CN105600848B - A kind of purification of water quality packet and its preparation method and application using the preparation of Khotan jade ore - Google Patents
A kind of purification of water quality packet and its preparation method and application using the preparation of Khotan jade ore Download PDFInfo
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/66—Treatment of water, waste water, or sewage by neutralisation; pH adjustment
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/01—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
- C04B35/16—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on silicates other than clay
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/34—Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3427—Silicates other than clay, e.g. water glass
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/34—Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3427—Silicates other than clay, e.g. water glass
- C04B2235/3436—Alkaline earth metal silicates, e.g. barium silicate
- C04B2235/3454—Calcium silicates, e.g. wollastonite
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/34—Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3427—Silicates other than clay, e.g. water glass
- C04B2235/3463—Alumino-silicates other than clay, e.g. mullite
Abstract
The present invention relates to a kind of purification of water quality packets and its preparation method and application using the preparation of Khotan jade ore.Preparation method includes the preparation of Ceramic Balls and the preparation of purification packet, and the preparation of the Ceramic Balls includes sorting, is crushed, mixed-forming, sintering.The Ceramic Balls main component includes at least one of Khotan jade ore, diopside and forsterite ophicalcite, and optionally contains Tourmaline, clinoptilolite, medical stone.Purified water quality is in alkalescent, and the water negative potential after activation is maintained at -50 to -100mV, is detected 017-NMP, shown the result is that small-micelle water.
Description
Technical field
The present invention relates to a kind of methods for preparing purification of water quality packet, and purification packet and purification packet that thus method obtains are used
In the purposes of purifying drinking water.
Background technique
The fast development of water purification industry has driven function ceramics ball market to continue to develop innovation.Function ceramics ball is mainly answered
Used in Water purifier filter, humidifier antibacterial and water heater scale removal etc..Major product has Chinese medicine stone ceramic ball, tourmaline ceramic
Ball, micropore anti-bacteria ceramic ball, negative potential Ceramic Balls, the dechlorination products such as Ceramic Balls and scale removal Ceramic Balls.
The manufacture of function ceramics ball mainly utilizes natural crystal material, such as medical stone, tourmaline, volcanic rock, diatomite
Equal mineral materials by materials such as addition anti-biotic material, anion material and magnesium alloys, then are equipped with the ceramics such as kaolin, clay
Material is made through techniques such as mixing, granulation, sintering, washing, screenings.
CN1123768A discloses a kind of component of purifying and mineralizing drinking water, selects argillaceous siltstoue, tiltedly hair
Zeolite, active carbon, Longjiang medical stone, celestine, selenium ore, shell, boehmite, garnet carry out grain size distribution and portion rate,
Harmful substance in absorption water, and netted using load silver and dissolve out silver ion and galactic pole plate release silver ion killing bacterium, after net mineralising
Water quality meets national Drinking Water matter.
CN1554590A discloses the method with artificial quartz sand substitution natural sand purifying drinking water.Exploitation is met into filter
The quartz mine that material requires carries out level-one and is crushed, and two-stage crushing, three-level is broken, and quartz sand ore is after three-level is broken, by skin
Band conveyer enters tumbling ball mill, is processed with 20kg/min, eliminates present on polygonal graininess quartz sand ore
Acute angle；Quartz sand by chamfering enters screening plant, and quartz sand after screening enters the hopper of different size, will process
Good granular quartz sand is put into the filter layer in purifying system of water plant as filtrate, and it is natural to complete artificial stone sand substitution
Sand purifying drinking water.
CN1698948A is disclosed using palygorskite, sepiolite as the water scavengine agent of carrier, is the mine in palygorskite, sepiolite
In object lattice and its surface is equipped with ferric ion and its hydroxide, by weight, the content of ferro element in the catalyst
For 1-25%.This kind of water scavengine agent is from a wealth of sources, cheap using natural palygorskite, sepiolite as primary raw material.
CN101481168A discloses a kind of drinking water purification treatment material, by high temperature sintering tourmaline nanometer powder, alkali
Property mineral dust and magnesium metal form.Peculiar smell in water can be effectively removed, there are antibacterial functions, there is mineralising, activation to drinking water
With the effect of smallization water clusters, the balance that physical efficiency reaches pH value is made one.
CN101519301A discloses a kind of ceramic ball for purifying water quality.By Tourmaline, Brazilian tourmaline, clinoptilolite, wheat meal
Stone, selenium stone, diatomite and binder are sintered jointly, and wherein each component granularity is 6000 mesh or more.Gained purification of water quality pottery
Porcelain ball activity is good, and salinity is high, long service life；Water quality after its activation is beneficial to human health.
