CN103536495A - Preparation method of grape seed procyanidin sun cream - Google Patents
Preparation method of grape seed procyanidin sun cream Download PDFInfo
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- CN103536495A CN103536495A CN201310514745.5A CN201310514745A CN103536495A CN 103536495 A CN103536495 A CN 103536495A CN 201310514745 A CN201310514745 A CN 201310514745A CN 103536495 A CN103536495 A CN 103536495A
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- vitis viniferae
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Abstract
The invention relates to the technical field of cosmetics, and specifically relates to a preparation method of grape seed procyanidin sun cream. Aiming at the characteristic of a plant sun cream, namely a grape seed procyanidin extract, the biological activity of procyanidin as an effective component is maintained to the maximum extent by adopting appropriate adding forms and adding methods. The technical scheme adopted by the invention comprises the following operational steps: I, screening grape brewing dregs, separating and sorting grape seeds with qualified quality, and crushing and degreasing to obtain grape seed degreased powder; II, preparing the grape seed procyanidin extract; III, preparing the sun cream; IV, packaging.
Description
One, technical field:
The present invention relates to cosmetics technical field, be specifically related to a kind of preparation method of grape pip procyanidin sunscreen cream.
Two, background technology:
Procyanidin has absworption peak ， 290-320nmUVB district to have good ultraviolet absorption ability at 280nm, and its antioxidant effect is V
c20 times, V
e50 times.Procyanidin can be by removing the effect performance beauty and health care functions such as free radical, antioxidation, radioprotective.So procyanidin is the natural plant sun agent of highly effective and safe.In recent years, China's wine industry presents good development momentum, and output continues to increase, and along with the increase of vintage, the by-product of vinify is also increasing year by year.The seed-producing rate of Fructus Vitis viniferae is 8%～10%, contain a large amount of aldehydes matters in Semen Vitis viniferae, and its content accounts for 50%～70% of grape fruit phenols.Wherein procyanidin accounts for 88%～90%, and the Semen Vitis viniferae of therefore usining is originated and had great economy, society, environmental benefit as the extraction of procyanidin.
The procyanidin extract that sell domestic and international market at present, conventional extractant has acetone, methanol, ethyl acetate, ethanol etc., and wherein acetone and methanol are because the high frequency of utilization of extraction ratio is high.In whole production process, will use multiple organic solvent, and the consumption of organic solvent is large, is difficult for reclaiming, contaminated environment, harmful human body organic solvent is easily residual; Operation is many, technique very complicated; Need repeatedly distill, heat time heating time is long, and procyanidin is oxidizable.And the sunscreen of preparing for cosmetics must be selected safety to extract medium and extract, to guarantee the complete noresidue of organic solvent of harmful human body in product.
At present the conventional sunscreen of cosmetic field or take the chemical sunscreen such as ethylhexyl methoxy cinnamate as main, during preparation, conventionally using sunscreen as oil phase or one of the component of water, be mixed and heated to 75 ℃～90 ℃.The feature that traditional handicraft is not easily decomposed and is oxidized for active components of plants high temperature.While preparing the sunscreen cream that contains procyanidin, on the basis of traditional handicraft, also to consider the maintenance of the effectiveness of active components of plants, procyanidin extract adds rear emulsion particle diameter size, the factors such as emulsion droplet form and distribution, 75～90 ℃ of high temperature can not be heated to, the suitable mode that adds should be selected.
The preparation method of tradition sunscreen cream is rule of thumb determined homogenizing rotating speed, and time and cooling procedure are accurate not, and the preparation that is only applicable to the formulation product that tradition contains chemical sunscreen is produced.Can not be able to not effectively control the size of product, cannot effectively guarantee being uniformly distributed and the emulsion droplet of formation rule form of procyanidin extract, be unfavorable for the stable performance of procyanidin sun-screening function.
Three, summary of the invention:
The present invention, in order to solve the weak point in above-mentioned background technology, provides a kind of special in usining the preparation method of grape pip procyanidin extract as the sunscreen cream of sunscreen.
For achieving the above object, the technical solution used in the present invention is: a kind of preparation method of grape pip procyanidin sunscreen cream, it is characterized in that: comprise following operating procedure: 1. sieve vinify skin slag, after the Semen Vitis viniferae separated, sort out is up-to-standard, pulverize defat and obtain Semen Vitis viniferae skimmed milk; 2. the preparation of grape pip procyanidin extract; 3. the preparation of sunscreen cream; 4. pack.
Described step is 1.: screening from wine brewing skin slag, sort out Semen Vitis viniferae, in screening process, reject the Semen Vitis viniferae raw material of moldy metamorphism, Semen Vitis viniferae raw material after screening is preserved in dry ventilation, Semen Vitis viniferae raw material is pulverized through plant pulverizer, cross 60～80 mesh sieves, after defat, the temperature of-20 ℃, preserve dried Semen Vitis viniferae skimmed milk.
