CN103242961A - Sugar-vitrified essential oil capsule prepared based on extrusion method and preparation method thereof - Google Patents
Sugar-vitrified essential oil capsule prepared based on extrusion method and preparation method thereof Download PDFInfo
- Publication number
- CN103242961A CN103242961A CN2013101814464A CN201310181446A CN103242961A CN 103242961 A CN103242961 A CN 103242961A CN 2013101814464 A CN2013101814464 A CN 2013101814464A CN 201310181446 A CN201310181446 A CN 201310181446A CN 103242961 A CN103242961 A CN 103242961A
- Authority
- CN
- China
- Prior art keywords
- volatile oil
- capsule
- extrusion
- extruding
- prescription
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Landscapes
- Medicinal Preparation (AREA)
- Fats And Perfumes (AREA)
- Seasonings (AREA)
Abstract
The invention relates to a sugar-vitrified essential oil capsule prepared based on an extrusion method and a preparation method thereof. Essential oil is instable in nature, high in volatility, poor in water solubility and easy to deteriorate under high-temperature conditions. The preparation method comprises the following steps: preparing soya bean lecithin, water and essential oil into a pasty emulsion; mixing sucrose, modified starch and maltodextrin at a high speed, adding the emulsion, mixing according to a dry method, feeding into an extruder through a screw feeder, and extruding to prepare the essential oil capsule. The capsule prepared by the invention has a more compact and stable structure; the capsule hermetically packaged in a moisture-proof material can be stored for a long time under room temperature conditions; and the stability is greatly improved, no antioxidant needs to be used, and the capsule has a certain slow release function in application.
Description
Technical field
The present invention relates to a kind of volatile oil capsule, be specifically related to a kind of sugared vitrifying volatile oil capsule and method thereof based on the extrusion process preparation.
Background technology
Sugar vitrifying technology is the encapsulated technology of a kind of low temperature, therefore is suitable for the embedding of heat-sensitive substance.Volatile oil is a kind of volatile essential oil that extracts from spice, claim perfume oil again, it is the big class of one in the natural perfume, generally tissue or the secretory product with the scented plants different sites is raw material, adopt methods such as cold grinding, extraction, squeezing, wet distillation to extract and obtain, the mixture that its composition is made up of aliphatics, alicyclic, terpenes etc.Volatile oil has unique fragrance and stronger efficiency of preservation and sterilizing power, but character is stable inadequately, under general condition has very high volatility, causes the loss of fragrance or disappearance too early, hot conditions is next apt to deteriorate, and poorly water-soluble also makes it be restricted in Application in Food simultaneously.Therefore, it is significant to improving its range of application and utilization ratio to carry out the stabilization research of volatile oil.Be these unstable raw materials of protection and adopt appropriate means to carry out encapsulated to volatile oil, avoid its volatilization or be subjected to extraneous heat, water and oxygen effect and one of best means of bad change take place.
The encapsulated research of essence and flavoring agent since nineteen fifties just, so far the research of this respect still is in gesture in the ascendant, compare with the microcapsulary of other cores, the encapsulated difficulty of volatile oil is bigger, main because: normally tens kinds in (1) volatile oil, even the mixture of hundreds of different components, they have nothing in common with each other to the solvability of water and oil, all components are embedded in the single-matrix fully very difficult; (2) different components in the volatile oil has different boiling, and component volatilization difference is big, even some components still have very strong volatility below 0 ℃, the volatilization loss of volatile component can cause the variation of odor type; (3) many components are to sensitivities such as heat, light, pH, oxygen in the volatile oil, and preparation has brought difficulty to capsule.
Summary of the invention
The purpose of this invention is to provide a kind of sugared vitrifying volatile oil capsule and method thereof based on the extrusion process preparation, need not to add antioxidant, improved the stability of volatile oil greatly, and had the good slow release effect.
The technology used in the present invention means are:
A kind of sugared vitrifying volatile oil capsule based on the extrusion process preparation is characterized in that:
Component by following mass parts is made:
Maltodextrin DE 8-15 10-80 part;
Sucrose 1-10 part;
Volatile oil 1-15 part;
Soybean lecithin 0.5-2 part;
Water 2-8 part.
The component that also includes following weight part in the described prescription:
Modified starch 0＜m≤40 part.