CN102942229A discloses a kind of preparation method of mineral substance water quality cleanser.Using natural zeolite as raw material, successively
By the broken and screening of natural zeolite ore, high-temperature roasting processing, aluminium processing, the preparation of acid processing and five sections of hydrophobic treatment processing
Step obtains.As filtering material, every gram of mineral substance water quality cleanser is greater than 200mg/g to the absorption exchange capacity of calcium, comprehensive to inhale
Attached exchange capacity is greater than 350mg/g.
CN103058291A discloses a kind of Activated-water hydrogen production material.It include the powder of copper, zinc, magnesium, component by component A
B granular magnesium, component C Tourmaline, purification ore, clay are made.Wherein component A is cooling manufactured spherical by high-temperature fusion
Body, component C are to crush the orbicule mediated and formed.The material can inhibit fungus grown in water.
CN103316627A discloses a kind of clean reagent in drinking water and the preparation method and application thereof, by bauxite, fluorite, side
Xie Shi, bentonite, attapulgite, volcanic rock are made；The impurity in each raw ore is rejected by picking now, then prepared, forged
The powdery clean reagent in drinking water that fineness is 400-600 mesh is prepared in burning, crushing grinding, compound, carbonization, stirring.It is purified
Water quality is up to national second level drinking water standard.
CN104987053A discloses a kind of Ceramic Balls of Water warfare, and by π stone ball, tourmaline ball, selenium-rich mineralization ball is born
Current potential ball, limonite ball, medical stone ball, active carbon are made.By evenly mixing, goal is levigate broken, crosses 5000-8000 mesh, so
Roll-forming or injection forming afterwards, it is then shady and cool to place dry and repaired biscuit, it reenters kiln 1250-1300oC high temperature and forms by a firing, pass through
Cross refine, kiln discharge dry in the shade after to obtain the final product.It is easily absorbed by the body it is reported that the processed water energy of the Ceramic Balls enough enhances metabolism
And vivotoxin and heavy metal are discharged, it builds up health.
Based on the above-mentioned prior art, it is seen that water quality cleansing agent mainly is made using various function mineral, then to drinking water
Or domestic water is filtered use.
In order to further develop novel water quality cleansing agent, improves Drinking Water in China quality, propose technical solution of the present invention.
Summary of the invention
The technical problem to be solved by the present invention is to advanced optimize water quality cleansing agent, provide it is a kind of prepare purification of water quality ceramics
The method of ball.Specifically provide a kind of preparation method of purification of water quality packet, the preparation of (one) Ceramic Balls, preparing for the Ceramic Balls be specific
Including：Include the following steps：(1) sorting selects good Khotan jade ore, diopside, forsterite ophicalcite, uses after dedusting
Water rinses, naturally dry；Optional, Tourmaline, clinoptilolite, one of medical stone or a variety of is added in selection；(2) it crushes,
Khotan jade ore, diopside, forsterite ophicalcite are ground into the powder of 4000 mesh or more；(3) mixed-forming, by above-mentioned powder
Mineral dust after broken is according to weight ratio, and 50-80 parts of Khotan jade ore of component A, 10-40 parts of component B diopside, component C magnesium olive
5-20 parts of olive stone griotte, it is one or more in component D Tourmaline, clinoptilolite or medical stone, it 0-10 parts, weighs uniformly mixed
Afterwards, mineral dust and binder are mixed, is formed in nodulizer, controls the diameter 5-10mm of ball；(4) it is sintered, ball after molding
It after drying, is sintered, temperature controls 1000oC or more, and time 1-5h, natural cooling is dried after sintering to obtain the final product.(2) water quality is net
Change the preparation of packet：Ceramic Balls obtained above are clayed into power shape, purification of water quality packet is made in pack.
Preferably, the dosage of Khotan jade ore is 60-70 parts.
Preferably, the dosage of diopside is 20-30 parts.
Preferably, the dosage of forsterite ophicalcite is 10-15 parts.
Preferably, component D is one or more in Tourmaline, clinoptilolite or medical stone, and dosage is 5 parts or less.More
It is preferred that not containing component D.
Preferably, the broken mesh number of mineral powder is 5000 mesh or more in step (2), more than more preferably 6000 mesh.
Preferably, the sintering temperature in step (4) is 1200oC or more.
Preferably, the sintering time in step (4) is 2-3h.
Technical effect of the invention：
(1) water quality is in alkalescent.7.2-8.2 is positively retained at through the modified water pH value of purification of water quality packet.
(2) anti-oxidant.Verified, the water negative potential after activation is maintained at -50 to -100mV, can play oxidation resistant work
With.
(3) small molecule.017-NMP is detected, is shown the result is that small-micelle water, is no longer stagnant water, degeneration water.
