CN103588510A - Method for manufacturing anti-slip glazed tile - Google Patents
Method for manufacturing anti-slip glazed tile Download PDFInfo
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- CN103588510A CN103588510A CN201310614314.6A CN201310614314A CN103588510A CN 103588510 A CN103588510 A CN 103588510A CN 201310614314 A CN201310614314 A CN 201310614314A CN 103588510 A CN103588510 A CN 103588510A
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Abstract
The invention relates to a method for manufacturing an anti-slip glazed tile, which comprises the following steps: step1) printing; selecting a dried ceramic green body, printing on the surface of the ceramic green body to form a printing layer; Step2) coating high temperature transparent frit; coating the high temperature transparent frit particles with particle size of less than or equal to 20 meshes on the surface of the printed green body in the step1); step3)roasting in kiln; roasting the green body of the high temperature transparent frit particles coated in the step2) under the roller-way kiln oxidation atmosphere, wherein the roasting temperature is 1150-1230 DEG C and the roasting period is 80-120 minutes; and step4) edge rounding grinding; after cooling the roasted green body in the step 3), rounding and grinding edge to obtain the anti-slip glazed tile finished product. Compared with the prior art, the anti-slip glazed tile has anti-slip projection on the surface, the friction area is larger, the anti-slip effect is good, the glaze quality is good, and the anti-slip glazed tile has no influence to decorative effect on the printing layer.
Description
Technical field
The present invention relates to a kind of architectural pottery Manufacturing Method of Products, relate in particular to a kind of method of manufacturing anti-skidding glaze face brick.
Background technology
Ornamental brick is a kind of building material product being widely used.By on adobe surface glazing burn till, obtain abundant decorative effect, and glaze is antifouling, easy to clean, be specially adapted to heavier and more kitchen and the toilet decoration of spot of steam.For stamp series product, can also protect printed layer not to be worn by glaze.Yet glaze product mostly is plane decoration, and smooth smooth glaze is not anti-skidding, is not suitable for ground paving.For this reason, people by arranging the anti-slip veins with concave convex texture on mould, make the adobe stamping out also have corresponding lines, but after glazing, anti-skidding lines can thicken, this mode can not form intensive anti-skidding projection at brick face, and also easily causes disconnected glaze, lacks the defects such as glaze at the concave convex texture of billet surface.
Summary of the invention
The object of the invention is to propose a kind of anti-skidding glaze face brick and manufacture method thereof, the present invention is by charity one deck granularity≤20 object high temperature clear frit powder on base substrate, high temperature clear frit incomplete fusion when burning till, the softening clinkering each other of frit particle forms transparent cover coat, and because do not have complete melting to sprawl, so can form anti-skidding projection on transparent cover coat, so the more existing ornamental brick of structure has better skidproof effect, be applicable to ground decoration paving, and do not affect the decorative effect that on base substrate, stamp forms.
For reaching this object, the present invention by the following technical solutions: a kind of anti-skidding glaze face brick, it comprises green body layer from the bottom to top, printed layer, transparent cover coat, on wherein said transparent cover coat, having is highly the anti-skidding projection of 0.1mm～0.6mm, described anti-skidding projection spacing≤2mm to each other.In this programme, described anti-skidding protruding distance to each other refers to two adjacent anti-skidding protruding spacings.
In above-mentioned anti-skidding glaze face brick, preferably, described anti-skidding projection spacing is to each other 0.2mm～0.5mm.
Impurity in green body layer impacts printed layer when burning till, and preferably, in above-mentioned anti-skidding glaze face brick, also comprises ground glaze layer between green body layer and printed layer.
In order to make manufacturing process more simple, avoid disconnected glaze or scarce glaze defect, in above-mentioned anti-skidding glaze face brick, described green body layer upper surface is plane.