A kind ofly prepare the method for sugared vitrifying volatile oil capsule based on extrusion process, it is characterized in that:
Realized by following steps:
Step 1: press each component in the following mass parts preparation prescription:
Maltodextrin DE 8-15 10-80 part;
Sucrose 1-10 part;
Modified starch 0-40 part
Volatile oil 1-15 part;
Soybean lecithin 0.5-2 part;
Water 2-8 part;
Step 2: doing of prescription material mixes:
Soybean lecithin in the prescription, water and volatile oil are prepared into the emulsion of paste under constantly stirring; Sucrose, modified starch are mixed in high-speed mixer with maltodextrin, three kinds of carbohydrate are fully mixed; The emulsion that will contain the paste of volatile oil joins in the above compound that contains three kinds of carbohydrate and carries out dry mixed, adopts high-speed mixer mixing 0.5-3 minute; The mixture that obtains is crossed the 10-60 mesh sieve make extruding Preblend;
Step 3: extruding Preblend is pushed:
Extruding Preblend enters extrusion machine by screw feeder, and the temperature of four sections extrusion chambers is set at 50-80 ℃, 80-105 ℃, 100-125 ℃, 90-115 ℃ respectively in the extrusion process; Screw speed is 40-80 rev/min, rate of feeding be the 0.8-1.5 kilogram/hour;
Step 4: the capsule of extrusion molding cools off at ambient temperature, arranges at the die head place that rotary cutter obtains the particulate state capsule product or with the capsule product that manually cuts into certain-length, capsule product is adopted every wet material pack.
In the step 3, the extrusion equipment of employing is to rotate twin-screw extruder synchronously, and length-to-diameter ratio is 24, and the die head of use is of a size of 3 millimeters, and spiro rod length is 600 millimeters, and it is four sections that extrusion chamber is divided into from the feeding mouth to the die head, and every section is equipped with inductive heater.
The present invention has the following advantages:
(1) carbohydrate matrix of embedding volatile oil has adopted the composition of three kinds of different carbohydrate.Wherein based on maltodextrin (ED8-15), adding have certain oil loving modified starch, make it make the oil soluble core more stable at embedding volatile oil, the small molecular sugar of adding such as sucrose make capsule form more form compact and stable structure.
(2) the extruding Preblend of having adopted dry mixed to prepare in the capsule formula.The carbohydrate matrix that uses in the extruding is powder, adopts mixing equipment to mix.On the other hand, the volatile oil of adding, water and soybean lecithin adopt low speed constantly to stir the emulsion of preparation paste.Direct and carbohydrate matrix directly mixes with volatile oil, water and soybean lecithin if adopt, and mixed effect can non-constant, and volatile oil will be difficult to disperse.The character that this method is prepared into paste emulsion with oil, water and soybean lecithin is added in the carbohydrate matrix and is adopted high-speed mixer to mix, and not only mixes simplyr, and makes various compositions effectively to disperse.
(3) extruding back volatile oil is scattered in the carbohydrate matrix of vitreous state with the form of small droplets, and the second-order transition temperature of capsule (35 ℃ of ﹥) is higher than room temperature.Capsule is packed can long storage under the room temperature condition in placing in wet material.The sugared vitrifying volatile oil capsule of extruding has improved the stability of volatile oil greatly.Sugar vitrifying essence does not need to use antioxidant.This capsule has certain slow-release function when using.
Embodiment
The present invention will be described in detail below in conjunction with embodiment.
Extrusion process sugar vitrifying embedding volatile oil is a kind of method of low temperature embedding, the volatile oil that can make is embedded in the carbohydrate matrix of fine and close vitreous state, and in capsule, do not need to add antioxidant, can obtain more natural, healthy, fresh product.In addition, because matrix is in vitreous state, so the stability of product is higher.
Involved in the present invention a kind ofly prepare the method for sugared vitrifying volatile oil capsule based on extrusion process, the maltodextrin of employing is DE8-15; The modified starch that adopts is HI-CAP100 or the CAPSULE that national of the United States's starch company produces; The extrusion equipment that adopts is the synchronous rotation twin-screw extruder HAAKE PolyLab System that U.S. Thermo Electron company makes, PTW24/25D, length-to-diameter ratio is 24, the die head that uses is of a size of 3 millimeters, spiro rod length is 600 millimeters, it is four sections that extrusion chamber is divided into from the feeding mouth to the die head, and every section is equipped with inductive heater; The screw feeder that adopts is DDSR20N-PRISM, Germany.