Described step is 2.: adopt quick solvent extraction, the ethanol of usining extracts procyanidin as solvent in Semen Vitis viniferae skimmed milk, and extraction time 10～14min extracts pressure 1100～1200psi, extract 60～70 ℃ of temperature, the volume fraction of described ethanol is 70%～80%.
Described step is 3.: by oil phase Oleum Vitis viniferae, white vaseline, lanoline, stearic acid, hexadecanol, octadecanol and emulsifier tween-80, glyceryl monostearate mixes as A phase, be heated to 75～85 ℃, by deionized water, glycerol, 18% sodium hydroxide solution, EDETATE SODIUM, methyl hydroxybenzoate, this propyl formate of hydroxyl is as B phase, be heated to 85～90 ℃, A be added to B mutually in, carry out homogenizing, rotating speed 1000～3000r/min, homogenizing time 4～6min, when temperature falls after rise to 40 ℃～45 ℃, procyanidin extract is dissolved in to 30% ethanol/water solution as C phase, add A, in the mixture of B phase.Under room temperature, carry out temperature-fall period, discharging.Can obtain particle diameter is the uniform and stable cream frost of 9.481～22.191 μ m.
4. described step packs.Choose the opaque plastics or the packing container that meet the requirement of QB1685-2006 cosmetic product packaging external appearance and carry out aseptic packaging.
Compared with prior art, the present invention has advantage and effect are as follows:
1, compared to common sunscreen cream, add chemical sunscreen, this preparation method is through the recycling of wine brewing garbage Semen Vitis viniferae, and the ethanol of usining extracts solvent as safety, can obtain plant sun agent, thereby prepares sunscreen cream safe, effective, natural, environmental protection.
2, for the characteristic of plant sun agent grape pip procyanidin extract, adopt suitable adding form and add method, kept to the full extent the biological activity of procyanidin as effective ingredient.
3, through experiment of single factor and Response Surface Method, optimize preparation technology, determined the homogenizing temperature of preparing for grape pip procyanidin sunscreen cream, homogenizing time, homogenizing rotating speed and the type of cooling.Obtained procyanidin and be evenly distributed, emulsion droplet regular shape, the cream frost that particle size distribution is even, stable, be conducive to the stable performance of product efficacy.
4, according to the evaluation methodology of GB QB-T 2410-1998 sun care preparations UVB district sun-proof result, record sample absorbance 1.1～1.5, effect is medium protection ultraviolet light effect, and service condition is moderate strength sun exposure.
Four, the specific embodiment:
The concrete implementation step of the present invention is as follows:
1, screening vinify skin slag, screening from wine brewing skin slag, sort out full seed, without moldy metamorphism Semen Vitis viniferae, save backup in dry ventilation after clean the drying of Semen Vitis viniferae raw material after screening.Semen Vitis viniferae raw material is pulverized through plant pulverizer, crosses 60～80 mesh sieves, after defat, and, the temperature of-20 ℃, preserve dried Semen Vitis viniferae skimmed milk.
2, the preparation of plant sun agent-grape pip procyanidin extract.Adopt quick solvent extraction, using ethanol as solvent extraction procyanidin, extraction time 10～14min, extracts pressure 1100～1200psi, extracts 60～70 ℃ of temperature, volume fraction of ethanol 70%～80%.
3, sunscreen cream preparation.By oil phase Oleum Vitis viniferae, white vaseline, lanoline, stearic acid, hexadecanol, octadecanol and emulsifier tween-80, glyceryl monostearate mixes as A phase, be heated to 75～85 ℃, by deionized water, glycerol, mass fraction is 18% sodium hydroxide solution, EDETATE SODIUM, methyl hydroxybenzoate, this propyl formate of hydroxyl is as B phase, be heated to 85～90 ℃, A be added to B mutually in, carry out homogenizing, rotating speed 1000～3000r/min, homogenizing time 4～6min, when temperature falls after rise to 40 ℃～45 ℃, procyanidin extract is dissolved in to 30% ethanol/water solution as C phase, add A, in the mixture of B phase.Under room temperature, carry out temperature-fall period, discharging, can obtain particle diameter is the uniform and stable cream frost of 9.481～22.191 μ m.
4, sun-proof result evaluation methodology.Evaluation methodology according to GB QB-T 2410-1998 sun care preparations UVB district sun-proof result, records sample absorbance 1.1～1.5, and effect is medium protection ultraviolet light effect, and service condition is moderate strength sun exposure.
5, packing.Choose the opaque plastics or the other materials packing container that meet the requirement of QB1685-2006 cosmetic product packaging external appearance and carry out aseptic packaging.
Claims (8)
1. a preparation method for grape pip procyanidin sunscreen cream, is characterized in that: comprise following operating procedure: 1. sieve vinify skin slag, after the Semen Vitis viniferae separated, sort out is up-to-standard, pulverize defat and obtain Semen Vitis viniferae skimmed milk; 2. the preparation of grape pip procyanidin extract; 3. the preparation of sunscreen cream; 4. pack.
