CN104474780B - Faint scent active carbon filter material with strong catalytic degradation effect, and preparation method thereof - Google Patents
Faint scent active carbon filter material with strong catalytic degradation effect, and preparation method thereof Download PDFInfo
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- CN104474780B CN104474780B CN201410639873.7A CN201410639873A CN104474780B CN 104474780 B CN104474780 B CN 104474780B CN 201410639873 A CN201410639873 A CN 201410639873A CN 104474780 B CN104474780 B CN 104474780B
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- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 title claims abstract description 35
- 239000000463 material Substances 0.000 title claims abstract description 23
- 230000000694 effects Effects 0.000 title claims abstract description 18
- 229910052799 carbon Inorganic materials 0.000 title claims abstract description 15
- 230000015556 catabolic process Effects 0.000 title claims abstract description 14
- 230000003197 catalytic effect Effects 0.000 title claims abstract description 14
- 238000006731 degradation reaction Methods 0.000 title claims abstract description 14
- 238000002360 preparation method Methods 0.000 title claims description 8
- 238000001179 sorption measurement Methods 0.000 claims abstract description 13
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 13
- 235000005976 Citrus sinensis Nutrition 0.000 claims abstract description 12
- 240000002319 Citrus sinensis Species 0.000 claims abstract description 12
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims abstract description 11
- 240000001008 Dimocarpus longan Species 0.000 claims abstract description 9
- 235000000235 Euphoria longan Nutrition 0.000 claims abstract description 9
- 239000005696 Diammonium phosphate Substances 0.000 claims abstract description 7
- 239000004927 clay Substances 0.000 claims abstract description 7
- 239000003245 coal Substances 0.000 claims abstract description 7
- MNNHAPBLZZVQHP-UHFFFAOYSA-N diammonium hydrogen phosphate Chemical compound [NH4+].[NH4+].OP([O-])([O-])=O MNNHAPBLZZVQHP-UHFFFAOYSA-N 0.000 claims abstract description 7
- 229910000388 diammonium phosphate Inorganic materials 0.000 claims abstract description 7
- 235000019838 diammonium phosphate Nutrition 0.000 claims abstract description 7
- 239000002994 raw material Substances 0.000 claims abstract description 7
- CHQMHPLRPQMAMX-UHFFFAOYSA-L sodium persulfate Substances [Na+].[Na+].[O-]S(=O)(=O)OOS([O-])(=O)=O CHQMHPLRPQMAMX-UHFFFAOYSA-L 0.000 claims abstract description 7
- SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 claims abstract description 4
- NIXOWILDQLNWCW-UHFFFAOYSA-N 2-Propenoic acid Natural products OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims abstract description 4
- OTYBMLCTZGSZBG-UHFFFAOYSA-L potassium sulfate Chemical compound [K+].[K+].[O-]S([O-])(=O)=O OTYBMLCTZGSZBG-UHFFFAOYSA-L 0.000 claims abstract description 4
- 229910052939 potassium sulfate Inorganic materials 0.000 claims abstract description 4
- 235000011151 potassium sulphates Nutrition 0.000 claims abstract description 4
- 239000000843 powder Substances 0.000 claims description 18
- 238000002386 leaching Methods 0.000 claims description 10
- 239000010502 orange oil Substances 0.000 claims description 10
- 244000144730 Amygdalus persica Species 0.000 claims description 9
- 235000017166 Bambusa arundinacea Nutrition 0.000 claims description 9
- 235000017491 Bambusa tulda Nutrition 0.000 claims description 9
- 235000015334 Phyllostachys viridis Nutrition 0.000 claims description 9
- 235000006040 Prunus persica var persica Nutrition 0.000 claims description 9
- 239000011425 bamboo Substances 0.000 claims description 9
- 239000000835 fiber Substances 0.000 claims description 9
- 239000003205 fragrance Substances 0.000 claims description 9
- 238000001816 cooling Methods 0.000 claims description 7
- OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 claims description 7
- 240000007594 Oryza sativa Species 0.000 claims description 6
- 235000007164 Oryza sativa Nutrition 0.000 claims description 6
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 6
- 244000269722 Thea sinensis Species 0.000 claims description 6
- 238000001914 filtration Methods 0.000 claims description 6
- 239000012467 final product Substances 0.000 claims description 6
- 239000010903 husk Substances 0.000 claims description 6
- 239000011812 mixed powder Substances 0.000 claims description 6
- 239000011268 mixed slurry Substances 0.000 claims description 6