The present invention also provides a kind of method of manufacturing above-mentioned anti-skidding glaze face brick: it comprises the steps:
Step 1): stamp; Select dried ceramic body, on its surface, carry out stamp, form printed layer;
Step 2): charity high temperature clear frit; By particle diameter≤20 object high temperature clear frit particle charity in the billet surface after step 1) stamp;
Step 3: enter klining; Under roller kiln oxidizing atmosphere to step 2) base substrate of charity high temperature clear frit particle burns till, firing temperature is 1150 ℃～1230 ℃, firing period is 80～120 minutes;
Step 4: edging chamfering; After the adobe of burning till until step 3) is cooling, after edging chamfering, can obtain anti-skidding glaze face brick finished product.
Preferably, 1250 ℃ of yield temperature >, the hemispherical temperature scope of above-mentioned high temperature clear frit are identical with firing range described in step 3).In the above conditions, can guarantee high temperature clear frit incomplete fusion effect, make the transparent cover coat and the base substrate that form have good bonding force, can form again the anti-skidding projection of good antiskid effect.
In order to avoid the impact on printed layer of impurity in green body layer, preferably, in aforesaid method, before step 1) stamp, first at billet surface charity one deck milkiness ground-coat enamel.Milkiness ground-coat enamel mainly plays covering effect, whiteness >=80 degree after burning, and it can select zirconium base opaque glaze, also can select phosphorus boron or the heterogeneous opaque glaze of boron calcium.
Because the draft of roller kiln kiln hood blower fan is larger, and step 2) in the high temperature clear frit granularity of charity little, be easy to be sucked away, therefore in step 2) in after charity high temperature clear frit, also comprise the operation of a sprinkling fixing agent.Fixing agent can be fixed on high temperature clear frit on base substrate, and fixing agent can be selected carboxymethyl cellulose aqueous solution etc.
Certainly, can also adopt following scheme to solve because the draft of roller kiln kiln hood blower fan is larger, the problem that high temperature clear frit is sucked away.Can be by step 2) in to use particle diameter≤30 object high temperature clear frit particle be that to add proportion be in 1.6～1.9 transparent slurry, the compound forming after stirring, its cloth is imposed on to the billet surface after step 1) stamp, glaze layer thickness≤the 0.5mm(forming accordingly, burn till formation transparent cover coat thickness also≤0.5mm, if transparent cover coat is blocked up, transparent high-temperature frit particle is difficult to protrude the anti-skidding projection of formation), wherein the mass ratio of high temperature clear frit particle and transparent slurry is 1:1～5.Like this, when step 3) enters klining and becomes, because high temperature clear frit is to be wrapped in glaze layer, therefore can not siphoned away by kiln hood blower fan, glaze melting when burning till, because of the yield temperature of firing temperature lower than high temperature clear frit, so high temperature clear frit can be dispersed on transparent cover coat and form anti-skidding projection after burning.
Here need above high temperature clear frit to do following explanation: at architectural pottery production field, frit refers to a kind of glass state material, and it can be used as the main raw material of glaze, in the field of businessly conventionally the frit being applicable at 1100 ℃ of firing temperatures is called to low temperature frit; The frit that is applicable to 1100 ℃～1250 ℃ of firing temperatures is called middle temperature frit; Be applicable to 1250 ℃ of above frits of firing temperature and be called high temperature frit.The transparence presenting after frit burns till, as the another kind of mode of distinguishing its kind, can see through the clear frit that is called of most of light; The very low lighttight milkiness frit that is called even completely of transmittance; Marginally be called translucent frit.The high temperature clear frit of mentioning in the present invention can be with reference to this section of explanation.
Compared with the existing technology, anti-skidding glaze face brick tool provided by the invention has the following advantages:
1, skidproof effect is better.Anti-skidding glaze face brick provided by the invention is next anti-skidding by have anti-skidding projection on transparent cover coat, and compared to the scheme that adopts punching press anti-slip veins in adobe, friction area is larger, good antiskid effect.
2, glaze quality is good, and on printed layer decorative effect without impact.The present invention adopts transparent cover coat, and when having skidproof effect, transparent cover coat can well present the decorative effect of printed layer, and the intensive anti-skidding projection having is under light refraction effect, can allow printed layer pattern more three-dimensional.
Accompanying drawing explanation
Fig. 1 is the cross section structure schematic diagram in prior art with the ornamental brick of skidproof effect.
