CN108576082A - A kind of novel disinfectant liquid and preparation method thereof - Google Patents

A kind of novel disinfectant liquid and preparation method thereof Download PDF

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CN108576082A
CN108576082A CN201810066258.XA CN201810066258A CN108576082A CN 108576082 A CN108576082 A CN 108576082A CN 201810066258 A CN201810066258 A CN 201810066258A CN 108576082 A CN108576082 A CN 108576082A
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parts
preparation
disinfectant liquid
leaf
crude product
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张安育
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Hefei Huagai Biotechnology Co Ltd
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Hefei Huagai Biotechnology Co Ltd
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    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08Magnoliopsida [dicotyledons]
    • A01N65/20Fabaceae or Leguminosae [Pea or Legume family], e.g. pea, lentil, soybean, clover, acacia, honey locust, derris or millettia
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08Magnoliopsida [dicotyledons]
    • A01N65/24Lauraceae [Laurel family], e.g. laurel, avocado, sassafras, cinnamon or camphor
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08Magnoliopsida [dicotyledons]
    • A01N65/36Rutaceae [Rue family], e.g. lime, orange, lemon, corktree or pricklyash
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/40Liliopsida [monocotyledons]
    • A01N65/42Aloeaceae [Aloe family] or Liliaceae [Lily family], e.g. aloe, veratrum, onion, garlic or chives
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/40Liliopsida [monocotyledons]
    • A01N65/48Zingiberaceae [Ginger family], e.g. ginger or galangal

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Natural Medicines & Medicinal Plants (AREA)
  • Microbiology (AREA)
  • Biotechnology (AREA)
  • Agronomy & Crop Science (AREA)
  • Mycology (AREA)
  • Plant Pathology (AREA)
  • Dentistry (AREA)
  • Wood Science & Technology (AREA)
  • Zoology (AREA)
  • Environmental Sciences (AREA)
  • Botany (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

A kind of novel disinfectant liquid of present invention offer and preparation method thereof, including following raw material:Camphortree leaf, emblic leafflower leaf, Swertia vacillana (Hance) Maxim., folium artemisiae argyi, garlic, the Fructus Sophorae, ginger, surgical appliance adhesive and iodo-complexes, emulsifier, distilled water, cosolvent and pH adjusting agent.The disinfection liquid and preparation method thereof of the present invention is simple, of low cost, and disinfection efficiency is high, and it is long to sterilize the duration, and main active is natural materials, green environmental protection degradable, and people and animals are non-hazardous.

Description

A kind of novel disinfectant liquid and preparation method thereof
Technical field
The invention belongs to thimerosal technical fields, and in particular to a kind of novel disinfectant liquid and preparation method thereof.
Background technology
With universal and environmental protection concept the raising of scientific knowledge, people are to existing disinfection drug to kindergarten, capper The safety in the place that the people such as institute, primary school, family, office live is paid special attention to, especially SARS, bird flu and all kinds of The continuous generation of infectious disease, people generally solve in the method for disinfection while not having effective way, are subject to prevention and control, Common thimerosal is the chemicals such as Peracetic acid, chlorine dioxide, C5H6Br2N2O2, benzalkonium bromide, chlorhexidine, these drugs Realize sterilize while, certain harm is also caused to our health, be especially to the injury of infant it is huge, Injury is very important especially caused by the nervous systems such as respiratory tract, eyes, skin, in addition to human injury, to article Utensil etc. also has certain corrosion and pollution, and it is many unfavorable to be brought to people's normal life.
Such as a kind of multifunctional disinfectant and preparation method thereof, CN101810186, the invention are related to a kind of multifunctional disinfecting Liquid and preparation method thereof, the multifunctional disinfectant is with hexamethylene, propylene glycol, glycerine, fatty alcohol polyoxy Vinethene, lauryl amidopropyl betaine, alkyl-glucoside, Citric Acid Mono, deionized water are raw material, are lived by surface Property agent reasonably compounding and addition cosurfactant, synergistic effect is played to bactericidal effect.The invention it is this multi-functional Thimerosal, the formula of use can not degrade while disinfection, and carry certain harm to people and animals, and the duration of disinfection is not yet It is high.
