage-spray, and its effective ingredient consumption is generally 2-3g/ mu, and active ingredient spraying concentration is generally 50-80ppm.Those skilled in the art can adjust consumption as required.
The pesticide control of rice blast provided by the invention has the following advantages:
1, in pesticide control provided by the invention:
Kasugarnycin (kasugamycin), have another name called kasugarnycin, chemical name: (5-amino-2-methyl-6-(2,3,4,5,6-hydroxy-cyclohexyl oxo) tetrahydropyran-3-base) amino-α-IMDA, be the metabolite that actinomycetes produce, sterling is white, needle-shaped crystals solid, hydrochloride is soluble in water, in 25 DEG C of water, dissolve 12.5%(W/V); Stablize at normal temperatures, stable under acidity and neutrallty condition, easily decompose in the basic conditions.Absorption antibiotic in kasugarnycin belongs to, the micro-poison of toxicity, for preventing and treating various bacterial disease and fungal disease, has preventive and therapeutic action concurrently, is the special antibiotic of control rice blast.
Portugal's polyene sugar, belonging to polysaccharose bioactivator, is a kind of novel plant resistance to environment stress derivant, and micro-poison is soluble in water.Portugal's polyene sugar can produce the protective plant protecting agent killing pathogenic microorganism by inducing plant as external source regulatory factor, reduces the generation of various crop disease; Can also as the effective Promoting plant growth of growth regulator, branch, bloom, every metabolic activity such as result, improve crop yield.
Research find, above-mentioned two kinds of active principle kasugarnycin and Portugal's polyene sugar mixture after, there is synergy, can significantly increase control rice blast effect.
2, the agricultural chemicals producing the control rice blast applied at present is the single dose of bactericide or the complex preparation of bactericide and bactericide, and control efficiency is poor.
3, the active ingredient of rice blast pesticide control of the present invention is formed by antibiotic kasugarnycin and active polysaccharide Portugal polyene sugar mixture, utilize the synergy of antibiotic bactericidal activity and active polysaccharide induction of resistance, strengthen control efficiency, the generation of prevention and corntrol rice blast and development.The present invention prevents and treats rice blast and has preventive and therapeutic action concurrently, and medication optimum period is long, and premorbid or the rear use of morbidity all can reach significant control efficiency.
Embodiment
Following examples for illustration of the present invention, but are not used for limiting the scope of the invention.
In the following examples, the particle size range of all raw materials is not limit, but in order to meet the obtained mobility of preparation, the needs of the uniformity, preferred size is the raw material components of 0.01-0.99mm.But should not form restriction of the present invention.
Embodiment 1: rice blast pesticide control " the polyene syrup agent of 0.1% kasugarnycin+0.1% Portugal "
1, component (100%): 0.1% kasugarnycin; 0.1% Portugal's polyene sugar.
2, compound method: take 65% kasugarnycin 0.15g, 95% Portugal polyene sugar 0.11g respectively, put into the volumetric flask of 100ml, be dissolved in water and be settled to 100ml, obtained aqua.
Embodiment 2: rice blast pesticide control " the polyene syrup agent of 2% kasugarnycin+0.5% Portugal "
1, component (100%): 2.0% kasugarnycin; 0.5% Portugal's polyene sugar.
2, compound method: take 65% kasugarnycin 3.1g, 95% Portugal polyene sugar 0.5g respectively, put into the volumetric flask of 100ml, be dissolved in water and be settled to 100ml, obtained aqua.
Embodiment 3: rice blast pesticide control " the solvable pulvis of 10% kasugarnycin+2% Portugal polyene sugar "
1, component (percentage by weight 100%): 10.0% kasugarnycin; 2.0% Portugal's polyene sugar; Filler copper sulphate.
2, compound method: take 65% kasugarnycin 15.4g, 95% Portugal polyene sugar 2.1g, filler copper sulphate 82.5g respectively, by said components Homogeneous phase mixing.
Embodiment 4: rice blast pesticide control " the solvable pulvis of 20% kasugarnycin+5% Portugal polyene sugar "
1, component (percentage by weight 100%): 20.0% kasugarnycin; 5.0% Portugal's polyene sugar; Filler ammonium chloride.
2, compound method: take 65% kasugarnycin 30.8g, 95% Portugal polyene sugar 5.3g, filler ammonium chloride 63.9g respectively, by said components Homogeneous phase mixing.
Embodiment 5: rice blast pesticide control " the solvable pulvis of 35% kasugarnycin+10% Portugal polyene sugar "
1, component (percentage by weight 100%): 35.0% kasugarnycin; 10.0% Portugal's polyene sugar; Filler manganese chloride.