Fig. 2 is the cross section structure schematic diagram of the anti-skidding glaze face brick that provides of the embodiment of the present invention 1.
Fig. 3 is the cross section structure schematic diagram of the anti-skidding glaze face brick that provides of the embodiment of the present invention 2.
Drawing reference numeral explanation: 101-green body layer; 201-ground glaze layer; 301-printed layer; 401-transparent cover coat.
Embodiment
Below in conjunction with accompanying drawing and by embodiment, further illustrate technical scheme of the present invention.Need to illustrate that accompanying drawing, only for explanation the present invention program, not in strict accordance with scale, does not therefore form any limitation of the invention, and wherein for needs are described, may have local zooming in or out.
With reference to accompanying drawing 1, accompanying drawing 1 provides the cross section structure schematic diagram of the ornamental brick in prior art with skidproof effect.It provides a kind of ornamental brick with printed layer 301.Here should illustrate, for there is no printed layer, be only that the ornamental brick of glazing in green body layer 101 also can be used as reference.Feature at these series product is that the anti-slip veins with concave convex texture is set in green body layer, then after glazing, glaze can rise and fall along with anti-slip veins, with this, reaches anti-skidding object.But because pattern and the degree of depth of anti-slip veins is subject to the thick restriction of glaze, be difficult to play good skidproof effect, and when anti-slip veins is narrower and when darker, easily occur lacking glaze, the defect of the glaze that breaks.The present invention is by adopting particle diameter≤20 object high temperature clear frit particle as the raw material that forms transparent cover coat for this reason, it is (1250 ℃) incomplete fusion under the highest sintering temperature of adobe, the softening liquid phase forming is bonded to each other particle, but not exclusively sprawl, on transparent cover coat, form anti-skidding projection.Below we are elaborated by embodiment 1 and 2 couples of the present invention program of embodiment.
In addition, for high temperature clear frit, can be by buying and obtain in colour glaze company, the clear frit for example using in embodiment provided by the invention is that Quincy's Caro is bought and obtained than glaze company, the similar frit product of other company also can be realized this programme certainly.In addition, can also be with reference to < < glaze and colorant > > [day] element wood ocean one work; Liu Kedong, Liu Guangyue is translated.-Beijing: China Construction Industry Press, publish in December, 1979.At < < glaze and colorant > > mono-book, be textbook known in this field, component formula wherein and utilize method that Sai Geshi determines glaze or frit formula to know for those skilled in the art.Therefore only need provide firing temperature for those skilled in the art, and the kind of glaze just can find corresponding chemical composition scope in book, and then can determine and specifically fill a prescription and glazing process parameter according to the mineral composition of used raw material.
Embodiment 1
With reference to Fig. 2, in the present embodiment, provide a kind of anti-skidding glaze face brick, it comprises green body layer 101 from the bottom to top, printed layer 301, transparent cover coat 401, wherein on transparent cover coat 401, having is highly the anti-skidding projection of 0.1mm～0.6mm, described anti-skidding projection spacing≤2mm to each other.
This kind of anti-skidding glaze face brick can be prepared as follows:
Select the middle temperature blank raw material that ornamental brick is conventional (to be firing temperature between the blank raw material of 1100 ℃～1250 ℃, with plastic clay, feldspar, sand, additive (additive can include but not limited to softening agent, water reducer etc.) etc., to add water for ball milling and make slurry; Then after deironing, the operation such as old, be delivered to the dry powder of making of spray-drying tower spraying; Again powder is delivered to the impact briquetting of formation system cloth, makes adobe, select in the present embodiment 600 * 600(mm) specification, mould coefficient is 1.09; It is dry that dry kiln is sent in the adobe of making; Dried base substrate is after the cleaning of surface, and stamp forms printed layer; Printing technology can select silk screen, cylinder, ink-jet or above several stamp mode to combine, select in the present embodiment ink-jet printed mode to form printed layer, printing machine is the ink-jet decorating machine of wishing that pottery machine is produced, and ink is palm fibre, Huang, indigo plant, brown four chromatic inks that Yi Dajia (esmaglassitaca) company produces; After stamp, dispense transparent high-temperature frit, particle diameter≤20 order of transparent high-temperature frit (formed so anti-skidding hill height is 0.1mm～0.6mm), then spray fixing agent, the aqueous solution that is carboxymethyl cellulose by the fixing agent of selecting in the present embodiment; Enter roller kiln oxidizing atmosphere and burn till, firing temperature is 1150 ℃～1230 ℃, and firing period is 80～120 minutes; Goods kiln discharge is cooling by after edging chamfered, can obtain finished product.