- 238000002156 mixing Methods 0.000 claims description 6
- 235000009566 rice Nutrition 0.000 claims description 6
- KRKNYBCHXYNGOX-UHFFFAOYSA-K Citrate Chemical compound [O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O KRKNYBCHXYNGOX-UHFFFAOYSA-K 0.000 claims description 3
- 240000000961 Setaria parviflora Species 0.000 claims description 3
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 claims description 3
- 238000010000 carbonizing Methods 0.000 claims description 3
- 238000010298 pulverizing process Methods 0.000 claims description 3
- 239000000377 silicon dioxide Substances 0.000 claims description 3
- 239000002002 slurry Substances 0.000 claims description 3
- 239000007921 spray Substances 0.000 claims description 3
- 238000003756 stirring Methods 0.000 claims description 3
- 244000082204 Phyllostachys viridis Species 0.000 claims 3
- 238000005202 decontamination Methods 0.000 abstract description 2
- 230000003588 decontaminative effect Effects 0.000 abstract description 2
- 238000005516 engineering process Methods 0.000 abstract description 2
- 241000759833 Cornus officinalis Species 0.000 abstract 2
- 235000013399 edible fruits Nutrition 0.000 abstract 2
- 239000004408 titanium dioxide Substances 0.000 abstract 2
- LCPVQAHEFVXVKT-UHFFFAOYSA-N 2-(2,4-difluorophenoxy)pyridin-3-amine Chemical compound NC1=CC=CN=C1OC1=CC=C(F)C=C1F LCPVQAHEFVXVKT-UHFFFAOYSA-N 0.000 abstract 1
- 230000003115 biocidal effect Effects 0.000 abstract 1
- 231100000614 poison Toxicity 0.000 abstract 1
- 239000003440 toxic substance Substances 0.000 abstract 1
- 239000000341 volatile oil Substances 0.000 abstract 1
- 241001330002 Bambuseae Species 0.000 description 6
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 description 3
- 238000004140 cleaning Methods 0.000 description 3
- 241000894006 Bacteria Species 0.000 description 2
- 230000000844 anti-bacterial effect Effects 0.000 description 2
- 239000000428 dust Substances 0.000 description 2
- 241000233866 Fungi Species 0.000 description 1
- 230000002730 additional effect Effects 0.000 description 1
- 238000004378 air conditioning Methods 0.000 description 1
- 238000004887 air purification Methods 0.000 description 1
- 231100001245 air toxic agent Toxicity 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000003421 catalytic decomposition reaction Methods 0.000 description 1
- 235000013339 cereals Nutrition 0.000 description 1
- 239000002781 deodorant agent Substances 0.000 description 1
- 239000008187 granular material Substances 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 230000001473 noxious effect Effects 0.000 description 1
- SOQBVABWOPYFQZ-UHFFFAOYSA-N oxygen(2-);titanium(4+) Chemical compound [O-2].[O-2].[Ti+4] SOQBVABWOPYFQZ-UHFFFAOYSA-N 0.000 description 1
- 238000011056 performance test Methods 0.000 description 1
- 238000007146 photocatalysis Methods 0.000 description 1
- 230000001699 photocatalysis Effects 0.000 description 1
- 239000011148 porous material Substances 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 239000002689 soil Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000003053 toxin Substances 0.000 description 1
- 231100000765 toxin Toxicity 0.000 description 1
- 238000010792 warming Methods 0.000 description 1
Abstract
The invention discloses a faint scent active carbon filter material with a strong catalytic degradation effect. The filter material is prepared by using the following raw materials, by weight, 137-147 parts of active carbon, 9-13 parts of nanometer titanium dioxide, 3-4 parts of acrylic acid, 3-5 parts of potassium sulfate, 8-11 parts of clay, 2-3 parts of diammonium phosphate, 1-2 parts of sodium persulfate, 0.6-0.9 parts of sweet orange essential oil, 20-25 parts of Cornus officinalis fruit shell, 24-28 parts of longan shell, 5-7 parts of rich coal, 4-6 parts of an adsorption aid and a proper amount of water. The Cornus officinalis fruit shell and the longan shell are added to active carbon through a series of technologies to make the filter material have various tunnel structures and a large specific area; the nanometer titanium dioxide is added to make the filter material have a strong catalytic degradation effect and effectively remove many toxic substances and have antibiosis and decontamination effects; and the sweet orange is added to refresh air. The active carbon filter material prepared in the invention has the advantages of good use effect and durability, and is suitable for making air conditioner filter screens or air purifiers.
