CN103555152A - UV light-cured transfer adhesive composition - Google Patents
UV light-cured transfer adhesive composition Download PDFInfo
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- CN103555152A CN103555152A CN201310451131.7A CN201310451131A CN103555152A CN 103555152 A CN103555152 A CN 103555152A CN 201310451131 A CN201310451131 A CN 201310451131A CN 103555152 A CN103555152 A CN 103555152A
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Abstract
The invention discloses a UV light-cured transfer adhesive composition. Being a 100% solid content UV coating, the coating comprises the following components by weight part: 40-70 of light-cured resin, 25-55 of a photopolymerizable monomer, 2-6 of a photoinitiator, and 1-5 of an assistant. In the invention, a UV light-cured transfer adhesive composition coating pressed by a template with specific lines is adopted, and at the same time of mold pressing, the specific lines of the template are transferred onto the UV light-cured transfer adhesive composition coating by UV light curing. Compared with the prior art, the composition provided by the invention employs a 100% solid content UV formula, which involves fewer solvents or no solvent, less solvent evaporation occurs during use, and air pollution is reduced. At the same time, the temperature is low during UV curing, and the influence of thermal deformation on a substrate decreases.
Description
Technical field
The present invention relates to UV photo-cured coating field, be specifically related to a kind of UV photocuring transfer printing glue composition.
Background technology
Along with lightening development of electronic product such as mobile phone, notebook, household electrical appliances, the accessory such as electronic product shell used, button adopts plasthetics, but plasthetics has the shortcomings such as resistance to solvent, abrasion performance be poor.Solve the above-mentioned shortcoming of plasthetics and can adopt one deck supercoat or ink in its surface, in traditional thermosetting coating or ink samples process, need to toast, most of plasthetics is all thermo-labile, in bake process, can cause the defects such as plastic deformed.Adopt UV photo-cured coating can effectively avoid the problem of plasthetics baking distortion, and in UV photo-cured coating formula, contain less solvent or not containing solvent, reduce solvent evaporates in production process, effectively protection of the environment.After plasthetics surface-coated UV transfer printing glue, UV transfer printing glue-line has the advantages such as resistance to solvent, abrasion performance, not only effectively avoids the shortcomings such as the resistance to solvent of plastic cement, abrasion performance be poor, also because UV glue-line has some special texture structures, such as drawing pattern, woven pattern, cloudy surface etc., can play the effect of beautiful decoration.
Summary of the invention
The object of the present invention is to provide a kind of UV photocuring transfer printing glue composition, by said composition, can produce the base material of specific lines.
The object of the invention is to be achieved through the following technical solutions:
The present invention relates to a kind of UV photocuring transfer printing glue composition, it is characterized in that, comprise following component and parts by weight:
Preferably, comprise following component and parts by weight:
Preferably, described light-cured resin is one or more of epoxy acrylic resin, Polyurethane acrylic resin, polyester acrylic resin, pure the third resin.
Preferably, described light-cured resin is CN104, CNUVE151, CN120, CN121, CN704, CN8000, CN9010, CN9013, CN9893 of Sartomer company etc., one or more in the 621-100 of Changxing chemistry, 6215-100,6071,6158-80,6195-100.
Preferably, described photopolymerization monomer be monofunctional acrylate, bifunctional acrylate, polyfunctional acrylic ester, in one or more.
Preferably, described photo polymerization monomer is that weight ratio is (2～3): (1.5～2): the compound of 1 monofunctional acrylate, bifunctional acrylate, polyfunctional acrylic ester.
Preferably, described monofunctional acrylate is one or more in Hydroxyethyl acrylate, Propylene glycol monoacrylate, 2-phenoxyethyl acrylate (as: SR339, EM210), lauric acid acrylate (as: EM215, EM315), isodecyl acrylate (as: SR395, EM219), iso-bornyl acrylate (as: SR506, EM219), benzyl acrylate (as: EM75), tetrahydrofurfuryl acrylate (as: SR285, EM214).
Preferably, described bifunctional acrylate is 1,6 hexanediol diacrylate (as: SR238, EM221), tripropylene glycol diacrylate (as: SR306, EM223), propylene glycol diacrylate (as: EM222), neopentylglycol diacrylate (as: EM225), ethoxyquin bisphenol a diacrylate (as: EM2261, EM2263), tristane dimethanol diacrylate (as: SR833S, EM2204).
Preferably, described polyfunctional acrylic ester is (ethoxyquin) Viscoat 295 (as: SR351, EM231, SR454, EM2380, SR9035, EM2382), tetramethylolmethane three/tetraacrylate (as: SR444, EM235), Dipentaerythritol four/five/six acrylate (as: SR399, EM265).
