CN103566872A - Dogwood kernel modified active carbon water purifier and preparation method thereof - Google Patents
Dogwood kernel modified active carbon water purifier and preparation method thereof Download PDFInfo
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- CN103566872A CN103566872A CN201310441938.2A CN201310441938A CN103566872A CN 103566872 A CN103566872 A CN 103566872A CN 201310441938 A CN201310441938 A CN 201310441938A CN 103566872 A CN103566872 A CN 103566872A
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Abstract
The invention relates to a dogwood kernel modified active carbon water purifier, which is prepared from the following raw materials in parts by weight: 50 to 60 parts of dogwood kernel, 9 to 12 parts of calcined gypsum, 5 to 6 parts of dried alum, 10 to 15 parts of lignocellulose, 6 to 9 parts of calcium-based montmorillonite, 3 to 5 parts of milk protein, 8 to 10 parts of acrylonitrile, 1 to 2 parts of ammonium persulfate, 100 to 110 parts of active carbon, 7 to 9 parts of gelatin, 10 to 13 parts of chitosan, 4 to 5 parts of modified diatomite and an appropriate amount of water. After the dogwood kernel is carbonized at a high temperature, a structure with multiple pores and strong adsorption capacity is formed, so that the cost is saved and the environmental pollution is reduced; due to use of the macromolecular compounds such as acrylonitrile, gelatin, lignocellulose and chitosan and the like, the adhesive force can be increased, the disintegration is unlikely to happen, an effect of chelating metal ions can be realized, and safe and non-toxic effects are achieved; due to use of calclium-based montmorillonite, an antibacterial function, a deodorizing function and an ion exchanging function can be achieved; due to use of the calcined gypsum and the dried alum, a sterilizing function can be achieved; the dogwood kernel modified active carbon water purifier is safe, healthy, low in cost and particularly suitable for water purification.
Description
Technical field
The present invention relates to a kind of modified function Material Field, relate in particular to a kind of Fructus Corni fruit stone modified activated carbon water purification agent and preparation method thereof.
Background technology
Air pollution at present has had a strong impact on people's productive life, so air cleaning has had to pay attention to.Adsorbent is often used in air cleaning, mainly contains activated alumina, active carbon, also has in addition for certain compositional selecting absorption and the sorbing material of development.But the most adsorption capacity of these adsorbents is limited, need to study different adsorbents for different requirements, bring into play best effect.Meanwhile, find new raw material, to strengthen adsorption effect, cost-saving.Along with people improve constantly the requirement of quality of life, also need the adsorbent that provides useful to human body.
Summary of the invention
The object of the present invention is to provide a kind of Fructus Corni fruit stone modified activated carbon water purification agent and preparation method thereof.
Technical scheme of the present invention is as follows:
A fruit stone modified activated carbon water purification agent, is characterized in that being made by the raw material of following weight portion: Fructus Corni fruit stone 50-60, calcined gypsum 9-12, alumen 5-6, lignocellulosic 10-15, calcium-base montmorillonite 6-9, milk protein 3-5, acrylonitrile 8-10, Ammonium Persulfate 98.5 1-2, active carbon 100-110, gelatin 7-9, shitosan 10-13, modification infusorial earth 4-5, water are appropriate;
Described modification infusorial earth is made by the raw material of following weight portion: diatomite 140-150, alum 10-12, nano-sized carbon 1-2, coix seed oil 1-2, ascorbic acid 2-3, citric acid 1-2, sodium phosphate trimer 2-3, ginseng pulverate 2-3; Preparation method puts into calcining furnace by diatomite to calcine 3-4 hour at 540-560 ℃, takes out, and the hydrochloric acid solution of putting into 12-15% soaks 4-5 hour, filter and take out, use clear water cyclic washing, dry, be added to the water, simultaneously, add nano-sized carbon, ascorbic acid, citric acid, alum, grind and obtain slurry, spraying is dry, other residual components is mixed with dried powder, and grinding distribution evenly and get final product.
The preparation method of described Fructus Corni fruit stone modified activated carbon water purification agent, it is characterized in that comprising the following steps: calcium-base montmorillonite is pulverized, sent in retort together with Fructus Corni fruit stone, calcined gypsum, alumen, at 650-700 ℃, 3-4 hour is processed in charing, take out, add furnishing mud shape in suitable quantity of water together with lignocellulosic, milk protein, acrylonitrile, Ammonium Persulfate 98.5, active carbon, gelatin, shitosan, be heated to 70-80 ℃, grind 2-3 hour to obtain 200-300 order slurry, it is neutral with clear water, washing to pH value, dries; Mix and be uniformly dispersed and get final product with other surplus stocks.
Beneficial effect of the present invention
It is flourishing that the present invention forms hole by Fructus Corni fruit stone high temperature carbonization, and the structure of high adsorption capacity, has saved cost, reduces environmental pollution; By using the macromolecular compounds such as acrylonitrile, gelatin, lignocellulosic, shitosan, not only cohesive force increases, easy disintegrating not, and there is the effect of chelated metal ions and safety non-toxic; By using calcium-base montmorillonite, can antibacterial and deodouring, ion-exchange; By using calcined gypsum, alumen, can sterilizing; Safety and Health of the present invention, cost is low, is particularly suitable for water and purifies.
