CN103598245A - Preparation method of anti-disease medicine against potato bacterial wilt - Google Patents

Abstract

The invention discloses a preparation method of an anti-disease medicine against potato bacterial wilt, which comprises the following steps: (A) material preparation: preparing streptomycin sulfate, 25% cuaminosulfate aqueous solution, 2% formalin, glycyrrhizic acid, chlorogenic acid, polyoxin, radix ampelopsis and dried orange peel; (B) alcohol digestion of the extraction liquid of radix ampelopsis and dried orange peel: crushing the radix ampelopsis and dried orange peel, washing and airing; putting into a closed container, adding 70% ethanol solution by mass, and soaking for 12 hours; putting into a percolator, wherein the percolator is of a bucket structure with a cone at the bottom, the cone is downward connected with equipment which can be opened/closed to drop water, and the percolator is used for extracting the components of the medicinal materials; uniformly putting the medicinal materials into the bucket, and adding the soaking liquid water or wine slowly and dropwise; collecting the percolation liquid; and heating to recover ethanol to obtain the extraction liquid; and (C) compounding the streptomycin sulfate, 25% cuaminosulfate aqueous solution, 2% formalin, glycyrrhizic acid, chlorogenic acid and polyoxin with the extraction liquid obtained by the step (B), stirring uniformly and performing ultraviolet sterilization to obtain the anti-disease medicine against potato bacterial wilt. The preparation method disclosed by the invention is simple, and the prepared product is simple in formula and convenient to use and realizes a good effect in treating the potato bacterial wilt.

Description

A kind of manufacture method of disease-resistant medicine of potato bacterial wilt

 

Technical field:

The present invention relates to vegetables medicine, particularly a kind of manufacture method of disease-resistant medicine of potato bacterial wilt.

 

Background technology:

Bacterial wilt is the Major Diseases of potato.Cardinal symptom be plant wilt rapidly, withered, it is green that cauline leaf still keeps.The brown stain position of sick stem is pushed with hand, has milky bacterium liquid to discharge., field ponding glutinous at hot and humid, continuous cropping continuous cropping, geodepression soil, soil meta-acid, partially in the situation such as nitrogen fertilizer application, this sickly look easily occurs.Ralstonia solanacearum, can together enter soil with the residual body of diseased plant.Long term survival forms source of infection.On it, the existence in soil affects greatly soil moisture.In the fluvisol of high humidity, can survive and reach 2～3 years, and in dry soil, can only survive several days.Ralstonia solanacearum is not survived with resting state, but is bred at the rhizosphere of above-mentioned disease plant or certain weeds in soil.The ralstonia solanacearum of existence in soil, is mainly the wound causing in operation process or the wound infection plant of being caused by root-feeding insects such as root nodule nematode, blue light rutelian larvas, in conduit position and the root morbidity of stem.Sometimes also can be by invading in plant and fall ill without wound radicula.

The present invention is directed to the pesticide resistance problem that current potato bacterial wilt produces, provide a kind of manufacture method simple, the product proportioning making is simple, easy to use, the manufacture method of the disease-resistant medicine of a kind of potato bacterial wilt that treatment potato bacterial wilt is effective.

 

Summary of the invention:

The object of the invention is to overcome the shortcoming existing in prior art, provide a kind of proportioning simple, easy to use, the manufacture method of the disease-resistant medicine of a kind of potato bacterial wilt that treatment potato bacterial wilt is effective.

To achieve these goals, the invention provides a kind of manufacture method of disease-resistant medicine of potato bacterial wilt, wherein, comprise the steps:

A, get the raw materials ready: streptomycin sulphate, 25% network ammonia copper aqua, 2% formalin solution, glycyrrhizic acid, chlorogenic acid, polyoxy is clear, radix ampelopsis, dried orange peel;

The extract of B, alcohol lixiviate radix ampelopsis and dried orange peel:

Radix ampelopsis, dried orange peel are carried out cataclasm, clean, dry after operation, put in a closed container, add mass percent 70% ethanolic solution, infiltrate vexed bubble after 12 hours, reinstall percolator, described percolator is a bucket structure, under be cone, under cone, connect the equipment that a switch can drip, for medicinal ingredient, extract, medicinal material is evenly put into bucket, add soak: water or wine, slowly water clock, collects percolate, obtains extract after heating recovery ethanol;

C, by streptomycin sulphate, 25% network ammonia copper aqua, 2% formalin solution, glycyrrhizic acid, chlorogenic acid, polyoxy is clear, carries out compositely with step B gained extract, after stirring, ultraviolet sterilization, obtains the disease-resistant medicine of potato bacterial wilt.

