CN103585044B - Cleaning care solution and manufacturing process thereof - Google Patents
Cleaning care solution and manufacturing process thereof Download PDFInfo
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- CN103585044B CN103585044B CN201310413790.1A CN201310413790A CN103585044B CN 103585044 B CN103585044 B CN 103585044B CN 201310413790 A CN201310413790 A CN 201310413790A CN 103585044 B CN103585044 B CN 103585044B
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Abstract
The invention discloses a cleaning care solution which is prepared from the following substances in percentage by weight: 0.2-0.3% of bactericide, 0.1-0.25% of dipotassium glycyrrhetate, 0.1-0.4% of menthol, 0.2-0.3% of stuffing, 1-3% of emollient, 0.05-0.2% of pH value regulator, 1-3% of thickening agent, 0.02-0.1% of humectant, 10-15% of sodium lauroyl oat amino acid, 15-25% of disodium cocoamphodiacetate, 15-25% of cocamidopropyl betaine and the balance of pure water, wherein the thickening agent is a mixture of Acacia senegal gum and xanthan gum, or PEG-150 distearate or methyl hydroxyethyl cellulose; and the bactericide is 2,4,4'-trichloro-2'-hydroxydiphenyl ether. The cleaning care solution has favorable antimicrobial effect, has an odor removing function, contains no perfume and greatly increases the use safety of the care solution.
Description
Technical field
The present invention relates to a kind of manufacture technology field of cleaning-nursing liquid, particularly relate to a kind of cleaning-nursing liquid for privacy places of human body and processing technology thereof.
Background technology
In daily life, people are women especially, need to clean privacy places-privates, various disinfectant, fancy soap, bath gel can be adopted to carry out when cleaning, but current this kind of articles for use are higher containing the composition of alkalescence, the sour environment of easy destruction privates, makes the self-cleaning function of privates weaken, and more easily makes antibacterial multiply and cause discomfort.Some current cleaning-nursing liquid, the antibacterial used, antiseptic, essence, surfactant all seldom carry out limiting the quantity, limit the use of, the consideration of drug resistance aspect, and have employed the material that some zests are large, biological degradability is poor, this have impact on safety in utilization and the comfortableness of nursing materials.
As can be seen here, how prior art is improved, a kind of cleaning-nursing liquid for privacy places is provided, it can keep the acid-base balance of vagina, and gentleness does not stimulate, effective anti-bacteria, use safety, this is the current technical issues that need to address in this area.
Summary of the invention
In order to solve above-mentioned the deficiencies in the prior art, the object of the invention is to, provide a kind of cleaning-nursing liquid, can keep the acid-base balance of vagina, gentleness does not stimulate, effective anti-bacteria, use safety.Based on this, the present invention also provides a kind of processing technology of cleaning-nursing liquid.
For solving above technical problem, technical scheme of the present invention is:
A kind of cleaning-nursing liquid, be made up of the material of following percentage by weight:
Antibacterial 0.2% ~ 0.3%;
Glycyrrhizic acid dipotassium 0.1% ~ 0.25%;
Mentholum 0.1% ~ 0.4%;
Filler 0.2% ~ 0.3%;
Emollient 1% ~ 3%;
PH value regulator 0.05% ~ 0.2%;
Thickening agent 1% ~ 3%;
Wetting agent 0.02% ~ 0.1%;
Lauroyl Herba bromi japonici amino acid sodium 10% ~ 15%;
Cocos nucifera oil acyl both sexes base oxalic acid disodium 15% ~ 25%;
Cocamido propyl betaine 15% ~ 25%;
Surplus is pure water;
Described thickening agent is the mixture of arabic gum natural gum and xanthan gum, or is PEG-150 distearate or methyl hydroxyethylcellulose; Described antibacterial is the chloro-2'-dihydroxy diphenyl ether of 2,4,4'-tri-.
Preferably, described wetting agent is any one or the two or more mixture in hyaluronic acid, water solublity olive oil, Jojoba oil.
Preferably, described emollient is the mixture of hydroxylating soybean phospholipid and glycerol, or is any one or the two or more mixture in lanoline, water-soluble silicon oil, PEG-7 glycerol coconut oil fat.
Preferably, described pH value regulator is lactic acid and/or citric acid.