In summary, it is therefore desirable to which a kind of better thimerosal improves the deficiencies in the prior art, improves disappearing for thimerosal The safety using thimerosal of toxic effect fruit and people.
Invention content
The object of the present invention is to provide a kind of novel disinfectant liquid and preparation method thereof, disinfection liquid and preparation method thereof letter of the invention Single, of low cost, disinfection efficiency is high, and the disinfection duration is long, and main active is natural materials, environmentally protective to drop Solution, people and animals are non-hazardous.
The present invention provides the following technical solutions:
A kind of novel disinfectant liquid includes the raw material of following parts by weight:20-30 parts of camphortree leaf, 25-35 parts of emblic leafflower leaf, Swertia vacillana (Hance) Maxim. 35- 40 parts, 30-45 parts of folium artemisiae argyi, 25-35 parts of garlic, 20-30 parts of the Fructus Sophorae, 35-55 parts of ginger, surgical appliance adhesive and iodo-complexes 18- 13-16 parts of 26 parts, 12-17 parts of emulsifier, 18-24 parts of distilled water, 12-16 parts of cosolvent and pH adjusting agent.
Preferably, the novel disinfectant liquid includes the raw material of following parts by weight:28 parts of camphortree leaf, 35 parts of emblic leafflower leaf, leafiness 37 parts red, 43 parts of folium artemisiae argyi, 32 parts of garlic, 25 parts of the Fructus Sophorae, 46 parts of ginger, surgical appliance adhesive and 22 parts of iodo-complexes, emulsifier 12 Part, 20 parts of distilled water, 16 parts of cosolvent and 14 parts of pH adjusting agent.
A kind of preparation method of novel disinfectant liquid, including following preparation process:
A, camphortree leaf, emblic leafflower leaf, Swertia vacillana (Hance) Maxim., folium artemisiae argyi, garlic, the Fructus Sophorae and ginger are cleaned up, then import in bruisher and smashs to pieces, Obtain mixture one;
B, it is blended into distilled water into mixture one, is placed in reaction kettle and heats, 30-35min is heated at 120-140 DEG C, then add Enter cosolvent, temperature is reduced to 80-90 DEG C, 15-20min is heated, obtains mixture two;
C, mixture two is imported in blender, 20-30min, heating temperature is stirred and heated under the rotating speed of 300-400r/min Degree is 60-80 DEG C, is slowly added to emulsifier while stirring, is placed in homogeneous in high pressure liquid stream homogenizer again later, filters out impurity, Obtain filtrate;
D, surgical appliance adhesive and iodo-complexes are added into filtrate, after stirring evenly, it is original volume to be placed in concentration in thickener 0.4-0.6 times, obtain crude product;
E, pH adjusting agent is added into crude product, adjusts the pH value of crude product in 2-3, then sterilization treatment is carried out to crude product, you can obtains Finished product.
Preferably, the raw material of the step a after cleaning, is first placed in water and impregnates 20-25min, and water temperature is 20-24 DEG C, When immersed with conducive to subsequently being heated to raw material, the active constituent accelerated in raw material is extracted, to improve extraction efficiency, contracting The time of short preparation flow.
Preferably, the cosolvent of the step b is any one of potassium bromide, sodium bromide, potassium iodide and sodium iodide or several The composition of kind.
Preferably, the surgical appliance adhesive of the step d and iodo-complexes are hydroxymethyl cellulose, hydroxypropyl methyl fiber Any one of element, povidone and starch or several compositions.
Preferably, the pH adjusting agent of the step e is appointing in citric acid, lactic acid, sulfuric acid, sorbic acid, phosphoric acid and hydrochloric acid One or more of compositions.