Specific embodiment
Hereinafter, preferred embodiments of the present invention will be described, it should be understood that preferred embodiment described herein is only used
In the description and interpretation present invention, it is not intended to limit the present invention.
Performance test：
Purification of water quality packet is placed in municipal tap water, all data is tested after 10min.
Embodiment 1：
(1) sorting selects good Khotan jade ore, diopside, forsterite ophicalcite and Tourmaline, uses water after dedusting
It rinses, naturally dry；(2) it crushes, Khotan jade ore, diopside, forsterite ophicalcite and Tourmaline powder is broken into 4000 mesh
Powder；(3) mixed-forming, by above-mentioned smashed mineral dust according to weight ratio, 50 parts of ore of component A Khotan jade, component B
10 parts of diopside, 5 parts of component C forsterite ophicalcite, 10 parts of component D Tourmaline, weigh after mixing, by mineral dust with
Binder mixes, and forms in nodulizer, controls the diameter 5-10mm of ball；(4) it is sintered, after ball after molding dries, is sintered,
Temperature controls 1000oC, and time 1h, natural cooling is dried after sintering to obtain the final product.Ceramic Balls obtained above are clayed into power shape, dress
Purification of water quality packet is made in bag.
Embodiment 1-a
Wherein the dosage of Khotan jade ore is 60 parts, the other the same as in Example 1.
Embodiment 1-b
Wherein the dosage of Khotan jade ore is 70 parts, the other the same as in Example 1.
Embodiment 1-c
Wherein the dosage of Khotan jade ore is 80 parts, the other the same as in Example 1.It the results are shown in Table 1.
Table 1：The dosage of Khotan jade ore
| Number | PH value | Small molecule/017-NMP spectral peak halfwidth | Negative potential/mV | Dissolved oxygen/mg/L |
| Embodiment 1 | 8.1 | 45.6Hz, 4-5 hydrones | 50 | 8-10 |
| Embodiment 1-a | 7.5 | 44.1Hz, 4 hydrones | 65 | 8-10 |
| Embodiment 1-b | 7.6 | 43.2Hz, 4 hydrones | 67 | 8-10 |
| Embodiment 1-c | 8.0 | 49.8Hz, 5 hydrones | 55 | 8-10 |
From the point of view of the result of table 1, the dosage of Khotan jade ore influences the pH value of water and negative potential and small molecule after purifying
Index.It is preferred that Khotan jade ore is 60-70 parts.
Embodiment 2
The dosage of diopside is 20 parts, the other the same as in Example 1.
Embodiment 2-a
The dosage of diopside is 30 parts, the other the same as in Example 2.
Embodiment 2-b
The dosage of diopside is 40 parts, the other the same as in Example 2.It the results are shown in Table 2.
Table 2：The dosage of diopside
| Number | PH value | Small molecule/017-NMP spectral peak halfwidth | Negative potential/mV | Dissolved oxygen/mg/L |
| Embodiment 1 | 8.1 | 45.6Hz, 4-5 hydrones | 50 | 8-10 |
| Embodiment 2 | 8.0 | 45.8Hz, 4-5 hydrones | 52 | 12-15 |
| Embodiment 2-a | 7.8 | 46.6Hz, 4-5 hydrones | 51 | 12-15 |
| Embodiment 2-b | 8.1 | 45.3Hz, 4-5 hydrones | 51 | 8-10 |
From the point of view of the result of table 2, the dosage of diopside is preferably 20-30 parts.Ratio is too high or too low all to be influenced to dissolve
The content of oxygen.
Embodiment 3
The dosage of forsterite ophicalcite is 10 parts, the other the same as in Example 1.
Embodiment 3-a
The dosage of forsterite ophicalcite is 15 parts, the other the same as in Example 3.
Embodiment 3-b
The dosage of forsterite ophicalcite is 20 parts, the other the same as in Example 3.It the results are shown in Table 3.
Table 3：The dosage of forsterite ophicalcite
| Number | PH value | Small molecule/017-NMP spectral peak halfwidth | Negative potential/mV | Dissolved oxygen/mg/L |
| Embodiment 1 | 8.1 | 45.6Hz, 4-5 hydrones | 50 | 8-10 |
| Embodiment 3 | 8.0 | 44.8Hz, 4-5 hydrones | 57 | 8-10 |
| Embodiment 3-a | 7.9 | 45.1Hz, 4-5 hydrones | 59 | 8-10 |
| Embodiment 3-b | 8.1 | 45.9Hz, 4-5 hydrones | 51 | 8-10 |
From the point of view of the result of table 3, the dosage of forsterite influences the negative potential of water quality, it is preferable to use 10-15 parts.
