CN103565691A - Slow-release water-soluble lavender essential oil and preparation process thereof - Google Patents
Slow-release water-soluble lavender essential oil and preparation process thereof Download PDFInfo
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- CN103565691A CN103565691A CN201310270219.9A CN201310270219A CN103565691A CN 103565691 A CN103565691 A CN 103565691A CN 201310270219 A CN201310270219 A CN 201310270219A CN 103565691 A CN103565691 A CN 103565691A
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Abstract
The invention discloses slow-release water-soluble lavender essential oil and a preparation process thereof. The slow-release water-soluble lavender essential oil comprises the following components in percentage by weight: 4 to 0.5% of lavender essential oil, 1 to 1.4% of lecithin, 1 to 1.4% of phytosterol, 2 to 3% of CO40 efficient solubilizer, and the balance of water. The preparation process comprises the following steps of: a, adding the lavender essential oil, lecithin, phytosterol and CO40 efficient solubilizer to a vessel based on the ratio, and uniformly agitating; b, mixing the mixed solution with water, uniformly agitating, and homogenizing at three times under high pressure; and c. distilling the homogenized mixed solution, and stopping distilling until 1/3 liquid remains in a distilling flask, wherein the obtained liquid is the slow-release water-soluble essential oil. According to the slow-release water-soluble essential oil, water is used as a main carrier which avoids the adverse reaction or allergic reaction of a user due to the addition of other components, and the properties are stable. The preparation process is simple and feasible; the essential oil can be dissolved well in water; the volatile components can be released slowly; and the slow-release water-soluble lavender essential oil has a good persistence in flavor.
Description
Technical field
The present invention relates to a kind of lavandula angustifolia slow release soluble fine and preparation technology thereof, belong to medicine, beauty treatment processed and applied field.
Background technology
Improving constantly along with people's living standard in recent years, the change of consumption idea, natural perfume material particularly vegetal natural perfume obtains liking of people day by day with features such as its green, natural, safety, environmental protection, range of application constantly expands, no matter, in China or other countries, the consumption figure of natural perfume material constantly increases.So far, the states such as France, Iran, Australia, the U.S., South Africa, Germany, Switzerland, open plants essential oil already in the application of the industries such as medicine, cosmetics, spice, obtain suitable effect, and the world market of plants essential oil is just flourish in recent years.It is Labiatae (Labiatae) that lavandula angustifolia (Lavender) belongs to purple, after plant is dry, has strong fragrance, and the quintessence oil quality of refinement is splendid, and abnormal smells from the patient is graceful fragrant, have the important flavor of raw material in the title ，Shi world today of " king of spice ".Lavandula angustifolia is one of plant group having concurrently medicinal plants and the total attribute of spice berry.Its contained fragrance component is the important component part of natural essence spice, and its quintessence oil is extracted for industry-by-industries such as medicine, food processing, cosmetics.Lavandula angustifolia, as a kind of important fragrant plant, is widely used in the perfumery of the daily chemical products such as foods and cosmetics, detergent, aromatic.But Herba Lysimachiae foenum-graeci quintessence oil is more volatile, wherein some composition, chemically also stable not, has affected its storage, transportation and use.On the other hand, highly purified plants essential oil zest is very strong, and directly use should not be controlled dosage, if directly wiped on skin as cosmetics, can damage, so before quintessence oil uses on skin, must first dilution process.After general employing base oil dilution allotment, use.But the shortcoming existing is that product oiliness is high, experiences poor.
Summary of the invention
The object of the present invention is to provide a kind of lavandula angustifolia slow release soluble fine and preparation technology thereof.
The technology implementation scheme that the present invention takes is, this lavandula angustifolia slow release soluble fine comprises the component of following percentage by weight: Herba Lysimachiae foenum-graeci quintessence oil 4-5 ‰, lecithin 1-1.4%, and plant sterol 1-1.4%, CO40 efficient solubilizing agents 2-3%, surplus is water.
The preparation technology of above-mentioned lavandula angustifolia slow release soluble fine, comprises the following steps: a, in container, add in proportion Herba Lysimachiae foenum-graeci quintessence oil, lecithin, plant sterol and CO40 efficient solubilizing agents, stir, quintessence oil dissolves completely; B, above-mentioned mixed liquor is mixed with water, stir, at 40-50 ℃, high pressure homogenize is three times: homogenizing 5min to 8min under 4000rmp to 8000rmp for the first time, homogenizing 8min to 12min under 8000rmp to 10000rmp, for the third time homogenizing 4min to 6min under 4000rmp to 5000rmp for the second time; C, by the mixed liquor after homogenizing, add in alembic and distill, liquid residue three in alembic/stop distillation for the moment, reclaims the liquid obtaining and is slow release soluble fine.
Owing to having taked technique scheme, therefore the slow release soluble fine that water is main carriers is take in the present invention, be the ideal essential oil product form of cosmetic field.The dissolubility of quintessence oil in water significantly improves, and the long-time placement of product can layering, stable in properties, avoided adding discomfort or the anaphylaxis that other compositions cause user. quintessence oil is excellent dissolution in water, concentration reduces, and volatile ingredient discharges slowly, and product fragrance is lasting.Easy to use, experience effect is good.Preparation technology's simple possible provided by the invention, prepared lavandula angustifolia slow release soluble fine is transparent liquid, has solved after current employing base oil dilution is allocated and has used, product oiliness is high, experiences poor shortcoming.
The specific embodiment
Below in conjunction with specific embodiment, the present invention is described in further detail.