Preferably, the method for the sterilization treatment of the step e is:Crude product is subjected to microwave sterilization 10-15min, the sterilizing Method is conducive to protect the ingredient in thimerosal not to be destroyed, and this method sterilization of high efficiency, can targetedly, selectivity It goes to sterilize.
The beneficial effects of the invention are as follows:
The disinfection liquid and preparation method thereof of the present invention is simple, of low cost, does not need special reaction unit, reaction condition is not mildly severe It carves.Its disinfection efficiency is high, and the disinfection duration is long, and main active is natural materials, green environmental protection degradable, Ren Xuwu Harm is suitble to large-scale promotion manufacture and uses.
Primary raw material of the present invention is natural plants, Chinese herbal medicine, and the unique mechanism for relying on raw material itself carrys out sterilization, because This bacterium is difficult to develop immunity to drugs so that the using effect of the thimerosal is extended, and applied widely.
The surgical appliance adhesive and iodo-complexes being added in the present invention are stained in use to reduce the thimerosal Irritation caused by with human body or animal.
Specific implementation mode
Embodiment 1
A kind of novel disinfectant liquid includes the raw material of following parts by weight:20 parts of camphortree leaf, 35 parts of emblic leafflower leaf, 35 parts of Swertia vacillana (Hance) Maxim., folium artemisiae argyi 18 parts of 30 parts, 25 parts of garlic, 20 parts of the Fructus Sophorae, 55 parts of ginger, surgical appliance adhesive and iodo-complexes, 17 parts of emulsifier, distilled water 24 13 parts of part, 12 parts of cosolvent and pH adjusting agent.
A kind of preparation method of novel disinfectant liquid, including following preparation process:
A, camphortree leaf, emblic leafflower leaf, Swertia vacillana (Hance) Maxim., folium artemisiae argyi, garlic, the Fructus Sophorae and ginger are cleaned up, then import in bruisher and smashs to pieces, Obtain mixture one;
B, it is blended into distilled water into mixture one, is placed in reaction kettle and heats, heated 35min at 120 DEG C, add hydrotropy Temperature is reduced to 90 DEG C, heats 15min, obtain mixture two by agent;
C, mixture two is imported in blender, 30min, heating temperature 80 is stirred and heated under the rotating speed of 300r/min DEG C, it is slowly added to emulsifier while stirring, is placed in homogeneous in high pressure liquid stream homogenizer again later, filters out impurity, obtain filtrate;
D, surgical appliance adhesive and iodo-complexes are added into filtrate, after stirring evenly, it is original volume to be placed in concentration in thickener 0.4 times, obtain crude product;
E, pH adjusting agent is added into crude product, adjusts the pH value of crude product 3, then sterilization treatment is carried out to crude product, you can obtains into Product.
The raw material of step a after cleaning, is first placed in water and impregnates 25min, water temperature is 20 DEG C, immersed with conducive to subsequently to original When material heating, the active constituent accelerated in raw material is extracted, and to improve extraction efficiency, shortens the time of preparation flow.
The cosolvent of step b be potassium bromide, sodium bromide, potassium iodide and sodium iodide composition.
The surgical appliance adhesive and iodo-complexes of step d is hydroxymethyl cellulose, hydroxypropyl methyl cellulose, povidone and shallow lake The composition of powder.
The pH adjusting agent of step e is the composition of citric acid, lactic acid, sulfuric acid, sorbic acid, phosphoric acid and hydrochloric acid.
The method of the sterilization treatment of step e is:Crude product is subjected to microwave sterilization 15min, which is conducive to protect Ingredient in thimerosal is not destroyed, and this method sterilization of high efficiency, can targetedly, selectivity go sterilize.