The processing technology of aforementioned cleaning-nursing liquid, comprises the steps:
1) at normal temperatures the gelatin polymer that chloro-for 2,4,4'-tri-2'-dihydroxy diphenyl ether, thickening agent, the filler of part formulation amount, wetting agent are mixed to form is added pure water and be stirred to dissolving;
2) add lauroyl Herba bromi japonici amino acid sodium, cocos nucifera oil acyl both sexes base oxalic acid, cocamido propyl betaine disodium again, stir while adding, make mixed liquor uniformly clarify Gel mile of state;
3) add the filler of emollient, glycyrrhizic acid dipotassium, Mentholum, surplus again, stir while adding, make mixed liquor uniformly emulsus mastic;
4) finally add the aqueous solution that pH value regulator and surplus pure water make and supply the water yield, start homogenizer, with rotating speed 2600r/min ~ 3000r/min homogenizing 8 ~ 12min;
Described thickening agent is the mixture of arabic gum natural gum and xanthan gum, or is PEG-150 distearate or methyl hydroxyethylcellulose.
Preferably, the process obtaining gelatin polymer in step 1) is specially: by weight, by dispersed for the water of 1 part of thickening agent and 3 ~ 5 parts; Then add the chloro-2'-dihydroxy diphenyl ether of 2,4,4'-tri-, the filler of part formulation amount stirs, standing and reacting 10 ~ 30 minutes, obtains jelly; Wetting agent is added in described jelly and mixes, make transparent gelatin polymer.
Preferably, step 1) and step 2) in, the speed of stirring is 30r/min ~ 50r/min, and mixing time is 8min ~ 12min; In step 3), the speed of stirring is 30r/min ~ 50r/min, and mixing time is 4min ~ 6min.
Preferably, described wetting agent is any one or the two or more mixture in hyaluronic acid, water solublity olive oil, Jojoba oil.
Preferably, described emollient is the mixture of hydroxylating soybean phospholipid and glycerol, or is any one or the two or more mixture in lanoline, water-soluble silicon oil, PEG-7 glycerol coconut oil fat; Described pH value regulator is lactic acid or citric acid, and described filler is sodium citrate.
Preferably, step 3) is specially: by Mentholum and emollient dispersed; Then the filler adding surplus stirs, and standing and reacting 10 ~ 30 minutes, obtains jelly; Glycyrrhizic acid dipotassium is added in jelly and mixes, make emulsus mastic.
Compared with prior art, the present invention passes through antibacterial---and 2,4,4'-tri-chloro-2'-dihydroxy diphenyl ether, Radix Glycyrrhizae extract-glycyrrhizic acid dipotassium, Mentholum join in formula as antibacterial, antiallergic, antipruritic composition with reasonable compatibility, mix with wetting agent, pH value regulator and thickening agent, filler, foaming agent, make obtain cleaning-nursing liquid, this cleaning-nursing liquid be used for clean Private Parts time, harmful bacteria can be suppressed to invade, promote probiotics growth; It is faintly acid, and can balance secret place environment, life-time service does not produce dependency; It can moisten, take good care of the tender skin of children of privacy places, character is gentle and do not stimulate, adopt lauroyl Herba bromi japonici amino acid sodium, cocos nucifera oil acyl both sexes base oxalic acid disodium, cocamido propyl betaine as foaming, foam enhancing composition simultaneously, cleaning-nursing liquid of the present invention is made to possess good frothing capacity, effective ingredient effectively can be disperseed to the position of needs nursing, improve conditioning liquid composition in the nursing position time of staying.
Compared with existing conditioning liquid, component prescription aspect of the present invention, can keep the acid-base balance of vagina, owing to adopting the foaming ingredient in natural green source, feel is extremely comfortable, contains the elite of natural plants, gentle sterilization, not Diazolidinyl Urea, feels refrigerant pleasant, fragrant odour after using, life-time service can keep the acid-base balance of vagina, menstrual period are antipruritic with warding off taste, and the growth of effective anti-bacteria prevents and prevent the generation of various gynecological inflammation.The Mentholum composition that formula of the present invention contains has clean function of odor, without the need to adding essence in formula, considerably increases the safety in utilization of conditioning liquid.In addition, formula raw material easily obtains, low price, and production cost is low.