The specific embodiment
A fruit stone modified activated carbon water purification agent, by following weight portion (kilogram) raw material make: Fructus Corni fruit stone 55, calcined gypsum 11, alumen 5, lignocellulosic 13, calcium-base montmorillonite 7, milk protein 4, acrylonitrile 9, Ammonium Persulfate 98.5 1.4, active carbon 104, gelatin 8, shitosan 11, modification infusorial earth 4, water are appropriate;
Described modification infusorial earth by following weight portion (kilogram) raw material make: diatomite 145, alum 11, nano-sized carbon 1.5, coix seed oil 1.5, ascorbic acid 2.5, citric acid 1.6, sodium phosphate trimer 2.4, ginseng pulverate 2.4; Preparation method puts into calcining furnace by diatomite at 550 ℃, to calcine 3.6 hours, takes out, and puts into 13% hydrochloric acid solution and soaks 4.5 hours, filter and take out, use clear water cyclic washing, dry, be added to the water, simultaneously, add nano-sized carbon, ascorbic acid, citric acid, alum, grind and obtain slurry, spraying is dry, other residual components is mixed with dried powder, and grinding distribution evenly and get final product.
The preparation method of described Fructus Corni fruit stone modified activated carbon water purification agent, comprise the following steps: calcium-base montmorillonite is pulverized, sent in retort together with Fructus Corni fruit stone, calcined gypsum, alumen, at 670 ℃, charing is processed 3 hours, take out, add furnishing mud shape in suitable quantity of water together with lignocellulosic, milk protein, acrylonitrile, Ammonium Persulfate 98.5, active carbon, gelatin, shitosan, be heated to 77 ℃, grind 2.8 hours to obtain 300 order slurries, it is neutral with clear water, washing to pH value, dries; Mix and be uniformly dispersed and get final product with other surplus stocks.
After measured, its iodine number 1531mg/g, methylene blue adsorption value 28.1mL/0.1g.
Claims (2)
1. a Fructus Corni fruit stone modified activated carbon water purification agent, is characterized in that being made by the raw material of following weight portion: Fructus Corni fruit stone 50-60, calcined gypsum 9-12, alumen 5-6, lignocellulosic 10-15, calcium-base montmorillonite 6-9, milk protein 3-5, acrylonitrile 8-10, Ammonium Persulfate 98.5 1-2, active carbon 100-110, gelatin 7-9, shitosan 10-13, modification infusorial earth 4-5, water are appropriate;
Described modification infusorial earth is made by the raw material of following weight portion: diatomite 140-150, alum 10-12, nano-sized carbon 1-2, coix seed oil 1-2, ascorbic acid 2-3, citric acid 1-2, sodium phosphate trimer 2-3, ginseng pulverate 2-3; Preparation method puts into calcining furnace by diatomite to calcine 3-4 hour at 540-560 ℃, takes out, and the hydrochloric acid solution of putting into 12-15% soaks 4-5 hour, filter and take out, use clear water cyclic washing, dry, be added to the water, simultaneously, add nano-sized carbon, ascorbic acid, citric acid, alum, grind and obtain slurry, spraying is dry, other residual components is mixed with dried powder, and grinding distribution evenly and get final product.
2. the preparation method of Fructus Corni fruit stone modified activated carbon water purification agent according to claim 1, it is characterized in that comprising the following steps: calcium-base montmorillonite is pulverized, sent in retort together with Fructus Corni fruit stone, calcined gypsum, alumen, at 650-700 ℃, 3-4 hour is processed in charing, take out, add furnishing mud shape in suitable quantity of water together with lignocellulosic, milk protein, acrylonitrile, Ammonium Persulfate 98.5, active carbon, gelatin, shitosan, be heated to 70-80 ℃, grind 2-3 hour to obtain 200-300 order slurry, it is neutral with clear water, washing to pH value, dries; Mix and be uniformly dispersed and get final product with other surplus stocks.