Description
Technical field
The present invention relates to a kind of filtering material and preparation method thereof, particularly a kind of have delicate fragrance type carbon leaching material of strong catalytic degradation effect and preparation method thereof.
Background technology
The time in all one's life of people at least 1/3rd is in interior, and the quality of IAQ has significant impact to the health of people.At present, improve indoor air quality Main Means be harmful substance is carried out adsorb by air cleaning facilities such as air conditioner, air cleaners, catalytic decomposition, filtration, antibacterial, humiture control etc., but, day by day raising with people's living standard, people to living room, office, public place environment requirement more and more higher, while requiring the cooling and warming of air cleaning facility, improve air quality effect, start the higher additional effect of requirement.However, the air cleaning facility such as the comparatively single air-conditioning of existing function, air cleaner can not meet above-mentioned requirements.
Nano titanium dioxide is the general name of the photosemiconductor material with photo-catalysis function of representative, in the presence of light, produces strong catalytic degradation function：Can effectively degrade in the air toxic and harmful；Various bacteria can effectively be killed, and the toxin that bacterium or fungi discharge can be decomposed and harmless treatment；It is also equipped with the deodorant, function such as anti-soil, purify air simultaneously.
Content of the invention
It is an object of the invention to provide a kind of have delicate fragrance type carbon leaching material of strong catalytic degradation effect and preparation method thereof.
In order to realize the purpose of the present invention, the present invention is implemented by below scheme：
A kind of delicate fragrance type carbon leaching material with strong catalytic degradation effect, is made up of the raw material of following weight portion：Activated carbon 137-147, nano titanium oxide 9-13, acrylic acid 3-4, potassium sulfate 3-5, clay 8-11, Diammonium phosphate (DAP) 2-3, sodium peroxydisulfate 1-2, sweet orange oil 0.6-0.9, Fructus Corni shell 20-25, longan pericarp 24-28, rich coal 5-7, adsorption aid 4-6, appropriate amount of water；
Described adsorption aid is made up of the raw material of following weight portion：Rice husk 9-12, tea seed episperm 8-11, silica 1 2-14, activated alumina 6-8, bamboo fibre 1-2, pulverizing monkey grass 2-3, ironic citrate 1-2, peach gum powder 2-3；Preparation method is that rice husk, tea seed episperm are dried under the conditions of 100 DEG C -120 DEG C 1-1.5 hour, it is ground into 40-60 mesh powder, it is subsequently adding suitable quantity of water to stir with remaining residual components in addition to bamboo fibre, peach gum powder, form purees, it is then placed in 400 DEG C -500 DEG C of retort carbonizing 2-3 hour, it is ground into 80-100 mesh powder after taking out cooling, add bamboo fibre, peach gum powder and pure water to grind 1-2 hour, be finally spray-dried and obtain final product.
A kind of delicate fragrance type carbon leaching material with strong catalytic degradation effect of the present invention, is made up of step in detail below：
（1）Fructus Corni shell, longan pericarp, rich coal are dried 1-1.5 hour under conditions of 90 DEG C -110 DEG C, is ground into 60-80 mesh mixed-powder stand-by；
（2）Appropriate water will be added in nano titanium oxide, clay, it is stirred continuously and make slurry, then after mixing with mixed-powder, add remaining residual components in addition to activated carbon, sweet orange oil, adsorption aid, it is heated to 40 DEG C -60 DEG C, it is incubated and is stirred continuously 1.5-2 hour, obtain mixed slurry stand-by；
（3）Activated carbon is pulverized and mixes with mixed slurry, be placed in Muffle furnace at 350 DEG C～450 DEG C, activate 65～90 minutes, after cooling, be ground into 100-120 mesh powder, spray sweet orange oil on surface after mixing with adsorption aid and obtain final product filtering material.
The invention has the beneficial effects as follows：Fructus Corni shell, longan pericarp are added in activated carbon by the present invention by series of process, product is made to have multiple pore passage structures and big specific surface area, add nano titanium oxide, there is strong catalytic degradation effect, effectively remove multiple noxious materials, antibacterial, decontamination, add sweet orange oil, fresh air, the carbon leaching material using effect that the present invention is obtained is good simultaneously, durable in use, it is suitable for making air conditioner filter screen or air purifier.
Specific embodiments
Below by instantiation, the present invention is described in detail.