The disease-resistant medicine of a kind of potato bacterial wilt making through manufacture method of the present invention, wherein, comprises the component of following unit of weight:

Streptomycin sulphate 10-15 part, 25% network ammonia copper aqua 8-12 part, 2% formalin solution 10-15 part, glycyrrhizic acid 4-8 part, chlorogenic acid 4-8 part, the clear 6-10 part of polyoxy, radix ampelopsis 4-8 part, dried orange peel 6-10 part.

Or, comprise the component of following unit of weight:

Streptomycin sulphate 10-12 part, 25% network ammonia copper aqua 8-10 part, 2% formalin solution 10-12 part, glycyrrhizic acid 4-6 part, chlorogenic acid 4-6 part, the clear 6-8 part of polyoxy, radix ampelopsis 4-6 part, dried orange peel 6-8 part.

Or, comprise the component of following unit of weight:

Streptomycin sulphate 12-15 part, 25% network ammonia copper aqua 10-12 part, 2% formalin solution 12-15 part, glycyrrhizic acid 6-8 part, chlorogenic acid 6-8 part, the clear 8-10 part of polyoxy, radix ampelopsis 6-8 part, dried orange peel 8-10 part.

During use, after said components is mixed, be configured to 400-600 times of liquid of quality multiple, carry out spraying operation.

Percentage sign is mass percent.

Advantage of the present invention is, proportioning is simple, easy to use, and treatment potato bacterial wilt is effective, is specially:

When the present invention uses, streptomycin sulphate, 25% network ammonia copper aqua, 2% formalin solution, glycyrrhizic acid, chlorogenic acid, polyoxy is clear, radix ampelopsis, dried orange peel.After being mixed, be configured to 400-600 times of liquid of quality multiple, carry out spraying operation.(when radix ampelopsis and dried orange peel are used, use alcohol leach extraction method to extract extract, what during mixing, use is extract.) through experimental test, the 400-600 of mixture times liquid, has obvious deactivation to ralstonia solanacearum, bactericidal effect is good.

 

Embodiment:

Example 1

10 parts of streptomycin sulphates, 25% 8 parts, network ammonia copper aqua, 2% 10 parts of formalin solutions, 4 parts of glycyrrhizic acids, 4 parts of chlorogenic acids, clear 6 parts of polyoxy, 4 parts of radix ampelopsis, 6 parts of dried orange peels.

Manufacture method is as follows:

A, get the raw materials ready: streptomycin sulphate, 25% network ammonia copper aqua, 2% formalin solution, glycyrrhizic acid, chlorogenic acid, polyoxy is clear, radix ampelopsis, dried orange peel;

The extract of B, alcohol lixiviate radix ampelopsis and dried orange peel:

Radix ampelopsis, dried orange peel are carried out cataclasm, clean, dry after operation, put in a closed container, add mass percent 70% ethanolic solution, infiltrate vexed bubble after 12 hours, reinstall percolator, described percolator is a bucket structure, under be cone, under cone, connect the equipment that a switch can drip, for medicinal ingredient, extract, medicinal material is evenly put into bucket, add soak: water or wine, slowly water clock, collects percolate, obtains extract after heating recovery ethanol;

C, by streptomycin sulphate, 25% network ammonia copper aqua, 2% formalin solution, glycyrrhizic acid, chlorogenic acid, polyoxy is clear, carries out compositely with step B gained extract, after stirring, ultraviolet sterilization, obtains the disease-resistant medicine of potato bacterial wilt.

 

Example 2

15 parts of streptomycin sulphates, 25% 12 parts, network ammonia copper aqua, 2% 15 parts of formalin solutions, 8 parts of glycyrrhizic acids, 8 parts of chlorogenic acids, clear 10 parts of polyoxy, 8 parts of radix ampelopsis, 10 parts of dried orange peels.