Detailed description of the invention
For making technical scheme of the present invention clearly, below in conjunction with being come by specific embodiment, the present invention is described in detail.
Cleaning-nursing liquid of the present invention, be made up of the material of following percentage by weight:
Antibacterial 0.2% ~ 0.3%;
Glycyrrhizic acid dipotassium 0.1% ~ 0.25%;
Mentholum 0.1% ~ 0.4%;
Filler 0.2% ~ 0.3%;
Emollient 1% ~ 3%;
PH value regulator 0.05% ~ 0.2%;
Thickening agent 1% ~ 3%;
Wetting agent 0.02% ~ 0.1%;
Lauroyl Herba bromi japonici amino acid sodium 10% ~ 15%;
Cocos nucifera oil acyl both sexes base oxalic acid disodium 15% ~ 25%;
Cocamido propyl betaine 15% ~ 25%;
Surplus is pure water;
Described thickening agent is the mixture that arabic gum natural gum and xanthan gum mix with arbitrary proportion, or is PEG-150 distearate or methyl hydroxyethylcellulose; Described antibacterial is the chloro-2'-dihydroxy diphenyl ether of 2,4,4'-tri-.
Wherein, as preferred scheme, described wetting agent is any one or two or more mixture in hyaluronic acid, water solublity olive oil, Jojoba oil.Wherein, more preferably, adopt hyaluronic acid, it can play water holding, moisturizing, care effect, food grade materials, and safety is good.
Wherein, as preferred scheme, described emollient is the mixture of hydroxylating soybean phospholipid and glycerol, or is any one or the two or more mixture in lanoline, water-soluble silicon oil, PEG-7 glycerol coconut oil fat.Wherein, more preferably, adopt the mixture of hydroxylating soybean phospholipid and glycerol, there is lubrication, nourishing, nutrition, sebum adjustment, strengthen elastic effect.
Wherein, as preferred scheme, described pH value regulator is lactic acid and/or citric acid.Wherein, more preferably, adopt lactic acid, it is natural pH value regulator, and gentleness does not stimulate.
Wherein, as preferred scheme, described filler is sodium citrate.
Radix Glycyrrhizae is a kind of tonification Chinese herbal medicine, and function cures mainly heat-clearing and toxic substances removing.Radix Glycyrrhizae, be apt to control urethralgia, urinary tract drenches, and SHENGCAO saves should subside a swelling poison, sharp joint; Radix Glycyrrhizae, lays particular stress on interior-heat clearly, eliminating heart-fire.Be both a thing, it is different that it concocts institute, then effect is also other.Radix Glycyrrhizae is controlled uncontrolled urination and itches: Radix Glycyrrhizae one chi, and cuts, and with five liters, water, boil and get three liters, stain washes it, day three, five degree.Treatment of smallpox skin ulcer excessive thirst: Radix Glycyrrhizae (processing), radices trichosanthis decile, be decocted in water for oral dose it, has antiinflammatory, antiviral, and the effect such as protecting liver and detoxication and enhancing immunologic function.Because glycyrrhizic acid has the pharmacological action of glucocorticoid sample without serious adverse reaction, be clinically widely used in treating various acute, chronic hepatitis, bronchitis and acquired immune deficiency syndrome (AIDS), also there is the functions such as anti-cancer and cancer-preventing, interferon inducer and cell immunomodulator.Extracted by Radix Glycyrrhizae that obtained derivant---glycyrrhizic acid dipotassium is anti-allergic agent, pharmaceutical grade, stop the release of histamine, have the effect such as antiinflammatory, antiallergic.
Mentholum is freshener, and USP level acts on skin or mucosa, has refrigerant itching-relieving action, taste of clearly dispelling, and Absorbable rod Sum decomposition abnormal flavour in menstrual period, life-time service no longer disturbs by abnormal flavour.
2,4, the chloro-2'-dihydroxy diphenyl ether of 4'-tri-is as antibacterial, belong to triclosan antimicrobial agent, as the most frequently used in chlorinated biphenyl ether family and that drug effect is the strongest antibacterial, to gram positive bacteria, comparatively gram-negative bacteria is more effective, as the common bacteria staphylococcus aureus of Postoperative infection in triclosan antimicrobial agent.Triclosan is easily degraded in environment around, does not produce bacterial drug resistance, the bactericidal effect effectively good to staphylococcus aureus, escherichia coli, Candida albicans.