A kind of common thimerosal is bought on the market and thimerosal manufactured in the present embodiment carries out check experiment, is chosen at The bacterium of the same race cultivated and obtained under the same conditions, two kinds of thimerosals for spraying equivalent are observed to obtain, bacterium after 1 day Survival volume:Common thimerosal is 3%, thimerosal 3% manufactured in the present embodiment;The survival volume of bacterium after 3 days:Common thimerosal It is 8%, thimerosal 3% manufactured in the present embodiment;The survival volume of bacterium after 7 days:Common thimerosal is 17%, prepared by the present embodiment Thimerosal 6%.It can be seen that the thimerosal bactericidal effect of the present invention is preferable, and the function and effect duration is long.
Embodiment 2
A kind of novel disinfectant liquid includes the raw material of following parts by weight:30 parts of camphortree leaf, 25 parts of emblic leafflower leaf, 35 parts of Swertia vacillana (Hance) Maxim., folium artemisiae argyi 18 parts of 30 parts, 35 parts of garlic, 20 parts of the Fructus Sophorae, 55 parts of ginger, surgical appliance adhesive and iodo-complexes, 12 parts of emulsifier, distilled water 18 13 parts of part, 16 parts of cosolvent and pH adjusting agent.
A kind of preparation method of novel disinfectant liquid, including following preparation process:
A, camphortree leaf, emblic leafflower leaf, Swertia vacillana (Hance) Maxim., folium artemisiae argyi, garlic, the Fructus Sophorae and ginger are cleaned up, then import in bruisher and smashs to pieces, Obtain mixture one;
B, it is blended into distilled water into mixture one, is placed in reaction kettle and heats, heated 30min at 120 DEG C, add hydrotropy Temperature is reduced to 80 DEG C, heats 20min, obtain mixture two by agent;
C, mixture two is imported in blender, 20min, heating temperature 60 is stirred and heated under the rotating speed of 300r/min DEG C, it is slowly added to emulsifier while stirring, is placed in homogeneous in high pressure liquid stream homogenizer again later, filters out impurity, obtain filtrate;
D, surgical appliance adhesive and iodo-complexes are added into filtrate, after stirring evenly, it is original volume to be placed in concentration in thickener 0.4 times, obtain crude product;
E, pH adjusting agent is added into crude product, adjusts the pH value of crude product 2, then sterilization treatment is carried out to crude product, you can obtains into Product.
The raw material of step a after cleaning, is first placed in water and impregnates 20min, water temperature is 20 DEG C, immersed with conducive to subsequently to original When material heating, the active constituent accelerated in raw material is extracted, and to improve extraction efficiency, shortens the time of preparation flow.
The cosolvent of step b be potassium bromide, sodium bromide, potassium iodide and sodium iodide composition.
The surgical appliance adhesive and iodo-complexes of step d is hydroxymethyl cellulose, hydroxypropyl methyl cellulose, povidone and shallow lake The composition of powder.
The pH adjusting agent of step e is the composition of citric acid, lactic acid, sulfuric acid, sorbic acid, phosphoric acid and hydrochloric acid.
The method of the sterilization treatment of step e is:Crude product is subjected to microwave sterilization 10min, which is conducive to protect Ingredient in thimerosal is not destroyed, and this method sterilization of high efficiency, can targetedly, selectivity go sterilize.
A kind of common thimerosal is bought on the market and thimerosal manufactured in the present embodiment carries out check experiment, is chosen at The bacterium of the same race cultivated and obtained under the same conditions, two kinds of thimerosals for spraying equivalent are observed to obtain, bacterium after 1 day Survival volume:Common thimerosal is 3%, thimerosal 2% manufactured in the present embodiment;The survival volume of bacterium after 3 days:Common thimerosal It is 8%, thimerosal 4% manufactured in the present embodiment;The survival volume of bacterium after 7 days:Common thimerosal is 17%, prepared by the present embodiment Thimerosal 6%.It can be seen that the thimerosal bactericidal effect of the present invention is preferable, and the function and effect duration is long.