A kind of delicate fragrance type carbon leaching material with strong catalytic degradation effect, by following weight portion（Kilogram）Raw material make：Activated carbon 137, nano titanium oxide 9, acrylic acid 3, potassium sulfate 3, clay 8, Diammonium phosphate (DAP) 2, sodium peroxydisulfate 1, sweet orange oil 0.6, Fructus Corni shell 20, longan pericarp 24, rich coal 5, adsorption aid 4, appropriate amount of water；
Described adsorption aid is by following weight portion（Kilogram）Raw material make：Rice husk 9, tea seed episperm 8, silica 12, activated alumina 6, bamboo fibre 1, pulverizing monkey grass 2, ironic citrate 1, peach gum powder 2；Preparation method is that rice husk, tea seed episperm are dried under the conditions of 100 DEG C -120 DEG C 1-1.5 hour, it is ground into 40-60 mesh powder, it is subsequently adding suitable quantity of water to stir with remaining residual components in addition to bamboo fibre, peach gum powder, form purees, it is then placed in 400 DEG C -500 DEG C of retort carbonizing 2-3 hour, it is ground into 80-100 mesh powder after taking out cooling, add bamboo fibre, peach gum powder and pure water to grind 1-2 hour, be finally spray-dried and obtain final product.
A kind of delicate fragrance type carbon leaching material with strong catalytic degradation effect of the present invention, is made up of step in detail below：
（1）Fructus Corni shell, longan pericarp, rich coal are dried 1-1.5 hour under conditions of 90 DEG C -110 DEG C, is ground into 60-80 mesh mixed-powder stand-by；
（2）Appropriate water will be added in nano titanium oxide, clay, it is stirred continuously and make slurry, then after mixing with mixed-powder, add remaining residual components in addition to activated carbon, sweet orange oil, adsorption aid, it is heated to 40 DEG C -60 DEG C, it is incubated and is stirred continuously 1.5-2 hour, obtain mixed slurry stand-by；
（3）Activated carbon is pulverized and mixes with mixed slurry, be placed in Muffle furnace at 350 DEG C～450 DEG C, activate 65～90 minutes, after cooling, be ground into 100-120 mesh powder, spray sweet orange oil on surface after mixing with adsorption aid and obtain final product filtering material.
Carry out performance test using the filter screen that filtering material of the present invention is obtained, important technological parameters are：The technical indicator of air purification processing equipment is：Dust granules minimum grain size scope 0.5-10 μm of capture；Trapping micronic dust efficiency >=99%；Through the effect of 4 hours, concentration of formaldehyde declined 87.1%.
Claims (1)
1. a kind of delicate fragrance type carbon leaching material with strong catalytic degradation effect is it is characterised in that be made up of the raw material of following weight portion：Activated carbon 137-147, nano titanium oxide 9-13, acrylic acid 3-4, potassium sulfate 3-5, clay 8-11, Diammonium phosphate (DAP) 2-3, sodium peroxydisulfate 1-2, sweet orange oil 0.6-0.9, Fructus Corni shell 20-25, longan pericarp 24-28, rich coal 5-7, adsorption aid 4-6, appropriate amount of water；
Described adsorption aid is made up of the raw material of following weight portion：Rice husk 9-12, tea seed episperm 8-11, silica 1 2-14, activated alumina 6-8, bamboo fibre 1-2, pulverizing monkey grass 2-3, ironic citrate 1-2, peach gum powder 2-3；Preparation method is that rice husk, tea seed episperm are dried under the conditions of 100 DEG C -120 DEG C 1-1.5 hour, it is ground into 40-60 mesh powder, it is subsequently adding suitable quantity of water to stir with remaining residual components in addition to bamboo fibre, peach gum powder, form purees, it is then placed in 400 DEG C -500 DEG C of retort carbonizing 2-3 hour, it is ground into 80-100 mesh powder after taking out cooling, add bamboo fibre, peach gum powder and pure water to grind 1-2 hour, be finally spray-dried and obtain final product；
A kind of described delicate fragrance type carbon leaching material with strong catalytic degradation effect is made up of step in detail below：
（1）Fructus Corni shell, longan pericarp, rich coal are dried 1-1.5 hour under conditions of 90 DEG C -110 DEG C, is ground into 60-80 mesh mixed-powder stand-by；
（2）Appropriate water will be added in nano titanium oxide, clay, it is stirred continuously and make slurry, then after mixing with mixed-powder, add remaining residual components in addition to activated carbon, sweet orange oil, adsorption aid, it is heated to 40 DEG C -60 DEG C, it is incubated and is stirred continuously 1.5-2 hour, obtain mixed slurry stand-by；