The anti-skidding glaze face brick that this programme provides, utilizes high temperature frit incomplete fusion in sintering process, and the softening liquid phase forming is bonded to each other particle, but not exclusively sprawls, and has intensive anti-skidding projection and play anti-skidding effect on transparent cover coat.It is larger that it has friction area, good antiskid effect; And the clear printed layer pattern that presents of energy; In production technique, select conventional mould, without for the extra die sinking of anti-slip veins is set in green body layer 101, more not because anti-slip veins is to each other apart from little, the problems such as the scarce glaze that lines causes occurs while being difficult to stamp and glazing, disconnected glaze.
Embodiment 2
With reference to Fig. 3, in the present embodiment, provide a kind of anti-skidding glaze face brick, it comprises green body layer 101 from the bottom to top, ground glaze layer 201, printed layer 301, transparent cover coat 401, wherein on transparent cover coat 401, having is highly the anti-skidding projection of 0.1mm～0.5mm, described anti-skidding projection spacing≤2mm to each other.
In the present embodiment, select following technique to prepare above-mentioned anti-skidding glaze face brick.
Select the middle temperature blank raw material that ornamental brick is conventional (to be firing temperature between the blank raw material of 1100 ℃～1250 ℃, with plastic clay, feldspar, sand, additive (additive can include but not limited to softening agent, water reducer etc.) etc., to add water for ball milling and make slurry; Then after deironing, the operation such as old, be delivered to the dry powder of making of spray-drying tower spraying; Again powder is delivered to the impact briquetting of formation system cloth, makes adobe, select in the present embodiment 600 * 600(mm) specification, mould coefficient is 1.09; It is dry that dry kiln is sent in the adobe of making; Dried base substrate is after the cleaning of surface, water spray is wetting, then execute ground-coat enamel and form ground glaze layer 201, ground-coat enamel is chosen as the opaque glaze of strong covering power, and its effect is to prevent that the impurity of green body layer 101 from can select the ground-coat enamel of chemical composition in the present embodiment on the impact of printed layer: silicon-dioxide 55.5%～61.5%; Aluminum oxide: 8.5%～11.5%; Ferric oxide :≤0.09%; Calcium oxide: 7.5%～12.5%; Boron oxide: 7.5%～10.5%; Magnesium oxide :≤1.0%; Sodium oxide: 1.0%～2.0%; Zinc oxide: 5.0%～6.0%; Potassium oxide: 9.0%～10.0%; Lithium Oxide 98min :≤1.0%; Anatase type titanium oxide: 0.5%, glazing mode is for drenching glaze, and glaze slip proportion is 1.80,325 mesh screen residues 1～2%, mobility < 100S; Execute after ground-coat enamel stamp again and form printed layer; Printing technology can select silk screen, cylinder, ink-jet or above several stamp mode to combine, select in the present embodiment ink-jet printed mode to form printed layer, printing machine is the ink-jet decorating machine of wishing that pottery machine is produced, and ink is palm fibre, Huang, indigo plant, brown four chromatic inks that Yi Dajia (esmaglassitaca) company produces; After stamp, dispense transparent high-temperature clear frit, particle diameter 30～100 object particles of high temperature transparent high-temperature frit particle account for the more than 90% of total amount, and all the other are the particle below 100 orders; Different from embodiment 1 at the present embodiment 2, selecting above high temperature clear frit to add proportion is in 1.6～1.9 transparent slurry, after stirring, cloth imposes on the billet surface after stamp again, glaze layer thickness≤the 0.5mm(forming accordingly, burn till formation transparent cover coat 401 thickness also≤0.5mm, if transparent cover coat is blocked up, transparent high-temperature frit particle is difficult to protrude the anti-skidding projection of formation), wherein the mass ratio of high temperature clear frit and transparent slurry is 1:1～5; Enter roller kiln oxidizing atmosphere and burn till, firing temperature is 1150 ℃～1230 ℃, and firing period is 80～120 minutes; Goods kiln discharge is cooling by after edging chamfered, can obtain finished product.