Embodiment 1, and this lavandula angustifolia slow release soluble fine comprises the component of following percentage by weight: Herba Lysimachiae foenum-graeci quintessence oil 4-5 ‰, lecithin 1-1.4%, and plant sterol 1-1.4%, CO40 efficient solubilizing agents 2-3%, surplus is water.The preparation technology of above-mentioned lavandula angustifolia slow release soluble fine, comprises the following steps: a, in container, add in proportion Herba Lysimachiae foenum-graeci quintessence oil, lecithin, plant sterol and CO40 efficient solubilizing agents, stir, quintessence oil dissolves completely; B, above-mentioned mixed liquor is mixed with water, stir, at 40-50 ℃, high pressure homogenize is three times: homogenizing 5min to 8min under 4000-8000rmp, for the second time homogenizing 8min to 12min under 8000-10000rmp, for the third time homogenizing 4min to 6min under 4000-5000rmp for the first time; C, by the mixed liquor after homogenizing, add in alembic and distill, liquid residue three in alembic/stop for the moment distilling, the liquid that Distillation recovery obtains is slow release soluble fine, in alembic, remaining 1/3rd liquid are the mixed liquor of lecithin, plant sterol, CO40 efficient solubilizing agents and a small amount of water, lecithin, plant sterol and CO40 efficient solubilizing agents play and make quintessence oil water-soluble effect well in preparation process, and not as the composition of slow release soluble fine.Product is transparent color, with obvious Herba Lysimachiae foenum-graeci quintessence oil fragrance, without oil-water separation, oil bloom phenomenon, occurs.
Claims (2)
1. a lavandula angustifolia slow release soluble fine, is characterized in that comprising the component of following percentage by weight: Herba Lysimachiae foenum-graeci quintessence oil 4-5 ‰, lecithin 1-1.4%, and plant sterol 1-1.4%, CO40 efficient solubilizing agents 2-3%, surplus is water.
2. the preparation technology of a lavandula angustifolia slow release soluble fine claimed in claim 1, it is characterized in that comprising the following steps: a, in container, add in proportion Herba Lysimachiae foenum-graeci quintessence oil, lecithin, plant sterol and CO40 efficient solubilizing agents, stir, quintessence oil dissolves completely; B, above-mentioned mixed liquor is mixed with water, stir, at 40-50 ℃, high pressure homogenize is three times: homogenizing 5-8min under 4000-8000rmp, for the second time homogenizing 8-12min under 8000-10000rmp, for the third time homogenizing 4-6min under 4000-5000rmp for the first time; C, by the mixed liquor after homogenizing, add in alembic and distill, liquid residue three in alembic/stop distillation for the moment, the liquid that distillation obtains is slow release soluble fine.
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| CN201310270219.9A CN103565691B (en) | 2013-06-21 | 2013-06-21 | Preparation process for slow-release water-soluble lavender essential oil |
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| CN201310270219.9A CN103565691B (en) | 2013-06-21 | 2013-06-21 | Preparation process for slow-release water-soluble lavender essential oil |
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| CN103565691A true CN103565691A (en) | 2014-02-12 |
| CN103565691B CN103565691B (en) | 2015-06-17 |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115386424A (en) * | 2022-09-14 | 2022-11-25 | 江西海瑞天然植物有限公司 | Preparation process of lavender slow-release water-soluble essential oil |
Citations (5)
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|---|---|---|---|---|
| JPH03111493A (en) * | 1989-09-25 | 1991-05-13 | Kanebo Ltd | Tranquilizing essential oil and perfumes containing it |
| KR20030050722A (en) * | 2001-12-19 | 2003-06-25 | 김윤일 | Perfume for underwear |
| CN1904012A (en) * | 2006-07-28 | 2007-01-31 | 上海应用技术学院 | Preparation method of lavender nano-essential oil |
| CN102250689A (en) * | 2011-05-30 | 2011-11-23 | 新疆大学 | Equipment and method for extracting perfume plant essential oil by reduced pressure steam distillation |
| CN103242961A (en) * | 2013-05-16 | 2013-08-14 | 陕西科技大学 | Sugar-vitrified essential oil capsule prepared based on extrusion method and preparation method thereof |
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2013
- 2013-06-21 CN CN201310270219.9A patent/CN103565691B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH03111493A (en) * | 1989-09-25 | 1991-05-13 | Kanebo Ltd | Tranquilizing essential oil and perfumes containing it |
| KR20030050722A (en) * | 2001-12-19 | 2003-06-25 | 김윤일 | Perfume for underwear |
| CN1904012A (en) * | 2006-07-28 | 2007-01-31 | 上海应用技术学院 | Preparation method of lavender nano-essential oil |
| CN102250689A (en) * | 2011-05-30 | 2011-11-23 | 新疆大学 | Equipment and method for extracting perfume plant essential oil by reduced pressure steam distillation |
| CN103242961A (en) * | 2013-05-16 | 2013-08-14 | 陕西科技大学 | Sugar-vitrified essential oil capsule prepared based on extrusion method and preparation method thereof |
Non-Patent Citations (2)
| Title |
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| 张秋霞，等: "薰衣草精油的研究进展", 《香料香精化妆品》 * |
| 玉筛成，等: "薰衣草精油微胶囊释放性能的测定", 《香料香精化妆品》 * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115386424A (en) * | 2022-09-14 | 2022-11-25 | 江西海瑞天然植物有限公司 | Preparation process of lavender slow-release water-soluble essential oil |
| CN115386424B (en) * | 2022-09-14 | 2023-06-06 | 江西海瑞天然植物有限公司 | Preparation process of lavender slow-release water-soluble essential oil |
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| CN103565691B (en) | 2015-06-17 |
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