Concrete steps are:
Step 1: press each component in the following mass parts preparation prescription:
Maltodextrin DE 8-15 10-80 part;
Sucrose 1-10 part;
Modified starch 0-40 part
Volatile oil 1-15 part;
Soybean lecithin 0.5-2 part;
Water 2-8 part.
Step 2: doing of prescription material mixes:
Soybean lecithin in the prescription, water and volatile oil are prepared into the emulsion of paste under constantly stirring; Sucrose, modified starch are mixed in high-speed mixer with maltodextrin, three kinds of carbohydrate are fully mixed; The emulsion that will contain volatile oil joins in the above compound that contains three kinds of carbohydrate and carries out dry mixed, adopts high-speed mixer mixing 0.5-3 minute; The mixture that obtains is crossed the 10-60 mesh sieve make extruding Preblend;
Step 3: extruding Preblend is pushed:
Extruding Preblend enters extrusion machine by screw feeder, and each section of extrusion chamber temperature is set and to be respectively 50-80 ℃, 80-105 ℃, 100-125 ℃, 90-115 ℃ in the extrusion process; Screw speed is 40-80 rev/min, rate of feeding be the 0.8-1.5 kilogram/hour;
Step 4: the capsule of extrusion molding cools off at ambient temperature, arranges at the die head place that rotary cutter obtains the particulate state capsule product or with the capsule product that manually cuts into certain-length, capsule product is adopted every wet material pack.
Embodiment 1:
Step 1: press each component in the following mass parts preparation prescription:
66.5 parts of maltodextrins;
16.5 parts of modified starches;
1 part of sucrose;
10 parts in volatile oil;
1 part of soybean lecithin;
5 parts in water.
Step 2: doing of prescription material mixes:
Soybean lecithin in the prescription, water and volatile oil are prepared into the emulsion of paste under constantly stirring; Sucrose, modified starch are mixed in high-speed mixer with maltodextrin, three kinds of carbohydrate are fully mixed; The emulsion that will contain volatile oil joins in the above compound that contains three kinds of carbohydrate and carries out dry mixed, adopts high-speed mixer to mix 1.5 minutes; The mixture that obtains is crossed 30 mesh sieves make extruding Preblend;
Step 3: extruding Preblend is pushed:
Extruding Preblend enters extrusion machine by screw feeder, and each section of extrusion chamber temperature is set and is respectively 65 ℃, 95 ℃, 110 ℃, 100 ℃ in the extrusion process; Screw speed is 60 rev/mins, and rate of feeding is 1.1 kilograms/hour;
Step 4: the capsule of extrusion molding cools off at ambient temperature, arranges at the die head place that rotary cutter obtains the particulate state capsule product or with the capsule product that manually cuts into certain-length, capsule product is adopted every wet material pack.
Embodiment 2:
Step 1: press each component in the following mass parts preparation prescription:
34 parts of maltodextrins;
40 parts of modified starches;
4 parts of sucrose;
15 parts in volatile oil;
2 parts of soybean lecithins;
5 parts in water.
Step 2: doing of prescription material mixes:
Soybean lecithin in the prescription, water and volatile oil are prepared into the emulsion of paste under constantly stirring; Sucrose, modified starch are mixed in high-speed mixer with maltodextrin, three kinds of carbohydrate are fully mixed; The emulsion that will contain volatile oil joins in the above compound that contains three kinds of carbohydrate and carries out dry mixed, adopts high-speed mixer to mix 0.5 minute; The mixture that obtains is crossed 10 mesh sieves make extruding Preblend;
Step 3: extruding Preblend is pushed:
Extruding Preblend enters extrusion machine by screw feeder, and each section of extrusion chamber temperature is set and is respectively 50 ℃, 80 ℃, 100 ℃, 90 ℃ in the extrusion process; Screw speed is 400 rev/mins, and rate of feeding is 0.8 kilogram/hour;
Step 4: the capsule of extrusion molding cools off at ambient temperature, arranges at the die head place that rotary cutter obtains the particulate state capsule product or with the capsule product that manually cuts into certain-length, capsule product is adopted every wet material pack.
Embodiment 3:
Step 1: press each component in the following mass parts preparation prescription:
50 parts of maltodextrins;
28 parts of modified starches;
6 parts of sucrose;
13.5 parts in volatile oil;
0.5 part of soybean lecithin;
2 parts in water.