Preferably, described light trigger is bitter almond oil camphor, benzoin alkylether, acetophenones light trigger, Anthraquinones light trigger, thioxanthone photoinitiator, ketal photoinitiator, organo-peroxide, mercaptan compound, Organohalogen compounds, Benzophenones light trigger, 2, 4, 6-trimethylbenzoyl diphenylphosphine oxide compound, two [2, the fluoro-3-of 6-bis-(1H-pyrryl-1) phenyl] titanium luxuriant (Irgacure784), two (pentafluorophenyl group) titanium is luxuriant, anthraquinone/tertiary amine light initiation system, camphorquinone (claiming again camphane spinach ketone CQ)/tertiary amine light initiation system, 3-ketone group tonka bean camphor/tertiary amine light initiation system, 2-methyl isophthalic acid-[4-(methyl sulfo-) phenyl]-2-morpholinyl acetone-1, one or more in 2-benzyl-2-dimethyl amido-1-(4-morpholinyl phenyl)-butane-1-ketone.
Preferably; described light trigger is 1-hydroxy-cyclohexyl phenyl ketone (as: Irgacure184), 2-hydroxy-2-methyl-1-phenyl-1-acetone (as: Darocur1173), 2; 4; 6-trimethylbenzoyl-diphenyl phosphine oxide (as: Darocur TPO), phenyl two (2; 4,6-trimethylbenzoyl) one or more in phosphine oxide (as: Irgacure819), st-yrax methyl-phenoxide (as: Irgacure651).
Preferably, described auxiliary agent comprises one or more the mixing in flow agent, defoamer, stopper, light-initiated auxiliary agent.
Preferably, described auxiliary agent is the silane containing acrylic-functional.As: tego2100, tego2300, tego2700 and the BYK371 of TEGO RAD series, one or more in BYK3530.
Compared with prior art, the present invention has following beneficial effect:
1, UV photocuring transfer printing glue composition coating is easier to template separation, is conducive to the base material of the specific lines of made.;
2, coating good film-forming property, ageing resistance is good;
3, the yield rate of filming is high, is beneficial to and enhances productivity;
When 4, UV solidifies, temperature is low, and base material can temperature distortion;
5, reduce solvent discharge, be conducive to environment protection.
Embodiment
Below in conjunction with specific embodiment, the present invention is described in detail.Following examples will contribute to those skilled in the art further to understand the present invention, but not limit in any form the present invention.It should be pointed out that to those skilled in the art, without departing from the inventive concept of the premise, can also make some distortion and improvement.These all belong to protection scope of the present invention.
comparative example 1～3
This comparative example provides a kind of UV cure coating compositions, and its preparation method comprises the steps:
(a) according to the component shown in table 1 and parts by weight, get the raw materials ready;
(b) described feed composition is mixed, middling speed is disperseed 2 hours, filters, and obtains a kind of UV curing transfer glue composition.
embodiment 1～7
Embodiment 1～7 provides respectively a kind of UV curing transfer glue composition, and feed composition and parts by weight that each composition is corresponding are as shown in table 1;
Respectively feed composition corresponding to each embodiment mixed by its parts by weight, middling speed is disperseed 2 hours, filters, and obtains corresponding a kind of UV curing transfer glue composition.
Table 1
embodiment 8, application
The application of the UV photocuring transfer printing glue composition of above-described embodiment 1～7 comprises following concrete steps:
1, coating process
UV photocuring transfer printing glue composition is gone up to the requirement of machine viscosity, glue spread, Painting effect according to coating, adopt certain coating method that UV photocuring transfer printing glue composition is coated on base material (PC, PMMA, PET or TPU etc.) equably, concrete coating method has dotting glue method, stencil, rolling method, spread coating etc., by adjusting the processing parameter of coating method, guarantee that UV photocuring transfer printing glue composition is uniformly coated on base material (PC, PMMA, PET or TPU etc.);
2, mould pressing process
The processing parameters such as the temperature while controlling mold pressing well, pressure, speed, adjust the energy of UV curing light source, guarantee speed and the effect of UV mould pressing process;
3, releasing process
Rolling method production process is line-connection type, after mold pressing illumination curing, is the demoulding, dotting glue method, stencil, spread coating be between breaking process, after illumination curing, need manual or mechanical mode by UV photocuring transfer printing glue composition coating and mould separated demolding;
4, subsequent technique
The base material of carrying out coating lines is printed, plates medium, the subsequent technique such as die-cut according to demand.
In sum, the present invention adopts the coating layer of the UV photocuring transfer printing glue composition of the template mold pressing that has specific lines, and mold pressing simultaneously UV illumination curing is transferred in the specific lines of template on the coating layer of UV photocuring transfer printing glue composition.
embodiment 9, Performance Detection
For the coating of the present invention and prior art compares, be coated with in the following method, measure planeness, sticking power, the fastness of aluminizing, specimen page outward appearance, the heatproof of coating.