2, compound method: take 65% kasugarnycin 53.8g, 95% Portugal polyene sugar 10.5g, filler manganese chloride 35.7g respectively, by said components Homogeneous phase mixing.
Embodiment 6: rice blast pesticide control " the solvable pulvis of 50% kasugarnycin+20% Portugal polyene sugar "
1, component (percentage by weight 100%): 50.0% kasugarnycin; 20.0% Portugal's polyene sugar; Filler potassium chloride.
2, compound method: take 65% kasugarnycin 76.9g, 95% Portugal polyene sugar 21.1g, filler potassium chloride 2.0g respectively, by said components Homogeneous phase mixing.
Embodiment 7: rice blast pesticide control " the solvable pulvis of 40% kasugarnycin+5% Portugal polyene sugar "
1, component (percentage by weight 100%): 40.0% kasugarnycin; 5.0% Portugal's polyene sugar; Filler calcium chloride.
2, compound method: take 65% kasugarnycin 61.5g, 95% Portugal polyene sugar 5.3g, filler calcium chloride 33.2g respectively, by said components Homogeneous phase mixing.
Embodiment 8: rice blast pesticide control " the solvable pulvis of 10% kasugarnycin+15% Portugal polyene sugar "
1, component (percentage by weight 100%): 10.0% kasugarnycin; 15.0% Portugal's polyene sugar; Filler urea.
2, compound method: take 65% kasugarnycin 15.4g, 95% Portugal polyene sugar 15.8g, filler urea 68.8g respectively, by said components Homogeneous phase mixing.
Experimental example 1
1, test process and method:
Test process and spraying concentration are in table 1, and the kasugarnycin spraying concentration arranged in each process is all about 80ppm.Wherein,
Process 1-8: be respectively the rice blast pesticide control that embodiment of the present invention 1-8 provides;
Contrast ck 1: 10% kasugarnycin wetting powder (commercially available product);
Contrast ck 2: 0.5% Portugal's polyene syrup agent (commercially available product);
Contrast ck 0: clear water contrasts.
Table 1 is tested process and is arranged
Experimental field be located at theatre township, Puyang County, fertilizer and water condition is good, and irrigation and drainage are convenient, and soil fertility is even.No. 6, rice varieties Zheng drought, waits line-spacing to plant, line-spacing 0.3m, cave distance 0.1m, density 2.2 ten thousand clumps/mu.Plot area 27m 2, 15 row districts, the long 6m of row.Test establishes 3 repetitions, Gong33Ge community, and random district group arranges.In process of the test, other field management is normal.
Rice blast their early stage starts first time medication, is the workers and peasants 16 type manual sprayer of 0.7mm with injection diameter, the test process even spraying arranged by above-mentioned table 1, community sprays amount of liquid medicine 1.2kg, amount to every mu time and spray amount of liquid medicine 30 kilograms, interval is once sprayed 2 times for 7 days altogether.
Every community is by selected 5 points of diagonal method, and often marks 5 clumps.Investigation state of an illness radix before dispenser, after second time dispenser 7 days, the stem tiller incidence of investigation mark clump.
Severity Scaling standard is as follows:
0 grade: anosis;
1 grade: leaf spot lesion is less than 5, and length is less than 1cm;
3 grades: leaf spot lesion 6-10, part scab length is greater than 1cm;
5 grades: leaf spot lesion 11-25, part scab is linked to be sheet, accounts for the 10%-25% of leaf area;
7 grades: leaf spot lesion more than 26, scab is linked to be sheet, accounts for the 26%-50% of leaf area;
9 grades: scab is linked to be sheet, account for more than 50% of leaf area, or full leaf is withered.
(1) and (2) calculates control efficiency according to the following formula.
2, result of the test: in table 2.
Table 2: rice blast pesticide control result of the test summary sheet
Table 2 result shows: the liquid that each process is configured to be about containing active ingredient kasugarnycin 80ppm carries out foliage-spray, and the effect that process 1-8 prevents and treats rice blast is 93.7%-95.5%, and between each process, difference is not remarkable, is all extremely significantly better than contrasting ck 1the preventive effect 75.1% of 10% kasugarnycin wetting powder; Contrast ck 2the preventive effect of 0.5% Portugal polyene syrup agent is 48.7%, is significantly inferior to other and respectively processes.
Result of the test can be found out, test arrange kasugarnycin weight portion 0.1-50.0, Portugal polyene sugar weight part 0.1-20.0 scope in, Portugal's polyene sugar can significantly improve kasugarnycin control rice blast effect.