Step 2: doing of prescription material mixes:
Soybean lecithin in the prescription, water and volatile oil are prepared into the emulsion of paste under constantly stirring; Sucrose, modified starch are mixed in high-speed mixer with maltodextrin, three kinds of carbohydrate are fully mixed; The emulsion that will contain volatile oil joins in the above compound that contains three kinds of carbohydrate and carries out dry mixed, adopts high-speed mixer to mix 1.5 minutes; The mixture that obtains is crossed 30 mesh sieves make extruding Preblend;
Step 3: extruding Preblend is pushed:
Extruding Preblend enters extrusion machine by screw feeder, and each section of extrusion chamber temperature is set and is respectively 65 ℃, 95 ℃, 110 ℃, 100 ℃ in the extrusion process; Screw speed is 60 rev/mins, and rate of feeding is 1.1 kilograms/hour;
Step 4: the capsule of extrusion molding cools off at ambient temperature, arranges at the die head place that rotary cutter obtains the particulate state capsule product or with the capsule product that manually cuts into certain-length, capsule product is adopted every wet material pack.
Embodiment 4:
Step 1: press each component in the following mass parts preparation prescription:
80 parts of maltodextrins;
10 parts of sucrose;
1 part in volatile oil;
1 part of soybean lecithin;
8 parts in water.
Step 2: doing of prescription material mixes:
Soybean lecithin in the prescription, water and volatile oil are prepared into the emulsion of paste under constantly stirring; Sucrose is mixed in high-speed mixer with maltodextrin, two kinds of carbohydrate are fully mixed; The emulsion that will contain volatile oil joins in the above compound that contains two kinds of carbohydrate and carries out dry mixed, adopts high-speed mixer to mix 3 minutes; The mixture that obtains is crossed 60 mesh sieves make extruding Preblend;
Step 3: extruding Preblend is pushed:
Extruding Preblend enters extrusion machine by screw feeder, and each section of extrusion chamber temperature is set and is respectively 80 ℃, 105 ℃, 125 ℃, 115 ℃ in the extrusion process; Screw speed is 80 rev/mins, and rate of feeding is 1.5 kilograms/hour;
Step 4: the capsule of extrusion molding cools off at ambient temperature, arranges at the die head place that rotary cutter obtains the particulate state capsule product or with the capsule product that manually cuts into certain-length, capsule product is adopted every wet material pack.
Embodiment 5:
Step 1: press each component in the following mass parts preparation prescription:
10 parts of maltodextrins;
40 parts of modified starches;
10 parts of sucrose;
15 parts in volatile oil;
2 parts of soybean lecithins;
8 parts in water.
Step 2: doing of prescription material mixes:
Soybean lecithin in the prescription, water and volatile oil are prepared into the emulsion of paste under constantly stirring; Sucrose, modified starch are mixed in high-speed mixer with maltodextrin, three kinds of carbohydrate are fully mixed; The emulsion that will contain volatile oil joins in the above compound that contains three kinds of carbohydrate and carries out dry mixed, adopts high-speed mixer to mix 3 minutes; The mixture that obtains is crossed 60 mesh sieves make extruding Preblend;
Step 3: extruding Preblend is pushed:
Extruding Preblend enters extrusion machine by screw feeder, and each section of extrusion chamber temperature is set and is respectively 80 ℃, 105 ℃, 125 ℃, 115 ℃ in the extrusion process; Screw speed is 80 rev/mins, and rate of feeding is 1.5 kilograms/hour;
Step 4: the capsule of extrusion molding cools off at ambient temperature, arranges at the die head place that rotary cutter obtains the particulate state capsule product or with the capsule product that manually cuts into certain-length, capsule product is adopted every wet material pack.
It is cited that content of the present invention is not limited to embodiment, and the conversion of any equivalence that those of ordinary skills take technical solution of the present invention by reading specification sheets of the present invention is claim of the present invention and contains.
Claims (4)
1. sugared vitrifying volatile oil capsule based on extrusion process preparation is characterized in that:
Component by following mass parts is made:
Maltodextrin DE 8-15 10-80 part;
Sucrose 1-10 part;
Volatile oil 1-15 part;
Soybean lecithin 0.5-2 part;
Water 2-8 part.
2. a kind of sugared vitrifying volatile oil capsule based on extrusion process preparation according to claim 1 is characterized in that:
The component that also includes following weight part in the described prescription:
Modified starch 0＜m≤40 part.