One, sticking power
With spread coating, coating is coated on the PET film that pre-treatment is good, while solidifying, the pattern of mold pressing version is compressed on to coating.Adopt adhesive tape method to test specimen page sticking power.
Appraisal procedure: do not come off for excellent completely, have and come off on a small quantity for good, come off in a large number for poor.
Two, water boiling resistance
Specimen page is put into 100 ℃ of boiling water, boil 10min.
Appraisal procedure: edge is without cracking, coating without turn white by.
Three, hardness
Making thickness is the thick sample of 20 μ m ± 2 μ m, sample is placed on the table top of a smooth level, and with MITSUBISHI UNI hardness pencil, loading 500g tests on filming.
Appraisal procedure: certain pencil of take can not scratch, scratch paint film as judging criterion, and this test pencil hardness is hardness of paint film.
Four, abrasion performance
To test specimen page (thickness is that 20 μ m ± 2 μ m are thick) and be placed on horizontal table top, with 175g loading, by friction head, paper tape will be pressed in to friction layer surface.
Appraisal procedure: roll 150 back and forth not bottom drain be qualified.
Five, humiture circulation
Specimen page is put into humiture circulating box
Incubator arranges+25 ℃/50%R.H. (2hr) → circulation (2hr) →-20 ℃/No R.H. (12hr) → circulation (4hr) →+43/80%R.H. (12hr) → circulation (3hr) →+65 ℃/20%R.H. (12hr) → circulation (2hr)=1 cycle.
Be more than one-period, repeat 3 times.
Appraisal procedure: specimen page is without blushing, and sticking power is without considerable change.
Six, thermal shock
A specimen page is put into thermal shock test chamber, first under 65 ℃ of high temperature, keep 2h, be switched under-40 ℃ of low temperature in 5min and keep 2h, do altogether 10 circulations.
Appraisal procedure: can not have cracking, peeling after test.
Performance test results to the UV Photocurable composition of the UV photocuring transfer printing glue composition of above embodiment 1～7 and comparative example 1～3 is as shown in table 2:
Table 2 Performance Detection situation
The over-all properties of the UV curing transfer glue composition that as shown in Table 2, embodiment 3,4,5 makes is better than embodiment 1,2; The over-all properties of the UV curing transfer glue composition that embodiment 6,7 makes is slightly lower than embodiment 1,2, far above comparative example 1,2,3.Analyze known: comparing embodiment 1～5 is known with embodiment 6,7, and the composite ratio of simple function, difunctionality, polyfunctional acrylic ester is (2～3): (1.5～2):, composition of the present invention all has good over-all properties at 1 o'clock; Further comparing embodiment 3,4,5 and embodiment 1,2 are known, at photo polymerization monomer compound proportion, meet (2～3): (1.5～2): the in the situation that of 1, there is more excellent scheme in the consumption of each component: light-cured resin 45～65 weight parts, photo polymerization monomer 30～50 weight parts, light trigger weight part 2～4, auxiliary agent 1～3 weight part; The comprehensive comparison of the UV curing transfer glue composition further making by embodiment 5,6,7 and comparative example 1,2,3 again can be clear and definite: when photo polymerization monomer is the compound of monofunctional acrylate, bifunctional acrylate, polyfunctional acrylic ester, the over-all properties of composition has obtained significant raising.In photo polymerization monomer of the present invention, high, the curing volumetric shrinkage of monofunctional acrylate transformation efficiency is low, snappiness good, can improve the sticking power of formulation for coating material to base material, and the low dilution capacity of viscosity is strong; Bifunctional acrylate's volatility is little, smell is low, still has better dilution capacity; Polyfunctional acrylic ester laser curing velocity is fast, solidified coating hardness is high, but viscosity is slightly large, and dilution effect is poor; When take weight ratio as (2～3): (1.5～2): 1 when composite, and three acts synergistically, take into account the hardness of UV curing speed and coating and pliable and tough, thereby strengthened the performance such as sticking power, abrasion performance, cold-hot impact of system of the present invention; Make UV curing transfer glue composition of the present invention outstanding in aspect performances such as sticking power, water boiling resistance, abrasion performances, humiture circulation, thermal shock have greatly improved, and have significantly promoted finished product rate.
Above specific embodiments of the invention are described.It will be appreciated that, the present invention is not limited to above-mentioned particular implementation, and those skilled in the art can make various distortion or modification within the scope of the claims, and this does not affect flesh and blood of the present invention.