The mixture of arabic gum natural gum and xanthan gum has thickening, gel, soft and smooth effect.
Lauroyl Herba bromi japonici amino acid sodium is surfactant, and natural, the foaming power of originating is strong, and feel is extremely gentle, comfortable.
Cocos nucifera oil acyl both sexes base oxalic acid disodium is the gentleest amphoteric surfactant, and medium foaming capacity, without degreasing power.
Cocamido propyl betaine is not glycerinated cocamido propyl betaine, foam enhancing, and performance is gentle.
The processing technology of a kind of cleaning-nursing liquid of the present invention, comprises the steps:
1) at normal temperatures the gelatin polymer that chloro-for 2,4,4'-tri-2'-dihydroxy diphenyl ether, thickening agent, the filler of part formulation amount, wetting agent are mixed to form is added pure water and be stirred to dissolving;
2) add lauroyl Herba bromi japonici amino acid sodium, cocos nucifera oil acyl both sexes base oxalic acid, cocamido propyl betaine disodium again, stir while adding, make mixed liquor uniformly clarify Gel mile of state;
3) add the filler of emollient, glycyrrhizic acid dipotassium, Mentholum, surplus again, stir while adding, make mixed liquor uniformly emulsus mastic;
4) the pH value regulator aqueous solution finally adding surplus supplies the water yield, starts homogenizer, with rotating speed 2600r/min ~ 3000r/min homogenizing 8 ~ 12min;
Described thickening agent is the mixture of arabic gum natural gum and xanthan gum, or is PEG-150 distearate or methyl hydroxyethylcellulose.
Preferably, in step 1), the process of obtained gelatin polymer is specially: by weight, by dispersed for the water of 1 part of thickening agent and 3 ~ 5 parts; Then add the chloro-2'-dihydroxy diphenyl ether of 2,4,4'-tri-, the filler of part formulation amount stirs, standing and reacting 10 ~ 30 minutes, obtains jelly; Wetting agent is added in described jelly and mixes, make transparent gelatin polymer.
Preferably, step 1) and step 2) in, the speed of stirring is 30r/min ~ 50r/min, and mixing time is 8 ~ 12min; In step 3), the speed of stirring is 30r/min ~ 50r/min, and mixing time is 4 ~ 6min.
Preferably, step 3) is specially: by Mentholum and emollient dispersed; Then the filler adding surplus stirs, and standing and reacting 10 ~ 30 minutes, obtains jelly; Glycyrrhizic acid dipotassium is added in jelly and mixes, make emulsus mastic.
Embodiment one
Cleaning-nursing liquid in the present embodiment, be made up of the material of following percentage by weight:
Antibacterial 0.2%;
Glycyrrhizic acid dipotassium 0.1%;
Mentholum 0.3%;
Filler 0.25%;
Emollient 2%;
PH value regulator 0.15%;
Thickening agent 2%;
Wetting agent 0.08%;
Lauroyl Herba bromi japonici amino acid sodium 12%;
Cocos nucifera oil acyl both sexes base oxalic acid disodium 18%;
Cocamido propyl betaine 23%;
Surplus is pure water;
Described thickening agent is the mixture of arabic gum natural gum and xanthan gum; Described antibacterial is the chloro-2'-dihydroxy diphenyl ether of 2,4,4'-tri-.
Wherein, described wetting agent is hyaluronic acid; Described emollient is the mixture of hydroxylating soybean phospholipid and glycerol; Described pH value regulator is lactic acid; Described filler is sodium citrate.
The processing technology of aforesaid cleaning-nursing liquid, comprises the steps:
Comprise the steps:
1) at normal temperatures the gelatin polymer that chloro-for 2,4,4'-tri-2'-dihydroxy diphenyl ether, thickening agent, the filler of part formulation amount, wetting agent are mixed to form is added pure water and be stirred to dissolving;
2) add lauroyl Herba bromi japonici amino acid sodium, cocos nucifera oil acyl both sexes base oxalic acid, cocamido propyl betaine disodium again, stir while adding, make mixed liquor uniformly clarify Gel mile of state;
3) add the filler of emollient, glycyrrhizic acid dipotassium, Mentholum, surplus again, stir while adding, make mixed liquor uniformly emulsus mastic;
4) aqueous solution that the pure water finally adding pH value regulator and surplus is made supplies the water yield, starts homogenizer, with rotating speed 3000r/min homogenizing 8min;
Wherein, step 1) is specially: by weight, by dispersed for the water of the mixture of 1 part of arabic gum natural gum and xanthan gum and 3 parts; Then the filler adding the chloro-2'-dihydroxy diphenyl ether of 2,4,4'-tri-and account for total formula weight 0.2% stirs, and standing and reacting 12 minutes, obtains jelly; The wetting agent of whole formula ratio is added in described jelly and mixes, make transparent gelatin polymer.