Embodiment 2
1, test material and method
Test medicine: 10% kasugarnycin+2% Portugal polyene solvable pulvis of sugar (embodiment 3);
Contrast medicament: 1. 22% spring thunder tricyclazole wettable powder, commercially available product;
2. the solvable pulvis of 10% kasugarnycin+5% amino-oligosaccharide;
3. 0.5% Portugal polyene syrup agent, commercially available product.
Test process is set to: " the solvable pulvis of 10% kasugarnycin+2% Portugal polyene sugar " 1000 times of liquid (120ppm), 1500 times of liquid (80ppm), 2000 times of liquid (60ppm), 1. 22% spring thunder tricyclazole wettable powder, 600 times of liquid (367ppm), the 2. solvable pulvis of 10% kasugarnycin+5% amino-oligosaccharide 1000 times of liquid (150ppm), 3. 0.5% Portugal polyene syrup agent, 900 times of liquid (5.6ppm) and clear water contrast 7 process to contrast medicament.
Test is located at Chen Zhuan township, Fan County, and experimental field design and preventive effect investigation method are with embodiment 1.
2, result of the test: result of the test is in table 3.
Table 3: test medicine control rice blast result of the test
Table 3 result shows: the average preventive effect of test medicine " the solvable pulvis of 10% kasugarnycin+2% Portugal polyene sugar " 1000 times of liquid, 1500 times of liquid, 2000 times of liquid is respectively 93.1%, 89.7%, 87.2%, and the average preventive effect of contrast medicament 22% spring thunder tricyclazole wettable powder 600 times of liquid, the solvable pulvis of 10% kasugarnycin+5% amino-oligosaccharide 1000 times of liquid, 0.5% Portugal's polyene syrup agent, 900 times of liquid is respectively 75.6%, 77.0%, 52.0%.Through significance of difference analysis, the preventive effect that test medicine three processes all extremely significantly is better than contrasting medicament.
Result shows: test medicine " the solvable pulvis of 10% kasugarnycin+2% Portugal polyene sugar ", the i.e. composite mixture of kasugarnycin and Portugal's polyene sugar, the effect of control rice blast is extremely significantly better than the preventive effect of the preventive effect of the high amount of limiting the use of of the best kasugarnycin of current known preventive effect and tricyclazole complex preparation and the high amount of limiting the use of of kasugarnycin and the composite mixture of amino-oligosaccharide; The preventive effect of the kasugarnycin that current known preventive effect is best and tricyclazole complex preparation is suitable with the preventive effect of kasugarnycin and amino-oligosaccharide complex preparation.
Experimental example 3
1, test material and method
Active ingredient: 10% kasugarnycin+2% Portugal polyene sugar
Test process: respectively with calcium chloride, potassium chloride, magnesium chloride, ammonium sulfate, potassium acetate, potassium dihydrogen phosphate, urea for filler, prepare the solvable pulvis of above-mentioned active ingredient rice blast pesticide control, be respectively process 1-7; The aqua of the rice blast pesticide control of the above-mentioned active ingredient of preparation is process 8; Clear water contrast is ck 0.
Compound method: 1. solvable pulvis: select the raw material components of granularity between 0.01 ~ 0.99mm, take 65% kasugarnycin 15.4g, 95% Portugal polyene sugar 2.1g respectively, take filler calcium chloride, potassium chloride, magnesium chloride, ammonium sulfate, potassium acetate, potassium dihydrogen phosphate, each 82.5g of urea successively again, respectively with said components Homogeneous phase mixing.2. aqua: take 65% kasugarnycin 15.4g, 95% Portugal polyene sugar 2.1g, put into the volumetric flask of 100ml, be dissolved in water and be settled to 100ml, obtained aqua.
Test method is with experimental example 1.
2, result of the test: in table 4.
Table 4: different filler control efficiency summary sheet
Table 4 result shows: respectively with calcium chloride, potassium chloride, magnesium chloride, ammonium sulfate, potassium acetate, potassium dihydrogen phosphate, urea etc. containing the soluble inorganic salt of plant nutrient or organic matter for filler, " 10% kasugarnycin+2% Portugal polyene sugar " the solvable pulvis of preparation or aqua, 1500 times of liquid (80ppm) foliage-sprays, control rice blast effect is 91.7%-96.2%.Through significance of difference analysis, between the solvable pulvis of different filler, aqua, difference is not remarkable.
Test shows: the different fillers in pesticide control provided by the invention, different dosage form, have no significant effect control efficiency.
Experimental example 4
Rice blast pesticide control " 10% kasugarnycin+2% Portugal polyene sugar solvable pulvis " prepared by embodiment 3, in Puyang County, Fan County, Yuanyang County, the ground experiment and demonstration such as Xuzhou the results are shown in Table 5.
