CN103565691B - Preparation process for slow-release water-soluble lavender essential oil - Google Patents
Preparation process for slow-release water-soluble lavender essential oil Download PDFInfo
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- CN103565691B CN103565691B CN201310270219.9A CN201310270219A CN103565691B CN 103565691 B CN103565691 B CN 103565691B CN 201310270219 A CN201310270219 A CN 201310270219A CN 103565691 B CN103565691 B CN 103565691B
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Abstract
The invention discloses a preparation process of slow-release water-soluble lavender essential oil, which includes steps of: a, adding lavender essential oil, lecithin, phytosterol, and PEG40 hydrogenated castor oil according to the weight percentage of 0.4 to 0.5% of lavender essential oil, 1 to 1.4% of lecithin, 1 to 1.4% of phytosterol, 2 to 3% of PEG40 hydrogenated castor oil, and the balance of water in a container, stirring uniformly, fully dissolving the essential oil; b, mixing the mixed solution with water, stirring uniformly, and homogenizing at three times under high pressure; and c. distilling the homogenized mixed solution, and stopping distilling until 1/3 liquid remains in a distilling flask, wherein the obtained liquid is the slow-release water-soluble essential oil. According to the slow-release water-soluble essential oil, water is used as a main carrier which avoids the adverse reaction or allergic reaction of a user due to the addition of other components, and the properties are stable. The preparation process is simple and feasible; the essential oil can be dissolved well in water; the volatile components can be released slowly; and the slow-release water-soluble lavender essential oil has a good persistence in flavor.
Description
Technical field
The present invention relates to a kind of preparation technology of slow-release water-soluble lavender essential oil, belong to medicine, beauty treatment processed and applied field.
Background technology
Improving constantly in recent years along with people's living standard, the change of consumption idea, the natural perfume material particularly feature such as vegetal natural perfume, safety green, natural with it, environmental protection obtains liking of people day by day, range of application constantly expands, no matter in China or other countries, the consumption figure of natural perfume material constantly increases.So far, the states such as France, Iran, Australia, the U.S., South Africa, Germany, Switzerland, open the application of plants essential oil in industries such as medicine, cosmetics, spice already, obtain suitable effect, the world market of plants essential oil is just flourish in recent years.Lavandula angustifolia (Lavender) belongs to purple system Labiatae (Labiatae), and have strong fragrance after plant is dry, the quintessence oil quality of refinement is splendid, and the graceful fragrance of abnormal smells from the patient, have the title of " king of spice ", is the important flavor of raw material in the world today.Lavandula angustifolia has one of medicinal plants and the spice berry plant group having attribute concurrently.Fragrance component contained by it is the important component part of natural essence spice, and its quintessence oil is extracted in the industry-by-industries such as medicine, food processing, cosmetics.Lavandula angustifolia, as a kind of important fragrant plant, is widely used in the perfumery of the daily chemical products such as foods and cosmetics, detergent, aromatic.But Herba Lysimachiae foenum-graeci quintessence oil is more volatile, wherein some composition is chemically also stable not, have impact on its storage, transport and use.On the other hand, highly purified plants essential oil zest is very strong, directly uses unsuitable control dose, if directly wiped on skin as cosmetics, can damage, so before quintessence oil uses on skin, and must first dilution process.Use after general employing base oil dilution allotment.But the shortcoming existed is that product oiliness is high, experiences poor.
Summary of the invention
The object of the present invention is to provide a kind of preparation technology of slow-release water-soluble lavender essential oil.
The technology implementation scheme that the present invention takes is, the preparation technology of this slow-release water-soluble lavender essential oil comprises the following steps: a, the percentage by weight being water by Herba Lysimachiae foenum-graeci quintessence oil 0.4-0.5%, lecithin 1-1.4%, plant sterol 1-1.4%, Cremophor RH40 2-3%, surplus in a reservoir add Herba Lysimachiae foenum-graeci quintessence oil, lecithin, plant sterol and Cremophor RH40, stir, quintessence oil dissolves completely; B, above-mentioned mixed liquor to be mixed with water, stir, high pressure homogenize three times at 40-50 DEG C: first time homogenizing 5-8min under 4000-8000rmp, second time homogenizing 8-12min under 8000-10000rmp, third time homogenizing 4-6min under 4000-5000rmp; C, by the mixed liquor after homogenizing, add in alembic and distill, liquid residual three in alembic/stop distillation for the moment, distills the liquid obtained and is slow release soluble fine.
Owing to taking technique scheme, therefore the present invention take water as the slow release soluble fine of main carriers, is the ideal essential oil product form of cosmetic field.The dissolubility of quintessence oil in water significantly improves, and product is placed for a long time can not layering, stable in properties, avoiding and add the discomfort or anaphylaxis that other compositions cause user. quintessence oil is excellent dissolution in water, concentration reduces, and slowly, product fragrance is lasting in volatile ingredient release.Easy to use, experience effect is good.Preparation technology's simple possible provided by the invention, prepared slow-release water-soluble lavender essential oil is transparent liquid, and solve after adopting base oil dilution allotment at present and use, product oiliness is high, experiences poor shortcoming.