Manufacture method is as follows:

A, get the raw materials ready: streptomycin sulphate, 25% network ammonia copper aqua, 2% formalin solution, glycyrrhizic acid, chlorogenic acid, polyoxy is clear, radix ampelopsis, dried orange peel;

The extract of B, alcohol lixiviate radix ampelopsis and dried orange peel:

Radix ampelopsis, dried orange peel are carried out cataclasm, clean, dry after operation, put in a closed container, add mass percent 70% ethanolic solution, infiltrate vexed bubble after 12 hours, reinstall percolator, described percolator is a bucket structure, under be cone, under cone, connect the equipment that a switch can drip, for medicinal ingredient, extract, medicinal material is evenly put into bucket, add soak: water or wine, slowly water clock, collects percolate, obtains extract after heating recovery ethanol;

C, by streptomycin sulphate, 25% network ammonia copper aqua, 2% formalin solution, glycyrrhizic acid, chlorogenic acid, polyoxy is clear, carries out compositely with step B gained extract, after stirring, ultraviolet sterilization, obtains the disease-resistant medicine of potato bacterial wilt.

 

Example 3

12 parts of streptomycin sulphates, 25% 10 parts, network ammonia copper aqua, 2% 12 parts of formalin solutions, 6 parts of glycyrrhizic acids, 6 parts of chlorogenic acids, clear 8 parts of polyoxy, 6 parts of radix ampelopsis, 8 parts of dried orange peels.

Manufacture method is as follows:

A, get the raw materials ready: streptomycin sulphate, 25% network ammonia copper aqua, 2% formalin solution, glycyrrhizic acid, chlorogenic acid, polyoxy is clear, radix ampelopsis, dried orange peel;

The extract of B, alcohol lixiviate radix ampelopsis and dried orange peel:

Radix ampelopsis, dried orange peel are carried out cataclasm, clean, dry after operation, put in a closed container, add mass percent 70% ethanolic solution, infiltrate vexed bubble after 12 hours, reinstall percolator, described percolator is a bucket structure, under be cone, under cone, connect the equipment that a switch can drip, for medicinal ingredient, extract, medicinal material is evenly put into bucket, add soak: water or wine, slowly water clock, collects percolate, obtains extract after heating recovery ethanol;

C, by streptomycin sulphate, 25% network ammonia copper aqua, 2% formalin solution, glycyrrhizic acid, chlorogenic acid, polyoxy is clear, carries out compositely with step B gained extract, after stirring, ultraviolet sterilization, obtains the disease-resistant medicine of potato bacterial wilt.

 

Proportioning of the present invention is simple, easy to use, and treatment potato bacterial wilt is effective, when the present invention uses, and streptomycin sulphate, 25% network ammonia copper aqua, 2% formalin solution, glycyrrhizic acid, chlorogenic acid, polyoxy is clear, radix ampelopsis, dried orange peel.After being mixed, be configured to 400-600 times of liquid of quality multiple, carry out spraying operation.

Claims (1)

1. a manufacture method for the disease-resistant medicine of potato bacterial wilt, is characterized in that, comprises the steps:

A, get the raw materials ready: streptomycin sulphate, 25% network ammonia copper aqua, 2% formalin solution, glycyrrhizic acid, chlorogenic acid, polyoxy is clear, radix ampelopsis, dried orange peel;

The extract of B, alcohol lixiviate radix ampelopsis and dried orange peel:

Radix ampelopsis, dried orange peel are carried out cataclasm, clean, dry after operation, put in a closed container, add mass percent 70% ethanolic solution, infiltrate vexed bubble after 12 hours, reinstall percolator, described percolator is a bucket structure, under be cone, under cone, connect the equipment that a switch can drip, for medicinal ingredient, extract, medicinal material is evenly put into bucket, add soak: water or wine, slowly water clock, collects percolate, obtains extract after heating recovery ethanol;

C, by streptomycin sulphate, 25% network ammonia copper aqua, 2% formalin solution, glycyrrhizic acid, chlorogenic acid, polyoxy is clear, carries out compositely with step B gained extract, after stirring, ultraviolet sterilization, obtains the disease-resistant medicine of potato bacterial wilt.