Table 5: embodiment 3 prevents and treats rice blast experiment and demonstration result summary sheet
Place Control efficiency (%) Effect of increasing production (%)
Puyang County 92.3~95.9 13.6~34.7
Fan County 89.1~94.6 11.5~32.9
Yuanyang County 91.2~93.0 12.7~30.1
Xuzhou City 92.2~94.7 10.9~27.8
Table 5 result shows: rice blast pesticide control prepared by the present invention, control efficiency 89.1%-95.9%, effect of increasing production 10.9%-34.7%.
Demonstration result shows: the present invention prevents and treats rice blast Be very effective, and volume increase obviously, is the favourable agents of control rice blast.
Although above with general explanation, embodiment and test, the present invention is described in detail, and on basis of the present invention, can make some modifications or improvements it, this will be apparent to those skilled in the art.Therefore, modifications or improvements without departing from theon the basis of the spirit of the present invention, all belong to the scope of protection of present invention.

Claims (10)

1. a pesticide control for rice blast, is characterized in that, the active component of described pesticide control is made up of following parts by weight ingredient: kasugarnycin 0.1-55.0 part and Portugal's polyene sugar 0.1-25.0 part.
2. pesticide control according to claim 1, is characterized in that, the active component of described pesticide control is made up of following parts by weight ingredient: kasugarnycin 0.1-50.0 part and Portugal's polyene sugar 0.1-20.0 part.
3. pesticide control according to claim 1 and 2, is characterized in that, also comprises soluble filler in described pesticide control.
4. pesticide control according to claim 3, is characterized in that, described soluble filler is mineral salt containing plant nutrient ingredient or organic matter.
5. pesticide control according to claim 4, is characterized in that, described soluble filler is mineral salt containing potassium, phosphorus, magnesium, calcium, manganese, copper, zinc or ammonium or organic salt, or the urea containing nitrogen.
6. pesticide control according to claim 4, it is characterized in that, described soluble filler is calcium chloride, potassium chloride, manganese chloride, magnesium chloride, ammonium chloride, urea, ferrous sulfate, zinc sulphate, copper sulphate, ammonium sulfate, magnesium sulfate, calcium acetate or potassium dihydrogen phosphate.
7. pesticide control according to claim 1 and 2, is characterized in that, described pesticide control is solvable pulvis and aqua.
8. pesticide control according to claim 3, is characterized in that, described pesticide control is solvable pulvis and aqua.
9. the pesticide control according to any one of claim 4-6, is characterized in that, described pesticide control is solvable pulvis and aqua.
10. the application of the pesticide control described in any one of claim 1-9 in the agricultural chemicals of preparation control rice blast.
CN201310656375.9A 2013-12-06 2013-12-06 Rice blast prevention and control insecticide Active CN103609561B (en)

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Publication number Priority date Publication date Assignee Title
CN106259432A (en) * 2016-08-07 2017-01-04 江苏辉丰农化股份有限公司 A kind of microbicide compositions
CN106417299A (en) * 2016-10-14 2017-02-22 陕西麦可罗生物科技有限公司 Pesticide composition containing kasugamycin and S-ABA (abscisic acid) as well as application of pesticide composition
CN108651463A (en) * 2017-03-28 2018-10-16 毕标能 A kind of efficient bactericidal composite containing kasugarnycin
CN107535524A (en) * 2017-07-04 2018-01-05 天津市华宇农药有限公司 The bactericidal composition of biological pesticide and its application
CN109221131B (en) * 2018-10-31 2021-02-19 安徽省锦江农化有限公司 Aqueous solution containing amino-oligosaccharin and kasugamycin and application thereof
CN110973161A (en) * 2019-11-28 2020-04-10 山东中新科农生物科技有限公司 Sterilization composition containing glucan
CN111184027A (en) * 2020-03-15 2020-05-22 雷志刚 Production method of inorganic pesticide for preventing and treating rice blast

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CN101946772A (en) * 2010-09-28 2011-01-19 李学员 Combined pesticide for controlling rice blast
CN102239845A (en) * 2011-05-05 2011-11-16 海利尔药业集团股份有限公司 Pesticide composition containing cytosinpeptidemycin and glucal

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101946772A (en) * 2010-09-28 2011-01-19 李学员 Combined pesticide for controlling rice blast
CN102239845A (en) * 2011-05-05 2011-11-16 海利尔药业集团股份有限公司 Pesticide composition containing cytosinpeptidemycin and glucal

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