3. one kind prepares the method for sugared vitrifying volatile oil capsule based on extrusion process, it is characterized in that:
Realized by following steps:
Step 1: press each component in the following mass parts preparation prescription:
Maltodextrin DE 8-15 10-80 part;
Sucrose 1-10 part;
Modified starch 0-40 part
Volatile oil 1-15 part;
Soybean lecithin 0.5-2 part;
Water 2-8 part;
Step 2: doing of prescription material mixes:
Soybean lecithin in the prescription, water and volatile oil are prepared into the emulsion of paste under constantly stirring; Sucrose, modified starch are mixed in high-speed mixer with maltodextrin, three kinds of carbohydrate are fully mixed; The emulsion that will contain the paste of volatile oil joins in the above compound that contains three kinds of carbohydrate and carries out dry mixed, adopts high-speed mixer mixing 0.5-3 minute; The mixture that obtains is crossed the 10-60 mesh sieve make extruding Preblend;
Step 3: extruding Preblend is pushed:
Extruding Preblend enters extrusion machine by screw feeder, and the temperature of four sections extrusion chambers is set at 50-80 ℃, 80-105 ℃, 100-125 ℃, 90-115 ℃ respectively in the extrusion process; Screw speed is 40-80 rev/min, rate of feeding be the 0.8-1.5 kilogram/hour;
Step 4: the capsule of extrusion molding cools off at ambient temperature, arranges at the die head place that rotary cutter obtains the particulate state capsule product or with the capsule product that manually cuts into certain-length, capsule product is adopted every wet material pack.
4. according to claim 3ly a kind ofly prepare the method for sugared vitrifying volatile oil capsule based on extrusion process, it is characterized in that:
In the step 3, the extrusion equipment of employing is to rotate twin-screw extruder synchronously, and length-to-diameter ratio is 24, and the die head of use is of a size of 3 millimeters, and spiro rod length is 600 millimeters, and it is four sections that extrusion chamber is divided into from the feeding mouth to the die head, and every section is equipped with inductive heater.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310181446.4A CN103242961B (en) | 2013-05-16 | 2013-05-16 | Sugar-vitrified essential oil capsule prepared based on extrusion method and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310181446.4A CN103242961B (en) | 2013-05-16 | 2013-05-16 | Sugar-vitrified essential oil capsule prepared based on extrusion method and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103242961A true CN103242961A (en) | 2013-08-14 |
| CN103242961B CN103242961B (en) | 2015-03-25 |
Family
ID=48922841
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201310181446.4A Active CN103242961B (en) | 2013-05-16 | 2013-05-16 | Sugar-vitrified essential oil capsule prepared based on extrusion method and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN103242961B (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103565691A (en) * | 2013-06-21 | 2014-02-12 | 伊犁紫苏丽人生物科技有限公司 | Slow-release water-soluble lavender essential oil and preparation process thereof |
| CN103805211A (en) * | 2014-01-08 | 2014-05-21 | 北京八亿时空液晶科技股份有限公司 | Liquid crystal composition for multiple modes and application thereof |
| CN106580916A (en) * | 2016-12-09 | 2017-04-26 | 天津科技大学 | Preparation method of novel allicin microcapsules |
| CN109674667A (en) * | 2019-01-25 | 2019-04-26 | 广州积美国际贸易有限公司 | A kind of hair washing essence that fragrance retention is lasting |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101816914A (en) * | 2010-04-15 | 2010-09-01 | 上海应用技术学院 | Preparation method of orange flavor capsule |
| CN102440365A (en) * | 2010-10-15 | 2012-05-09 | 郝征 | Preparation technology of sugar vitrification essence |
-
2013
- 2013-05-16 CN CN201310181446.4A patent/CN103242961B/en active Active
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101816914A (en) * | 2010-04-15 | 2010-09-01 | 上海应用技术学院 | Preparation method of orange flavor capsule |
| CN102440365A (en) * | 2010-10-15 | 2012-05-09 | 郝征 | Preparation technology of sugar vitrification essence |
Non-Patent Citations (2)
| Title |
|---|
| 常大伟等: ""糖玻璃化抗坏血酸胶囊制备的挤压工艺研究"", 《食品工业科技》, vol. 31, no. 10, 31 December 2010 (2010-12-31) * |