By high temperature clear frit powder is added in transparent slurry, can avoid when burning till in the present embodiment, because kiln hood blower fan has been taken out greatly, and make the problem that high temperature clear frit is sucked away.After burning till, high temperature clear frit is dispersed in transparent uniformly, and its projection that does not have complete melting to form has formed the anti-skidding projection on transparent cover coat 401, makes this kind of throwing glazed brick have skidproof effect.In addition, the skidproof effect when anti-skidding projection spacing is to each other 0.2mm～0.5mm is better.
Know-why of the present invention has below been described in conjunction with specific embodiments.These are described is in order to explain principle of the present invention, and can not be interpreted as by any way limiting the scope of the invention.Explanation based on herein, those skilled in the art does not need to pay performing creative labour can associate other embodiment of the present invention, within these modes all will fall into protection scope of the present invention.
Claims (8)
1. a method of manufacturing anti-skidding glaze face brick: it comprises the steps:
Step 1): stamp; Select dried ceramic body, on its surface, carry out stamp, form printed layer;
Step 2): charity high temperature clear frit; By particle diameter≤20 object high temperature clear frit particle charity in the billet surface after step 1) stamp;
Step 3: enter klining; Under roller kiln oxidizing atmosphere to step 2) base substrate of charity high temperature clear frit particle burns till, firing temperature is 1150 ℃～1230 ℃, firing period is 80～120 minutes;
Step 4: edging chamfering; After the adobe of burning till until step 3) is cooling, after edging chamfering, can obtain anti-skidding glaze face brick finished product.
2. the method for manufacture anti-skidding glaze face brick as claimed in claim 1, is characterized in that, 1250 ℃ of the yield temperature > of described high temperature clear frit, hemispherical temperature scope are identical with firing range described in step 3).
3. the method for manufacture anti-skidding glaze face brick as claimed in claim 1 or 2, is characterized in that, before step 1) stamp, first at billet surface charity one deck milkiness ground-coat enamel.
4. the method for manufacture anti-skidding glaze face brick as claimed in claim 1, is characterized in that, in step 2) in after charity high temperature clear frit, also comprise an operation of spraying fixing agent.
5. the method for manufacture anti-skidding glaze face brick as claimed in claim 4, is characterized in that, described fixing agent is carboxymethyl cellulose aqueous solution.
6. a method of manufacturing anti-skidding glaze face brick: it comprises the steps:
Step 1): stamp; Select dried ceramic body, on its surface, carry out stamp, form printed layer;
Step 2): charity high temperature clear frit; By particle diameter≤30 object high temperature clear frit particle, be that to add proportion be in 1.6～1.9 transparent slurry, after stirring, form compound, again its cloth of compound is imposed on to the billet surface after step 1) stamp, glaze layer thickness≤the 0.5mm forming, wherein, the mass ratio of described high temperature clear frit particle and described transparent slurry is 1:1～5;
Step 3: enter klining; Under roller kiln oxidizing atmosphere to step 2) base substrate of charity high temperature clear frit particle burns till, firing temperature is 1150 ℃～1230 ℃, firing period is 80～120 minutes;
Step 4: edging chamfering; After the adobe of burning till until step 3) is cooling, after edging chamfering, can obtain anti-skidding glaze face brick finished product.
7. the method for manufacture anti-skidding glaze face brick as claimed in claim 6, is characterized in that, 1250 ℃ of the yield temperature > of described high temperature clear frit, hemispherical temperature scope are identical with firing range described in step 3).