Claims (10)
1. a UV photocuring transfer printing glue composition, is characterized in that, comprises each component of following parts by weight:
2. UV photocuring transfer printing glue composition according to claim 1, is characterized in that, comprises each component of following parts by weight:
3. UV photocuring transfer printing glue composition according to claim 1 and 2, is characterized in that, described light-cured resin is one or more in epoxy acrylic resin, Polyurethane acrylic resin, polyester acrylic resin, pure the third resin.
4. UV photocuring transfer printing glue composition according to claim 1 and 2, is characterized in that, described photo polymerization monomer is one or more in monofunctional acrylate, bifunctional acrylate, polyfunctional acrylic ester.
5. UV photocuring transfer printing glue composition according to claim 4, it is characterized in that, described photo polymerization monomer is that weight ratio is (2～3): (1.5～2): the compound of 1 monofunctional acrylate, bifunctional acrylate, polyfunctional acrylic ester.
6. UV photocuring transfer printing glue composition according to claim 4, it is characterized in that, described monofunctional acrylate is one or more in Hydroxyethyl acrylate, Propylene glycol monoacrylate, 2-phenoxyethyl acrylate, lauric acid acrylate, isodecyl acrylate, iso-bornyl acrylate, benzyl acrylate, tetrahydrofurfuryl acrylate; Described bifunctional acrylate is one or more in 1,6 hexanediol diacrylate, tripropylene glycol diacrylate, propylene glycol diacrylate, neopentylglycol diacrylate, ethoxyquin bisphenol a diacrylate, tristane dimethanol diacrylate; Described polyfunctional acrylic ester is one or more in ethoxyquin trimethylolpropane trimethacrylate, tetramethylolmethane three/tetraacrylate, Dipentaerythritol four/five/six acrylate.
7. UV photocuring transfer printing glue composition according to claim 1 and 2, it is characterized in that, described light trigger is bitter almond oil camphor, benzoin alkylether, acetophenones light trigger, Anthraquinones light trigger, thioxanthone photoinitiator, ketal photoinitiator, organo-peroxide, mercaptan compound, Organohalogen compounds, Benzophenones light trigger, 2, 4, 6-trimethylbenzoyl diphenylphosphine oxide compound, two [2, the fluoro-3-of 6-bis-(1H-pyrryl-1) phenyl] titanium is luxuriant, two (pentafluorophenyl group) titanium is luxuriant, anthraquinone/tertiary amine light initiation system, camphorquinone/tertiary amine light initiation system, 3-ketone group tonka bean camphor/tertiary amine light initiation system, 2-methyl isophthalic acid-[4-(methyl sulfo-) phenyl]-2-morpholinyl acetone-1, the mixing of one or more in 2-benzyl-2-dimethyl amido-1-(4-morpholinyl phenyl)-butane-1-ketone.
8. UV photocuring transfer printing glue composition according to claim 7; it is characterized in that; described light trigger is 1-hydroxy-cyclohexyl phenyl ketone, 2-hydroxy-2-methyl-1-phenyl-1-acetone, 2; 4; 6-trimethylbenzoyl-diphenyl phosphine oxide, phenyl two (2; 4,6-trimethylbenzoyl) one or more in phosphine oxide, st-yrax methyl-phenoxide.
9. UV transfer printing glue composition according to claim 1 and 2, is characterized in that, described auxiliary agent is one or more in flow agent, defoamer, stopper, light-initiated auxiliary agent.
10. UV transfer printing glue composition according to claim 9, is characterized in that, described light-initiated auxiliary agent is the silane containing acrylic-functional.
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| CN103923470B (en) * | 2014-04-01 | 2015-11-25 | 江苏科技大学 | A kind of bio-based degradation material printed for 3D |
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| CN104592796A (en) * | 2014-12-26 | 2015-05-06 | 上海维凯光电新材料有限公司 | Vacuum aluminum plating transferring ultraviolet-curable coating |
| CN105045039A (en) * | 2015-08-04 | 2015-11-11 | 上海维凯光电新材料有限公司 | Ultraviolet (UV) make-up adhesive composition and application thereof |
| CN105038392A (en) * | 2015-08-04 | 2015-11-11 | 上海乘鹰新材料有限公司 | UV reprinting coating composition and application thereof |
| CN105733389A (en) * | 2016-04-13 | 2016-07-06 | 湖南省金海科技有限公司 | LED-UV-cured transfer printing adhesive and preparation method thereof |
| CN106046927A (en) * | 2016-07-12 | 2016-10-26 | 昆山市曙光照明器材有限公司 | Hydrographic transfer printing ink and preparation method thereof |
| CN106189425B (en) * | 2016-08-11 | 2018-07-10 | 河北智生环保科技有限公司 | A kind of photocuring cold forming transfer coatings, preparation method and application |
| CN106189425A (en) * | 2016-08-11 | 2016-12-07 | 河北智生环保科技有限公司 | A kind of photocuring cold forming transfer coatings, its preparation method and application |
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