Wherein, step 1) and step 2) in, the speed of stirring is 30r/min, and mixing time is 12min; The speed of step 3), stirring is 35r/min, and mixing time is 6min.
Wherein, step 3) is specially: by Mentholum and emollient dispersed; Then the filler adding surplus stirs, and standing and reacting 20 minutes, obtains jelly; Glycyrrhizic acid dipotassium is added in jelly and mixes, make emulsus mastic.
Embodiment two
Cleaning-nursing liquid in the present embodiment, be made up of the material of following percentage by weight:
Antibacterial 0.25%;
Glycyrrhizic acid dipotassium 0.15%;
Mentholum 0.35%;
Filler 0.2%;
Emollient 1%;
PH value regulator 0.2%;
Thickening agent 1%;
Wetting agent 0.05%;
Lauroyl Herba bromi japonici amino acid sodium 15%;
Cocos nucifera oil acyl both sexes base oxalic acid disodium 16%;
Cocamido propyl betaine 20%;
Surplus is pure water;
Described thickening agent is PEG-150 distearate; Described antibacterial is the chloro-2'-dihydroxy diphenyl ether of 2,4,4'-tri-.
Wherein, described wetting agent is water solublity olive oil; Described emollient is lanoline; Described pH value regulator is lactic acid; Described filler is sodium citrate, and described thickening agent is PEG-150 distearate.
The processing technology of aforesaid cleaning-nursing liquid, comprises the steps:
Comprise the steps:
1) at normal temperatures the gelatin polymer that chloro-for 2,4,4'-tri-2'-dihydroxy diphenyl ether, thickening agent, the filler of part formulation amount, wetting agent are mixed to form is added pure water and be stirred to dissolving;
2) add lauroyl Herba bromi japonici amino acid sodium, cocos nucifera oil acyl both sexes base oxalic acid, cocamido propyl betaine disodium again, stir while adding, make mixed liquor uniformly clarify Gel mile of state;
3) add the filler of emollient, glycyrrhizic acid dipotassium, Mentholum, surplus again, stir while adding, make mixed liquor uniformly emulsus mastic;
4) aqueous solution that the pure water finally adding pH value regulator and surplus is made supplies the water yield, starts homogenizer, with rotating speed 2600r/min12min;
Wherein, step 1) is specially: by weight, by dispersed for the water of the mixture of 1 part of arabic gum natural gum and xanthan gum and 3 parts; Then the filler adding the chloro-2'-dihydroxy diphenyl ether of 2,4,4'-tri-and account for total formula weight 0.15% stirs, and standing and reacting 23 minutes, obtains jelly; The wetting agent of whole formula ratio is added in described jelly and mixes, make transparent gelatin polymer.
Wherein, step 1) and step 2) in, the speed of stirring is 39r/min, and mixing time is 9min; The speed of step 3), stirring is 45r/min, and mixing time is 4min.
Wherein, step 3) is specially: by Mentholum and emollient dispersed; Then the filler adding surplus stirs, and standing and reacting 25 minutes, obtains jelly; Glycyrrhizic acid dipotassium is added in jelly and mixes, make emulsus mastic.
Embodiment three
Cleaning-nursing liquid in the present embodiment, be made up of the material of following percentage by weight:
Antibacterial 0.3%;
Glycyrrhizic acid dipotassium 0.22%;
Mentholum 0.4%;
Filler 0.4%;
Emollient 2%;
PH value regulator 0.1%;
Thickening agent 2%;
Wetting agent 0.07%;
Lauroyl Herba bromi japonici amino acid sodium 13%;
Cocos nucifera oil acyl both sexes base oxalic acid disodium 21%;
Cocamido propyl betaine 17%;
Surplus is pure water;
Described thickening agent is methyl hydroxyethylcellulose; Described antibacterial is the chloro-2'-dihydroxy diphenyl ether of 2,4,4'-tri-.