8. the method for the manufacture anti-skidding glaze face brick as described in claim 6 or 7, is characterized in that, particle diameter 30～100 object particles of described high temperature clear frit particle account for the more than 90% of total amount, and all the other are the particle below 100 orders.
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| CN201310614314.6A CN103588510B (en) | 2013-11-28 | 2013-11-28 | Method for manufacturing anti-slip glazed tile |
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Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN104230387A (en) * | 2014-09-23 | 2014-12-24 | 佛山市禾才科技服务有限公司 | Production method of pattern glazed ceramic tile |
| CN106477886A (en) * | 2016-09-27 | 2017-03-08 | 佛山市东鹏陶瓷有限公司 | A kind of adobe of glazed tile improving surface anti-skidding performance and preparation method thereof |
| CN106698945A (en) * | 2017-01-03 | 2017-05-24 | 澧县新鹏陶瓷有限公司 | Glazed tile with waste glaze as glaze raw material and preparation method thereof |
| CN107417121A (en) * | 2017-08-18 | 2017-12-01 | 佛山市石湾裕龙陶瓷有限公司 | A kind of ceramics with anti-skidding glaze |
| CN108545944A (en) * | 2018-06-29 | 2018-09-18 | 佛山石湾鹰牌陶瓷有限公司 | The preparation method and ship-and-galley tile of ship-and-galley tile |
| CN108546159A (en) * | 2018-06-29 | 2018-09-18 | 佛山石湾鹰牌陶瓷有限公司 | The preparation method and ship-and-galley tile of ship-and-galley tile |
| CN112851369A (en) * | 2021-01-28 | 2021-05-28 | 成都新西南陶瓷艺术股份公司 | Production process of anti-skid ceramic tile |
| CN114521220A (en) * | 2020-02-10 | 2022-05-20 | 东兴聚合体株式会社 | Tile type floor finishing material containing anti-slip foam and method for preparing the same |
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Cited By (11)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN104230387A (en) * | 2014-09-23 | 2014-12-24 | 佛山市禾才科技服务有限公司 | Production method of pattern glazed ceramic tile |
| CN104230387B (en) * | 2014-09-23 | 2016-06-29 | 佛山市禾才科技服务有限公司 | A kind of production method of pattern glazed ceramic brick |
| CN106477886A (en) * | 2016-09-27 | 2017-03-08 | 佛山市东鹏陶瓷有限公司 | A kind of adobe of glazed tile improving surface anti-skidding performance and preparation method thereof |
| CN106477886B (en) * | 2016-09-27 | 2019-01-22 | 佛山市东鹏陶瓷有限公司 | A kind of adobe of glazed tile and preparation method thereof improving surface anti-skidding performance |
| CN106698945A (en) * | 2017-01-03 | 2017-05-24 | 澧县新鹏陶瓷有限公司 | Glazed tile with waste glaze as glaze raw material and preparation method thereof |
| CN107417121A (en) * | 2017-08-18 | 2017-12-01 | 佛山市石湾裕龙陶瓷有限公司 | A kind of ceramics with anti-skidding glaze |
| CN108545944A (en) * | 2018-06-29 | 2018-09-18 | 佛山石湾鹰牌陶瓷有限公司 | The preparation method and ship-and-galley tile of ship-and-galley tile |
| CN108546159A (en) * | 2018-06-29 | 2018-09-18 | 佛山石湾鹰牌陶瓷有限公司 | The preparation method and ship-and-galley tile of ship-and-galley tile |
| CN108545944B (en) * | 2018-06-29 | 2021-02-26 | 佛山石湾鹰牌陶瓷有限公司 | Preparation method of anti-skid floor tile and anti-skid floor tile |
| CN114521220A (en) * | 2020-02-10 | 2022-05-20 | 东兴聚合体株式会社 | Tile type floor finishing material containing anti-slip foam and method for preparing the same |
| CN112851369A (en) * | 2021-01-28 | 2021-05-28 | 成都新西南陶瓷艺术股份公司 | Production process of anti-skid ceramic tile |
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| CN103588510B (en) | 2015-04-22 |
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