2. the preparation method of a kind of grape pip procyanidin sunscreen cream according to claim 1, it is characterized in that: described step 1.: screening from wine brewing skin slag, sort out Semen Vitis viniferae, in screening process, reject the Semen Vitis viniferae raw material of moldy metamorphism, Semen Vitis viniferae raw material after screening is preserved in dry ventilation, Semen Vitis viniferae raw material is pulverized through plant pulverizer, cross 60～80 mesh sieves, after defat, the temperature of-20 ℃, preserve dried Semen Vitis viniferae skimmed milk.
3. the preparation method of a kind of grape pip procyanidin sunscreen cream according to claim 1 and 2, it is characterized in that: described step 2.: adopt quick solvent extraction, the ethanol of usining extracts procyanidin as solvent in Semen Vitis viniferae skimmed milk, extraction time 10～14min, extract pressure 1100～1200psi, extract 60～70 ℃ of temperature, the volume fraction of described ethanol is 70%～80%.
4. the preparation method of a kind of grape pip procyanidin sunscreen cream according to claim 3, it is characterized in that: described step 3.: by oil phase Oleum Vitis viniferae, white vaseline, lanoline, stearic acid, hexadecanol, octadecanol and emulsifier tween-80, glyceryl monostearate mixes as A phase, be heated to 75～85 ℃, by deionized water, glycerol, 18% sodium hydroxide solution, EDETATE SODIUM, methyl hydroxybenzoate, this propyl formate of hydroxyl is as B phase, be heated to 85～90 ℃, A be added to B mutually in, carry out homogenizing, rotating speed 1000～3000r/min, homogenizing time 4～6min, when temperature falls after rise to 40 ℃～45 ℃, procyanidin extract is dissolved in to 30% ethanol/water solution as C phase, add A, in the mixture of B phase.
5. under room temperature, carry out temperature-fall period, discharging.
6. can obtain particle diameter is the uniform and stable cream frost of 9.481～22.191 μ m.
7. the preparation method of a kind of grape pip procyanidin sunscreen cream according to claim 4, is characterized in that: 4. described step packs.
8. choose the opaque plastics or the packing container that meet the requirement of QB1685-2006 cosmetic product packaging external appearance and carry out aseptic packaging.
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105106039A (en) * | 2015-09-17 | 2015-12-02 | 南京林业大学 | Method for preparing proanthocyanidin whitening sunscreen cream |
| CN105342892A (en) * | 2015-12-09 | 2016-02-24 | 武汉科技大学 | Pyracantha fortuneana fruit procyanidine cream and preparing method thereof |
| CN108936151A (en) * | 2018-06-04 | 2018-12-07 | 天津商业大学 | A kind of compound antianxiety sleeping drink of black fruit fructus lycii and preparation method thereof |
| CN113101247A (en) * | 2021-04-19 | 2021-07-13 | 广东丸美生物技术股份有限公司 | Blueberry anthocyanin sunscreen composition, sunscreen mud cream and preparation method thereof |
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| CN103239384A (en) * | 2013-04-25 | 2013-08-14 | 新疆大学 | Grape seed compounded horse oil skin care product and preparation method thereof |
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| CN103239384A (en) * | 2013-04-25 | 2013-08-14 | 新疆大学 | Grape seed compounded horse oil skin care product and preparation method thereof |
Non-Patent Citations (2)
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| 姜守霞 等: "《葡萄籽中提取原花青素的研究》", 《应用化工》 * |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105106039A (en) * | 2015-09-17 | 2015-12-02 | 南京林业大学 | Method for preparing proanthocyanidin whitening sunscreen cream |
| CN105106039B (en) * | 2015-09-17 | 2019-03-19 | 南京林业大学 | A kind of preparation method of proanthocyanidin Whitening sunscreen cream |
| CN105342892A (en) * | 2015-12-09 | 2016-02-24 | 武汉科技大学 | Pyracantha fortuneana fruit procyanidine cream and preparing method thereof |
| CN108936151A (en) * | 2018-06-04 | 2018-12-07 | 天津商业大学 | A kind of compound antianxiety sleeping drink of black fruit fructus lycii and preparation method thereof |
| CN113101247A (en) * | 2021-04-19 | 2021-07-13 | 广东丸美生物技术股份有限公司 | Blueberry anthocyanin sunscreen composition, sunscreen mud cream and preparation method thereof |
| CN113101247B (en) * | 2021-04-19 | 2022-09-23 | 广东丸美生物技术股份有限公司 | Blueberry anthocyanin sunscreen composition, sunscreen mud cream and preparation method thereof |
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| CN103536495B (en) | 2015-08-26 |
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Effective date of registration: 20200210 Address after: 016000 Saihan Usu Ecological Park, Hainan District, Wuhai City, Inner Mongolia Autonomous Region Patentee after: Inner Mongolia Sunshine Tianyu Grape Wine Co., Ltd. Address before: 712100 Yangling demonstration area, Xi'an agricultural college, Northwest Agriculture and Forestry University, Shaanxi, China Patentee before: NORTHWEST A & F University |
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