Wherein, described wetting agent is Jojoba oil; Described emollient is water-soluble silicon oil; Described pH value regulator is citric acid; Described filler is sodium citrate.
The processing technology of aforesaid cleaning-nursing liquid, comprises the steps:
Comprise the steps:
1) at normal temperatures the gelatin polymer that chloro-for 2,4,4'-tri-2'-dihydroxy diphenyl ether, thickening agent, the filler of part formulation amount, wetting agent are mixed to form is added pure water and be stirred to dissolving;
2) add lauroyl Herba bromi japonici amino acid sodium, cocos nucifera oil acyl both sexes base oxalic acid, cocamido propyl betaine disodium again, stir while adding, make mixed liquor uniformly clarify Gel mile of state;
3) add the filler of emollient, glycyrrhizic acid dipotassium, Mentholum, surplus again, stir while adding, make mixed liquor uniformly emulsus mastic;
4) aqueous solution that the pure water finally adding pH value regulator and surplus is made supplies the water yield, starts homogenizer, with rotating speed 2800r/min homogenizing 10min;
Wherein, step 1) is specially: by weight, by dispersed for the water of the mixture of 1 part of arabic gum natural gum and xanthan gum and 3 parts; Then the filler adding the chloro-2'-dihydroxy diphenyl ether of 2,4,4'-tri-and account for total formula weight 0.3% stirs, and standing and reacting 14 minutes, obtains jelly; The wetting agent of whole formula ratio is added in described jelly and mixes, make transparent gelatin polymer.
Wherein, step 1) and step 2) in, the speed of stirring is 43r/min, and mixing time is 9min; The speed of step 3), stirring is 36r/min, and mixing time is 5min.
Wherein, step 3) is specially: by Mentholum and emollient dispersed; Then the filler adding surplus stirs, and standing and reacting 16 minutes, obtains jelly; Glycyrrhizic acid dipotassium is added in jelly and mixes, make emulsus mastic.
Embodiment four
Cleaning-nursing liquid in the present embodiment, be made up of the material of following percentage by weight:
Antibacterial 0.26%;
Glycyrrhizic acid dipotassium 0.18%;
Mentholum 0.18%;
Filler 0.24%;
Emollient 2.5%;
PH value regulator 0.16%;
Thickening agent 3%;
Wetting agent 0.08%;
Lauroyl Herba bromi japonici amino acid sodium 14%;
Cocos nucifera oil acyl both sexes base oxalic acid disodium 21%;
Cocamido propyl betaine 25%;
Surplus is pure water;
Described thickening agent is the mixture of arabic gum natural gum and xanthan gum; Described antibacterial is the chloro-2'-dihydroxy diphenyl ether of 2,4,4'-tri-.
Wherein, described wetting agent is hyaluronic acid; Described emollient is PEG-7 glycerol coconut oil fat; Described pH value regulator is lactic acid; Described filler is sodium citrate.
The processing technology of aforesaid cleaning-nursing liquid, comprises the steps:
Comprise the steps:
1) at normal temperatures the gelatin polymer that chloro-for 2,4,4'-tri-2'-dihydroxy diphenyl ether, thickening agent, the filler of part formulation amount, wetting agent are mixed to form is added pure water and be stirred to dissolving;
2) add lauroyl Herba bromi japonici amino acid sodium, cocos nucifera oil acyl both sexes base oxalic acid, cocamido propyl betaine disodium again, stir while adding, make mixed liquor uniformly clarify Gel mile of state;
3) add the filler of emollient, glycyrrhizic acid dipotassium, Mentholum, surplus again, stir while adding, make mixed liquor uniformly emulsus mastic;
4) aqueous solution that the pure water finally adding pH value regulator and surplus is made supplies the water yield, starts homogenizer, with rotating speed 2700r/min homogenizing 11min;
Wherein, step 1) is specially: by weight, by dispersed for the water of the mixture of 1 part of arabic gum natural gum and xanthan gum and 3 parts; Then the filler adding the chloro-2'-dihydroxy diphenyl ether of 2,4,4'-tri-and account for total formula weight 0.2% stirs, and standing and reacting 25 minutes, obtains jelly; The wetting agent of whole formula ratio is added in described jelly and mixes, make transparent gelatin polymer.