Embodiment 3
A kind of novel disinfectant liquid includes the raw material of following parts by weight:28 parts of camphortree leaf, 35 parts of emblic leafflower leaf, 37 parts of Swertia vacillana (Hance) Maxim., folium artemisiae argyi 22 parts of 43 parts, 32 parts of garlic, 25 parts of the Fructus Sophorae, 46 parts of ginger, surgical appliance adhesive and iodo-complexes, 12 parts of emulsifier, distilled water 20 14 parts of part, 16 parts of cosolvent and pH adjusting agent.
A kind of preparation method of novel disinfectant liquid, including following preparation process:
A, camphortree leaf, emblic leafflower leaf, Swertia vacillana (Hance) Maxim., folium artemisiae argyi, garlic, the Fructus Sophorae and ginger are cleaned up, then import in bruisher and smashs to pieces, Obtain mixture one;
B, it is blended into distilled water into mixture one, is placed in reaction kettle and heats, heated 35min at 140 DEG C, add hydrotropy Temperature is reduced to 90 DEG C, heats 20min, obtain mixture two by agent;
C, mixture two is imported in blender, 30min, heating temperature 80 is stirred and heated under the rotating speed of 400r/min DEG C, it is slowly added to emulsifier while stirring, is placed in homogeneous in high pressure liquid stream homogenizer again later, filters out impurity, obtain filtrate;
D, surgical appliance adhesive and iodo-complexes are added into filtrate, after stirring evenly, it is original volume to be placed in concentration in thickener 0.6 times, obtain crude product;
E, pH adjusting agent is added into crude product, adjusts the pH value of crude product 3, then sterilization treatment is carried out to crude product, you can obtains into Product.
The raw material of step a after cleaning, is first placed in water and impregnates 25min, water temperature is 24 DEG C, immersed with conducive to subsequently to original When material heating, the active constituent accelerated in raw material is extracted, and to improve extraction efficiency, shortens the time of preparation flow.
The cosolvent of step b be potassium bromide, sodium bromide, potassium iodide and sodium iodide composition.
The surgical appliance adhesive and iodo-complexes of step d is hydroxymethyl cellulose, hydroxypropyl methyl cellulose, povidone and shallow lake The composition of powder.
The pH adjusting agent of step e is the composition of citric acid, lactic acid, sulfuric acid, sorbic acid, phosphoric acid and hydrochloric acid.
The method of the sterilization treatment of step e is:Crude product is subjected to microwave sterilization 15min, which is conducive to protect Ingredient in thimerosal is not destroyed, and this method sterilization of high efficiency, can targetedly, selectivity go sterilize.
A kind of common thimerosal is bought on the market and thimerosal manufactured in the present embodiment carries out check experiment, is chosen at The bacterium of the same race cultivated and obtained under the same conditions, two kinds of thimerosals for spraying equivalent are observed to obtain, bacterium after 1 day Survival volume:Common thimerosal is 3%, thimerosal 2% manufactured in the present embodiment;The survival volume of bacterium after 3 days:Common thimerosal It is 8%, thimerosal 3% manufactured in the present embodiment;The survival volume of bacterium after 7 days:Common thimerosal is 17%, prepared by the present embodiment Thimerosal 5%.It can be seen that the thimerosal bactericidal effect of the present invention is preferable, and the function and effect duration is long.
The foregoing is only a preferred embodiment of the present invention, is not intended to restrict the invention, although with reference to aforementioned reality Applying example, invention is explained in detail, for those skilled in the art, still can be to aforementioned each implementation Technical solution recorded in example is modified or equivalent replacement of some of the technical features.All essences in the present invention With within principle, any modification, equivalent replacement, improvement and so on should all be included in the protection scope of the present invention god.

Claims (8)

1. a kind of novel disinfectant liquid, which is characterized in that include the raw material of following parts by weight:20-30 parts of camphortree leaf, emblic leafflower leaf 25- 35 parts, 35-40 parts of Swertia vacillana (Hance) Maxim., 30-45 parts of folium artemisiae argyi, 25-35 parts of garlic, 20-30 parts of the Fructus Sophorae, 35-55 parts of ginger, surgical appliance adhesive And 13-16 parts of 18-26 parts of iodo-complexes, 12-17 parts of emulsifier, 18-24 parts of distilled water, 12-16 parts of cosolvent and pH adjusting agent.