Embodiment 4
The dosage of Tourmaline is 5 parts, the other the same as in Example 1.
Embodiment 4-a
The dosage of Tourmaline is 0 part, the other the same as in Example 4.
Embodiment 4-b
Clinoptilolite replaces Tourmaline, the other the same as in Example 4.
Embodiment 4-c
Medical stone replaces Tourmaline, the other the same as in Example 4.It the results are shown in Table 4.
Table 4：The selection of component D
| Number | PH value | Small molecule/017-NMP spectral peak halfwidth | Negative potential/mV | Dissolved oxygen/mg/L |
| Embodiment 1 | 8.1 | 45.6Hz, 4-5 hydrones | 50 | 8-10 |
| Embodiment 4 | 8.0 | 43.8Hz, 4-5 hydrones | 51 | 8-10 |
| Embodiment 4-a | 7.9 | 42.1Hz, 4 hydrones | 52 | 8-10 |
| Embodiment 4-b | 8.1 | 45.7Hz, 4-5 hydrones | 51 | 8-10 |
| Embodiment 4-c | 8.1 | 45.6Hz, 4-5 hydrones | 51 | 8-10 |
From table 4, it can be seen that can more activated micromolecular water without using component D.Tourmaline, medical stone, clinoptilolite
It is similar for the effect of water quality.
Embodiment 5
Replace that " 50 parts of ore of component A Khotan jade, 10 parts of component B diopside, component C forsterite is big with 65 parts of diopsides
Manage 5 parts of rock ", other conditions are same as Example 1.Negative potential/mV is 42, and dissolved oxygen/mg/L is 7-8.
Embodiment 6
Replaced with 65 parts of forsterite ophicalcites " 50 parts of ore of component A Khotan jade, 10 parts of component B diopside, component C magnesium
5 parts of olivine griotte ", other conditions are same as Example 1.Negative potential/mV is 40, and dissolved oxygen/mg/L is 6-8.
The foregoing is only a preferred embodiment of the present invention, is not intended to restrict the invention, although referring to aforementioned reality
Applying example, invention is explained in detail, for those skilled in the art, still can be to aforementioned each implementation
Technical solution documented by example is modified or equivalent replacement of some of the technical features.It is all in essence of the invention
Within mind and principle, any modification, equivalent replacement, improvement and so on be should all be included in the protection scope of the present invention.
Claims (5)
1. a kind of preparation method of the purification of water quality packet using the preparation of Khotan jade ore, includes the following steps：
(1) preparation of the preparation of Ceramic Balls, the Ceramic Balls specifically includes：(1) sorting selects Khotan jade ore, diopside, magnesium
At least one of olivine griotte, is rinsed with water after dedusting, naturally dry；(2) crush, by Khotan jade ore, diopside,
Forsterite ophicalcite is ground into the powder of 4000 mesh or more；(3) above-mentioned smashed mineral dust is mixed by mixed-forming
Type；(4) it is sintered, after ball after molding dries, is sintered, temperature controls 1200 DEG C or more, and time 2-3h is naturally cold after sintering
But it dries to obtain the final product；The mixed-forming step includes：It is weighed according to weight ratio, 60-70 parts of Khotan jade ore of component A, component B is saturating
20-30 parts of pyroxene, 10-15 parts of component C forsterite ophicalcite after mixing mixes mineral dust and binder, at
Ball machine molding, controls the diameter 5-10mm of ball；
(2) preparation of purification of water quality packet：Ceramic Balls obtained above are clayed into power shape, purification of water quality packet is made in pack.
2. preparation method according to claim 1, it is characterised in that：The broken mesh number of mineral powder is 5000 mesh in step (2)
More than.
3. preparation method according to claim 2, it is characterised in that：The broken mesh number of mineral powder is 6000 mesh in step (2)
More than.
4. the purification of water quality packet that preparation method according to claim 1-3 is prepared.
5. the purposes that purification of water quality packet described in claim 4 is used for purifying drinking water.
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| CN106966460A (en) * | 2017-05-27 | 2017-07-21 | 刘华文 | Water quality treater |
| CN110872194A (en) * | 2018-09-03 | 2020-03-10 | 上海安娜奥环境科技有限公司 | Ceramic ball capable of reducing water molecule agglomeration and preparation method thereof |
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| CN104086165A (en) * | 2014-07-15 | 2014-10-08 | 任新年 | Anion ceramic ball and preparation method thereof |
| CN105130401A (en) * | 2015-09-01 | 2015-12-09 | 王化頔 | Ceramic material with function of treating water into alkalescent small molecular group water, preparing method and application |
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