Wherein, step 1) and step 2) in, the speed of stirring is 43r/min, and mixing time is 9min; The speed of step 3), stirring is 48r/min, and mixing time is 4min.
Wherein, step 3) is specially: by Mentholum and emollient dispersed; Then the filler adding surplus stirs, and standing and reacting 16 minutes, obtains jelly; Glycyrrhizic acid dipotassium is added in jelly and mixes, make emulsus mastic.
The cleaning-nursing liquid that the above embodiment of the present invention obtains is by the inspection of Guangdong Prov. Disease Prevention-control Center (steady survey, pH, microorganism, antibacterial), report display: effective substance: trichloro hydroxyl diphenyl ether content is 0.25%, the relative differences 4%, pH(20 DEG C measured) be about 5.46; Adopt the above embodiment of the present invention to obtain 50% diluent of cleaning-nursing liquid, effect 1min, is 100% to staphylococcus aureus and colibacillary bacteriostasis rate; The above embodiment of the present invention obtains 50% diluent of cleaning-nursing liquid, and effect 1min, is 100% to the bacteriostasis rate of Candida albicans; Meet the regulation of GB15979-2002 " Disposable Sanitary Accessory sanitary standard " completely.
The cleaning-nursing liquid that above for the present invention embodiment is obtained carries out a vaginal mucomembranous irritant test, and result shows, and it belongs to nonirritant to the vaginal mucosa irritation of female sd inbred rats, test basis GB15979-2002 " Disposable Sanitary Accessory sanitary standard ".
The obtained cleaning-nursing liquid of the above embodiment of the present invention is pressed: the SN/T1495-2004 detection method gas phase spectrometry of phthalate ester " in the cosmetics " does not detect <≤5mg/kg.
Below be only the preferred embodiment of the present invention, it should be pointed out that above-mentioned preferred implementation should not be considered as limitation of the present invention, protection scope of the present invention should be as the criterion with claim limited range.For those skilled in the art, without departing from the spirit and scope of the present invention, can also make some improvements and modifications, these improvements and modifications also should be considered as protection scope of the present invention.
Claims (10)
1. a cleaning-nursing liquid, is characterized in that, is made up of the material of following percentage by weight:
Antibacterial 0.2% ~ 0.3%;
Glycyrrhizic acid dipotassium 0.1% ~ 0.25%;
Mentholum 0.1% ~ 0.4%;
Filler 0.2% ~ 0.3%;
Emollient 1% ~ 3%;
PH value regulator 0.05% ~ 0.2%;
Thickening agent 1% ~ 3%;
Wetting agent 0.02% ~ 0.1%;
Lauroyl Herba bromi japonici amino acid sodium 10% ~ 15%;
Cocos nucifera oil acyl both sexes base oxalic acid disodium 15% ~ 25%;
Cocamido propyl betaine 15% ~ 25%;
Surplus is pure water;
Described thickening agent is the mixture of arabic gum natural gum and xanthan gum, or is PEG-150 distearate or methyl hydroxyethylcellulose; Described antibacterial is the chloro-2'-dihydroxy diphenyl ether of 2,4,4'-tri-.
2. cleaning-nursing liquid as claimed in claim 1, is characterized in that, described wetting agent is any one or two or more mixture in hyaluronic acid, water solublity olive oil, Jojoba oil.
3. cleaning-nursing liquid as claimed in claim 1, it is characterized in that, described emollient is the mixture of hydroxylating soybean phospholipid and glycerol, or is any one or the two or more mixture in lanoline, water-soluble silicon oil, PEG-7 glycerol coconut oil fat.
4. cleaning-nursing liquid as claimed in claim 1, it is characterized in that, described pH value regulator is lactic acid and/or citric acid.