（3）Activated carbon is pulverized and mixes with mixed slurry, be placed in Muffle furnace at 350 DEG C～450 DEG C, activate 65～90 minutes, after cooling, be ground into 100-120 mesh powder, spray sweet orange oil on surface after mixing with adsorption aid and obtain final product filtering material.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201410639873.7A CN104474780B (en) | 2014-11-13 | 2014-11-13 | Faint scent active carbon filter material with strong catalytic degradation effect, and preparation method thereof |
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| CN201410639873.7A CN104474780B (en) | 2014-11-13 | 2014-11-13 | Faint scent active carbon filter material with strong catalytic degradation effect, and preparation method thereof |
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| CN104474780B true CN104474780B (en) | 2017-02-08 |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN104905724B (en) * | 2015-05-11 | 2017-06-16 | 广德县新杭镇聚源新型材料压膜厂 | A kind of toilet lid that can adsorb stink substance |
| CN104841369A (en) * | 2015-05-15 | 2015-08-19 | 陈君武 | Air filter element for cellular network active carbon filter and preparation method thereof |
| CN105647213A (en) * | 2015-12-31 | 2016-06-08 | 赵星安 | Bamboo charcoal plate and manufacturing method thereof |
| CN106268632A (en) * | 2016-07-19 | 2017-01-04 | 浙江绿冠环保科技有限公司 | A kind of charcoal photocatalyst formaldehyde purifying agent and preparation method thereof |
| CN107252588B (en) * | 2017-07-26 | 2019-08-09 | 浙江玉智德新材料科技有限公司 | A kind of antibacterial filter material and preparation method thereof |
| CN107497396B (en) * | 2017-09-13 | 2019-08-09 | 浙江玉智德新材料科技有限公司 | A kind of antibacterial filter material and its anhydrous method preparation process |
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| JPH05138017A (en) * | 1991-11-20 | 1993-06-01 | Nippondenso Co Ltd | Production of deodorant |
| CN1454708A (en) * | 2002-04-30 | 2003-11-12 | 中国人民解放军63971部队 | Method of preparing composite photocatalytic material for air purification |
| CN102784621A (en) * | 2012-08-29 | 2012-11-21 | 西南科技大学 | Method for preparing biomass adsorption material based on modified rice husks |
| CN103566872A (en) * | 2013-09-26 | 2014-02-12 | 蚌埠华纺滤材有限公司 | Dogwood kernel modified active carbon water purifier and preparation method thereof |
| CN103977760A (en) * | 2014-05-09 | 2014-08-13 | 苏州洁宝机械有限公司 | Filter material for air purifier |
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2014
- 2014-11-13 CN CN201410639873.7A patent/CN104474780B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH05138017A (en) * | 1991-11-20 | 1993-06-01 | Nippondenso Co Ltd | Production of deodorant |
| CN1454708A (en) * | 2002-04-30 | 2003-11-12 | 中国人民解放军63971部队 | Method of preparing composite photocatalytic material for air purification |
| CN102784621A (en) * | 2012-08-29 | 2012-11-21 | 西南科技大学 | Method for preparing biomass adsorption material based on modified rice husks |
| CN103566872A (en) * | 2013-09-26 | 2014-02-12 | 蚌埠华纺滤材有限公司 | Dogwood kernel modified active carbon water purifier and preparation method thereof |
| CN103977760A (en) * | 2014-05-09 | 2014-08-13 | 苏州洁宝机械有限公司 | Filter material for air purifier |
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Inventor after: Wang Lixin Inventor before: Sun Xiyu |
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Effective date of registration: 20161109 Address after: 241200 Anhui Province, Wuhu City asan cypress Fanchang County Town Village Industrial Park Applicant after: WUHU CHUANGYUAN NEW MATERIALS CO., LTD. Address before: 233000 building, long march road, high tech Zone, Anhui, Bengbu, No. 1188, building No. 1 Applicant before: Bengbu Demo Filtration Technology Co., Ltd. |
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Effective date of registration: 20190122 Address after: No. 2199 Lane 38, Jiangchuan Road, Minhang District, Shanghai 201100 Patentee after: Shanghai Activated Carbon Factory Limited Address before: 241200 Baishu Village Industrial Park, Eshan Town, Fanchang County, Wuhu City, Anhui Province Patentee before: WUHU CHUANGYUAN NEW MATERIALS CO., LTD. |
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Address after: 201500 no.5359 Nanting Road, Tinglin Town, Jinshan District, Shanghai Patentee after: SHANGHAI ACTIVATED CARBON FACTORY Co.,Ltd. Address before: No. 2199 Lane 38, Jiangchuan Road, Minhang District, Shanghai 201100 Patentee before: SHANGHAI ACTIVATED CARBON FACTORY Co.,Ltd. |