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| CN201310441938.2A CN103566872A (en) | 2013-09-26 | 2013-09-26 | Dogwood kernel modified active carbon water purifier and preparation method thereof |
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| CN201310441938.2A CN103566872A (en) | 2013-09-26 | 2013-09-26 | Dogwood kernel modified active carbon water purifier and preparation method thereof |
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Cited By (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104445468A (en) * | 2014-12-07 | 2015-03-25 | 浙江省淡水水产研究所 | Water purifier for cultivating Chinese softshell turtles |
| CN104474780A (en) * | 2014-11-13 | 2015-04-01 | 蚌埠德美过滤技术有限公司 | Faint scent active carbon filter material with strong catalytic degradation effect, and preparation method thereof |
| CN104591345A (en) * | 2014-12-26 | 2015-05-06 | 安徽省中日农业环保科技有限公司 | Plaster-base cyanobacteria treating agent and preparation method thereof |
| CN104604959A (en) * | 2014-12-26 | 2015-05-13 | 安徽省中日农业环保科技有限公司 | Blue-green algae treatment agent adopting konjac powder and preparation method of treatment agent |
| CN104604948A (en) * | 2014-12-26 | 2015-05-13 | 安徽省中日农业环保科技有限公司 | Blue algae treating agent prepared from kelp and preparation method thereof |
| CN104803453A (en) * | 2015-05-11 | 2015-07-29 | 安徽省中日农业环保科技有限公司 | Blue-green algae treatment agent prepared from coconut shell and preparation method of blue-green algae treatment agent |
| CN105129941A (en) * | 2015-08-31 | 2015-12-09 | 蚌埠龙达农业专业合作社 | Aquaculture pond pollutant curing decomposing agent and preparation method thereof |
| CN105126779A (en) * | 2015-07-24 | 2015-12-09 | 安徽雪城超细碳酸钙有限公司 | Porous modified bentonite with foaming effect and preparation method thereof |
| CN105124249A (en) * | 2015-08-31 | 2015-12-09 | 蚌埠龙达农业专业合作社 | Aquatic product mixed culturing feed capable of self degradation and preparation method of aquatic product mixed culturing feed |
| CN105123790A (en) * | 2015-08-31 | 2015-12-09 | 蚌埠龙达农业专业合作社 | Aquaculture water body sterilization and degradation particles and preparation method thereof |
| CN105166408A (en) * | 2015-08-31 | 2015-12-23 | 蚌埠龙达农业专业合作社 | Feed additive capable of treating viral fish diseases and preparation method of feed additive |
| CN105253969A (en) * | 2015-08-31 | 2016-01-20 | 蚌埠龙达农业专业合作社 | Contamination-reducing nutrient-increasing additive for aquaculture water and preparation method thereof |
| CN108328675A (en) * | 2018-03-01 | 2018-07-27 | 河南省亚乐生物科技股份有限公司 | Nontoxic water treatment agent of Chinese herbal medicine and preparation method thereof |
| CN108393070A (en) * | 2018-05-07 | 2018-08-14 | 合肥浦尔菲电线科技有限公司 | A kind of composite efficient adsorbent for purifying water |
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Cited By (15)
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| CN104474780B (en) * | 2014-11-13 | 2017-02-08 | 芜湖市创源新材料有限公司 | Faint scent active carbon filter material with strong catalytic degradation effect, and preparation method thereof |
| CN104474780A (en) * | 2014-11-13 | 2015-04-01 | 蚌埠德美过滤技术有限公司 | Faint scent active carbon filter material with strong catalytic degradation effect, and preparation method thereof |
| CN104445468A (en) * | 2014-12-07 | 2015-03-25 | 浙江省淡水水产研究所 | Water purifier for cultivating Chinese softshell turtles |
| CN104591345A (en) * | 2014-12-26 | 2015-05-06 | 安徽省中日农业环保科技有限公司 | Plaster-base cyanobacteria treating agent and preparation method thereof |
| CN104604959A (en) * | 2014-12-26 | 2015-05-13 | 安徽省中日农业环保科技有限公司 | Blue-green algae treatment agent adopting konjac powder and preparation method of treatment agent |
| CN104604948A (en) * | 2014-12-26 | 2015-05-13 | 安徽省中日农业环保科技有限公司 | Blue algae treating agent prepared from kelp and preparation method thereof |
| CN104803453A (en) * | 2015-05-11 | 2015-07-29 | 安徽省中日农业环保科技有限公司 | Blue-green algae treatment agent prepared from coconut shell and preparation method of blue-green algae treatment agent |
| CN105126779A (en) * | 2015-07-24 | 2015-12-09 | 安徽雪城超细碳酸钙有限公司 | Porous modified bentonite with foaming effect and preparation method thereof |
| CN105129941A (en) * | 2015-08-31 | 2015-12-09 | 蚌埠龙达农业专业合作社 | Aquaculture pond pollutant curing decomposing agent and preparation method thereof |
| CN105123790A (en) * | 2015-08-31 | 2015-12-09 | 蚌埠龙达农业专业合作社 | Aquaculture water body sterilization and degradation particles and preparation method thereof |
| CN105166408A (en) * | 2015-08-31 | 2015-12-23 | 蚌埠龙达农业专业合作社 | Feed additive capable of treating viral fish diseases and preparation method of feed additive |
| CN105253969A (en) * | 2015-08-31 | 2016-01-20 | 蚌埠龙达农业专业合作社 | Contamination-reducing nutrient-increasing additive for aquaculture water and preparation method thereof |
| CN105124249A (en) * | 2015-08-31 | 2015-12-09 | 蚌埠龙达农业专业合作社 | Aquatic product mixed culturing feed capable of self degradation and preparation method of aquatic product mixed culturing feed |
| CN108328675A (en) * | 2018-03-01 | 2018-07-27 | 河南省亚乐生物科技股份有限公司 | Nontoxic water treatment agent of Chinese herbal medicine and preparation method thereof |
| CN108393070A (en) * | 2018-05-07 | 2018-08-14 | 合肥浦尔菲电线科技有限公司 | A kind of composite efficient adsorbent for purifying water |
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Application publication date: 20140212 |