Detailed description of the invention
Below in conjunction with specific embodiment, the present invention is described in further detail.
Embodiment 1, the preparation technology of this slow-release water-soluble lavender essential oil comprises the following steps: a, the percentage by weight being water by Herba Lysimachiae foenum-graeci quintessence oil 0.4-0.5%, lecithin 1-1.4%, plant sterol 1-1.4%, Cremophor RH40 2-3%, surplus in a reservoir add Herba Lysimachiae foenum-graeci quintessence oil, lecithin, plant sterol and Cremophor RH40, stir, quintessence oil dissolves completely; B, above-mentioned mixed liquor to be mixed with water, stir, high pressure homogenize three times at 40-50 DEG C: first time homogenizing 5min to 8min under 4000-8000rmp, second time homogenizing 8min to 12min under 8000-10000rmp, third time homogenizing 4min to 6min under 4000-5000rmp; C, by the mixed liquor after homogenizing, add in alembic and distill, in alembic, liquid residual stops distillation three/a period of time, the liquid that Distillation recovery obtains is slow release soluble fine, in alembic, remaining 1/3rd liquid are the mixed liquor of lecithin, plant sterol, Cremophor RH40 and a small amount of water, lecithin, plant sterol and Cremophor RH40 play the effect making quintessence oil water-soluble well in preparation process, and not as the composition of slow release soluble fine.The transparent color of product, with obvious Herba Lysimachiae foenum-graeci quintessence oil fragrance, occurs without oil-water separation, oil bloom phenomenon.
Claims (1)
1. the preparation technology of a slow-release water-soluble lavender essential oil, it is characterized in that comprising the following steps: a, the percentage by weight being water by Herba Lysimachiae foenum-graeci quintessence oil 0.4-0.5%, lecithin 1-1.4%, plant sterol 1-1.4%, Cremophor RH40 2-3%, surplus in a reservoir add Herba Lysimachiae foenum-graeci quintessence oil, lecithin, plant sterol and Cremophor RH40, stir, quintessence oil dissolves completely; B, above-mentioned mixed liquor to be mixed with water, stir, high pressure homogenize three times at 40-50 DEG C: first time homogenizing 5-8min under 4000-8000rmp, second time homogenizing 8-12min under 8000-10000rmp, third time homogenizing 4-6min under 4000-5000rmp; C, by the mixed liquor after homogenizing, add in alembic and distill, liquid residual three in alembic/stop distillation for the moment, distills the liquid obtained and is slow release soluble fine.
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| CN201310270219.9A CN103565691B (en) | 2013-06-21 | 2013-06-21 | Preparation process for slow-release water-soluble lavender essential oil |
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| CN201310270219.9A CN103565691B (en) | 2013-06-21 | 2013-06-21 | Preparation process for slow-release water-soluble lavender essential oil |
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| CN103565691A CN103565691A (en) | 2014-02-12 |
| CN103565691B true CN103565691B (en) | 2015-06-17 |
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| CN115386424B (en) * | 2022-09-14 | 2023-06-06 | 江西海瑞天然植物有限公司 | Preparation process of lavender slow-release water-soluble essential oil |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1904012A (en) * | 2006-07-28 | 2007-01-31 | 上海应用技术学院 | Preparation method of lavender nano-essential oil |
| CN102250689A (en) * | 2011-05-30 | 2011-11-23 | 新疆大学 | Equipment and method for extracting perfume plant essential oil by reduced pressure steam distillation |
| CN103242961A (en) * | 2013-05-16 | 2013-08-14 | 陕西科技大学 | Sugar-vitrified essential oil capsule prepared based on extrusion method and preparation method thereof |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH03111493A (en) * | 1989-09-25 | 1991-05-13 | Kanebo Ltd | Tranquilizing essential oil and perfumes containing it |
| KR100469179B1 (en) * | 2001-12-19 | 2005-01-31 | 김윤일 | Perfume for underwear |
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Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1904012A (en) * | 2006-07-28 | 2007-01-31 | 上海应用技术学院 | Preparation method of lavender nano-essential oil |
| CN102250689A (en) * | 2011-05-30 | 2011-11-23 | 新疆大学 | Equipment and method for extracting perfume plant essential oil by reduced pressure steam distillation |
| CN103242961A (en) * | 2013-05-16 | 2013-08-14 | 陕西科技大学 | Sugar-vitrified essential oil capsule prepared based on extrusion method and preparation method thereof |
Non-Patent Citations (2)
| Title |
|---|
| 张秋霞,等.薰衣草精油的研究进展.《香料香精化妆品》.2006,第21-24页. * |
| 玉筛成,等.薰衣草精油微胶囊释放性能的测定.《香料香精化妆品》.2008,第17-20页. * |
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