| 李柱等: ""挤压技术在微胶囊化香精中的应用"", 《学术交流论文集》, 31 March 2004 (2004-03-31), pages 63 - 65 * |
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103565691A (en) * | 2013-06-21 | 2014-02-12 | 伊犁紫苏丽人生物科技有限公司 | Slow-release water-soluble lavender essential oil and preparation process thereof |
| CN103565691B (en) * | 2013-06-21 | 2015-06-17 | 伊犁紫苏丽人生物科技有限公司 | Preparation process for slow-release water-soluble lavender essential oil |
| CN103805211A (en) * | 2014-01-08 | 2014-05-21 | 北京八亿时空液晶科技股份有限公司 | Liquid crystal composition for multiple modes and application thereof |
| CN103805211B (en) * | 2014-01-08 | 2015-09-23 | 北京八亿时空液晶科技股份有限公司 | A kind of liquid-crystal composition and application thereof that can be used for various modes |
| CN106580916A (en) * | 2016-12-09 | 2017-04-26 | 天津科技大学 | Preparation method of novel allicin microcapsules |
| CN106580916B (en) * | 2016-12-09 | 2019-10-18 | 天津科技大学 | A kind of preparation method of allicin microcapsule |
| CN109674667A (en) * | 2019-01-25 | 2019-04-26 | 广州积美国际贸易有限公司 | A kind of hair washing essence that fragrance retention is lasting |
| CN109674667B (en) * | 2019-01-25 | 2022-01-21 | 毓美生物科技(广州)有限公司 | Shampoo essence with lasting fragrance retention |
Also Published As
| Publication number | Publication date |
|---|---|
| CN103242961B (en) | 2015-03-25 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN101322851B (en) | Method for producing Tibetan medicinal herb incense | |
| CN103242961B (en) | Sugar-vitrified essential oil capsule prepared based on extrusion method and preparation method thereof | |
| CN106619479A (en) | Plant fiber product and preparation method thereof | |
| CN106561734A (en) | A solid mosquito repellent containing argy wormwood leaf essence oil and a preparing method thereof | |
| CN103070920A (en) | Preparation process of novel salvia miltiorrhiza submicron powder particle traditional Chinese medicine decoction pieces | |
| CN104312727A (en) | Preparation method for garlic oil essence microcapsules | |
| CN103976168B (en) | A kind of take corn as the pig feed of major ingredient | |
| CN102783646A (en) | Preparation method for kudzuvine root flavone lozenge | |
| AU2014243047B2 (en) | Lutein composition suitable for infant food formulations | |
| CN101711875B (en) | Soft capsule shell composition, soft capsule prepared from same and method for preparing soft capsule shell composition and soft capsule | |
| CN105338836A (en) | Encapsulation compositions comprising spices, herbs, fruit, and vegetable powders | |
| CN103750255B (en) | A kind of blending type powder essence and preparation method thereof | |
| CN103242963A (en) | Sugar-vitrified essential oil capsule prepared based on two-stage extrusion method and preparation method thereof | |
| TWI508752B (en) | A preparation method of chrysanthemum broken wall preparation | |
| CN104382824A (en) | Nourishing and moisturizing eye cream and preparation method thereof | |
| CN102018140B (en) | Process for producing shellfish premix feed | |
| CN104171145A (en) | Gardenia-fragrance tea and preparation method thereof | |
| CN102532071A (en) | L-ascorbyl palmitate particles, and preparation method and application thereof | |
| KR101121713B1 (en) | The broccoli soap to produce with the conc. solution of beanstalk's ash and pottery core | |
| KR101330142B1 (en) | Composition for Oral administration and method for the production thereof | |
| CN103040952B (en) | Moistureproof coating method of dangfei liganning capsule | |
| CN104187537A (en) | Edible aromatic flavoring | |
| KR102195259B1 (en) | Mixture powder formulation comprising tocopherol | |
| CN106333961A (en) | Vitamin D calcium chewable tablet and preparation method thereof | |
| CN101406444B (en) | Allium chinensis extract cosmetic additive agent and use |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20170612 Address after: 510730, No. 1, building 1, No. third, bank Avenue, Guangzhou Free Trade Zone, Guangzhou, Guangdong Patentee after: Guangzhou Zhen Xin Flavors & Fragrances Co., Ltd. Address before: 710021 Shaanxi city of Xi'an province Weiyang University City Patentee before: Shaanxi University of Science and Technology |
|
| TR01 | Transfer of patent right |