2. a kind of novel disinfectant liquid according to claim 1, which is characterized in that include the raw material of following parts by weight:Camphor tree 28 parts of leaf, 35 parts of emblic leafflower leaf, 37 parts of Swertia vacillana (Hance) Maxim., 43 parts of folium artemisiae argyi, 32 parts of garlic, 25 parts of the Fructus Sophorae, 46 parts of ginger, surgical appliance adhesive and 14 parts of 22 parts of iodo-complexes, 12 parts of emulsifier, 20 parts of distilled water, 16 parts of cosolvent and pH adjusting agent.
3. a kind of preparation method of novel disinfectant liquid as claimed in claim 1 or 2, which is characterized in that including following preparation process:
A, camphortree leaf, emblic leafflower leaf, Swertia vacillana (Hance) Maxim., folium artemisiae argyi, garlic, the Fructus Sophorae and ginger are cleaned up, then import in bruisher and smashs to pieces, Obtain mixture one;
B, it is blended into distilled water into mixture one, is placed in reaction kettle and heats, 30-35min is heated at 120-140 DEG C, then add Enter cosolvent, temperature is reduced to 80-90 DEG C, 15-20min is heated, obtains mixture two;
C, mixture two is imported in blender, 20-30min, heating temperature is stirred and heated under the rotating speed of 300-400r/min Degree is 60-80 DEG C, is slowly added to emulsifier while stirring, is placed in homogeneous in high pressure liquid stream homogenizer again later, filters out impurity, Obtain filtrate;
D, surgical appliance adhesive and iodo-complexes are added into filtrate, after stirring evenly, it is original volume to be placed in concentration in thickener 0.4-0.6 times, obtain crude product;
E, pH adjusting agent is added into crude product, adjusts the pH value of crude product in 2-3, then sterilization treatment is carried out to crude product, you can obtains Finished product.
4. a kind of preparation method of novel disinfectant liquid according to claim 3, which is characterized in that the raw material of the step a After cleaning, it is first placed in water and impregnates 20-25min, water temperature is 20-24 DEG C.
5. a kind of preparation method of novel disinfectant liquid according to claim 3, which is characterized in that the hydrotropy of the step b Agent is any one of potassium bromide, sodium bromide, potassium iodide and sodium iodide or several compositions.
6. a kind of preparation method of novel disinfectant liquid according to claim 3, which is characterized in that the skin of the step d Adhesive and iodo-complexes are any one of hydroxymethyl cellulose, hydroxypropyl methyl cellulose, povidone and starch or several Composition.
7. a kind of preparation method of novel disinfectant liquid according to claim 3, which is characterized in that the pH tune of the step e Section agent is any one of citric acid, lactic acid, sulfuric acid, sorbic acid, phosphoric acid and hydrochloric acid or several compositions.
8. a kind of preparation method of novel disinfectant liquid according to claim 3, which is characterized in that the sterilizing of the step e The method of processing is:Crude product is subjected to microwave sterilization 10-15min.
CN201810066258.XA 2018-01-24 2018-01-24 A kind of novel disinfectant liquid and preparation method thereof Withdrawn CN108576082A (en)

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CN103768405A (en) * 2014-01-19 2014-05-07 赵静 Traditional Chinese medicine disinfectant and preparation method thereof
CN104491787A (en) * 2014-12-09 2015-04-08 李跃 Traditional Chinese medicine liquid for sterilizing skin
CN105663158A (en) * 2016-03-15 2016-06-15 浙江海正药业股份有限公司 High-concentration iodine disinfection solution and preparation method thereof
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CN107158251A (en) * 2017-07-12 2017-09-15 合肥华盖生物科技有限公司 A kind of Traditional Chinese medicine disinfectant and preparation method thereof
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