5. a processing technology for the cleaning-nursing liquid described in any one of Claims 1 to 4, is characterized in that, comprise the steps:
1) at normal temperatures the gelatin polymer that chloro-for 2,4,4'-tri-2'-dihydroxy diphenyl ether, thickening agent, the filler of part formulation amount, wetting agent are mixed to form is added pure water and be stirred to dissolving;
2) add lauroyl Herba bromi japonici amino acid sodium, cocos nucifera oil acyl both sexes base oxalic acid disodium, cocamido propyl betaine again, stir while adding, make mixed liquor uniformly clarify Gel mile of state;
3) add the filler of emollient, glycyrrhizic acid dipotassium, Mentholum, surplus again, stir while adding, make mixed liquor uniformly emulsus mastic;
4) finally add the aqueous solution that pH value regulator and surplus pure water make and supply the water yield, start homogenizer, with rotating speed 2600r/min ~ 3000r/min homogenizing 8 ~ 12min;
Described thickening agent is the mixture of arabic gum natural gum and xanthan gum, or is PEG-150 distearate or methyl hydroxyethylcellulose.
6. the processing technology of cleaning-nursing liquid as claimed in claim 5, is characterized in that, step 1) in obtain gelatin polymer process be specially: by weight, by dispersed for the water of 1 part of thickening agent and 3 ~ 5 parts; Then add the chloro-2'-dihydroxy diphenyl ether of 2,4,4'-tri-, the filler of part formulation amount stirs, standing and reacting 10 ~ 30 minutes, obtains jelly; Wetting agent is added in described jelly and mixes, make transparent gelatin polymer.
7. the processing technology of cleaning-nursing liquid as claimed in claim 5, is characterized in that, step 1) and step 2) in, the speed of stirring is 30r/min ~ 50r/min, and mixing time is 8min ~ 12min; Step 3) in, the speed of stirring is 30r/min ~ 50r/min, and mixing time is 4min ~ 6min.
8. the processing technology of cleaning-nursing liquid as claimed in claim 5, is characterized in that, described wetting agent is any one or two or more mixture in hyaluronic acid, water solublity olive oil, Jojoba oil.
9. the processing technology of cleaning-nursing liquid as claimed in claim 5, it is characterized in that, described emollient is the mixture of hydroxylating soybean phospholipid and glycerol, or is any one or the two or more mixture in lanoline, water-soluble silicon oil, PEG-7 glycerol coconut oil fat; Described pH value regulator is lactic acid or citric acid, and described filler is sodium citrate.
10. the processing technology of cleaning-nursing liquid as claimed in claim 5, is characterized in that, step 3) be specially: by Mentholum and emollient dispersed; Then the filler adding surplus stirs, and standing and reacting 10 ~ 30 minutes, obtains jelly; Glycyrrhizic acid dipotassium is added in jelly and mixes, make emulsus mastic.
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| CN104382748A (en) * | 2014-10-15 | 2015-03-04 | 胡兰春 | Feminine hygiene wash and preparation method thereof |
| CN105342945A (en) * | 2015-08-06 | 2016-02-24 | 铜陵百锐设备配件有限公司 | Fleece care solution |
| CN105412973A (en) * | 2015-12-31 | 2016-03-23 | 广东景兴卫生用品有限公司 | Moderate antimicrobial sanitary towel |
| CN106309237A (en) * | 2016-09-26 | 2017-01-11 | 杭州惠博士生物科技有限公司 | Hyaluronic acid private part care gel and preparation method thereof |
| CN107802880B (en) * | 2017-12-05 | 2021-07-16 | 云南白药清逸堂实业有限公司 | Anticoagulation care solution, preparation method thereof and anticoagulation sanitary towel |
| CN108078816A (en) * | 2017-12-26 | 2018-05-29 | 南京顺禹电子商务有限公司 | A kind of women no-alcohol type high-efficiency antimicrobial liquid and preparation method thereof |
| CN109464341B (en) * | 2018-12-27 | 2021-09-03 | 广东景兴健康护理实业股份有限公司 | Health care composition |
| CN112826770A (en) * | 2021-01-20 | 2021-05-25 | 广州他秘生物科技有限公司 | Male care solution and preparation method thereof |
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Address after: 528000 Guicheng, Foshan, Nanhai District, East Street, No. 23 gem Patentee after: KINGDOM HEALTHCARE HOLDINGS CO., LTD., GUANGDONG Address before: 528200 Foshan, Nanhai, Guicheng, South China Sea, North Road, Hang Seng Bank Building, No. 8, building 50, No. Patentee before: Kingdom Sanitary Products Co., Ltd. |