CN103239384A - Grape seed compounded horse oil skin care product and preparation method thereof - Google Patents
Grape seed compounded horse oil skin care product and preparation method thereof Download PDFInfo
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- CN103239384A CN103239384A CN2013101485522A CN201310148552A CN103239384A CN 103239384 A CN103239384 A CN 103239384A CN 2013101485522 A CN2013101485522 A CN 2013101485522A CN 201310148552 A CN201310148552 A CN 201310148552A CN 103239384 A CN103239384 A CN 103239384A
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Abstract
The invention relates to the technical field of natural skin care products and production methods thereof, and more particularly relates to a grape seed compounded horse oil skin care product and a preparation method thereof. The grape seed compounded horse oil skin care product comprises the following raw materials in percentage by weight: 10%-13% of grape seed oil, 5%-7% of horse oil, 2%-3% of glyceryl monostearate, 0.5%-2% of hexadecanol, 8%-10% of glycerol, 1%-3% of triethanolamine, 1%-3% of tween-80, 0.2%-0.5% of xanthan gum, 0.2%-0.5% of grape seed procyanidine and 0.2%-0.3% of essence. The production method provided by the invention is simple and convenient in process and a safe and high-quality natural skin care product suitable for industrial production; and as the grape seed oil and the horse oil are taken as raw materials, the grape seed compounded horse oil skin care product has the advantages of moisturizing and smoothing skin, enabling skin to have high resilience, delaying senescence and preventing formation of acnes, freckles and the like.
Description
Technical field
the present invention relates to natural skin care product and production method technical field thereof, is compound house oil skin care item of a kind of Semen Vitis viniferae and preparation method thereof.
Background technology
the raw material that in current skin care field, skin care item are used mostly is chemical reagent, and skin and human body are had to a lot of side effect, while exceeding standard as the lead in skin care product additive, hydrargyrum, can cause skin to produce mottle, can cause the diseases such as renal failure when serious.
fructus Vitis viniferae is the higher planting fruit-trees of economic worth in the world, has another name called single Herba Tubocapsici Anomali, mountain calabash, Jambul, for Vitaceae (
vitaceae) Vitis (
vitis) plant.Oleum Vitis viniferae contains multiple unsaturated fatty acid, vitamin E and various trace element, and wherein linoleic acid has the hypertension of control, arteriosclerosis, cardiopathic function, and reduction human serum cholesterol and vegetative nervous function imbalance are had to obvious curative effect; Various fat-soluble, water soluble vitamins and various trace elements, to the acute and chronic avitaminosis, particularly have specially good effect to old man, child, weak women, anemia of pregnant woman.The application that Oleum Vitis viniferae has all had in food, cosmetics and medical industry.
house oil is all goodr to affinity and its spread-coating of skin, especially to senile plaque, wrinkle, alopecia, headache, flu, asthma, allergic rhinitis, pollinosis, eczema, scald, tinea pedis, pachylosis, atopic dermatitis, disgrace skin ulcer, constipation, hemorrhoid, hold the diseases such as pus disease, dysmenorrhoea curative effect in various degree arranged.
Summary of the invention
the invention provides compound house oil skin care item of a kind of Semen Vitis viniferae and preparation method thereof, overcome the deficiency of above-mentioned prior art, it can effectively solve current many cosmetics and take the problem that chemical reagent is raw material.
one of technical scheme of the present invention realizes by following measures: the compound house oil skin care item of a kind of Semen Vitis viniferae, and raw material is the percent meter by weight: Oleum Vitis viniferae is 10% to 13%, house oil is 5% to 7%, glyceryl monostearate is 2% to 3%, hexadecanol is 0.5% to 2%, glycerol is 8% to 10%, triethanolamine is 1% to 3%, tween 80 is 1% to 3%, xanthan gum is 0.2% to 0.5%, grape pip procyanidin is 0.2% to 0.5%, essence is 0.2% to 0.3%, antiseptic is 0.2% to 0.3% and the deionized water of surplus; Wherein the compound house oil skin care item of this Semen Vitis viniferae obtain as follows: the first step is dissolve under 80 ℃ to 90 ℃ conditions and be mixed into oil phase in temperature after Oleum Vitis viniferae, house oil, glyceryl monostearate and hexadecanol are mixed; Second step is dissolve under 80 ℃ to 90 ℃ conditions and be mixed into water in temperature after glycerol, triethanolamine, tween 80, xanthan gum, grape pip procyanidin and deionized water are mixed; The 3rd step, be, under 80 ℃ to 90 ℃ conditions, oil phase is added to water in temperature, and be that under 800r/min to 1000r/min condition, emulsifying 30min to 60min obtains emulsion in stir speed (S.S.); The 4th step after emulsion is cooled to 40 ℃ to 45 ℃, obtains the compound house oil skin care item of Semen Vitis viniferae after adding essence and antiseptic mix homogeneously in emulsion.
two of technical scheme of the present invention realizes by following measures: the preparation method of the compound house oil skin care item of a kind of Semen Vitis viniferae, and raw material is the percent meter by weight: Oleum Vitis viniferae is 10% to 13%, house oil is 5% to 7%, glyceryl monostearate is 2% to 3%, hexadecanol is 0.5% to 2%, glycerol is 8% to 10%, triethanolamine is 1% to 3%, tween 80 is 1% to 3%, xanthan gum is 0.2% to 0.5%, grape pip procyanidin is 0.2% to 0.5%, essence is 0.2% to 0.3%, antiseptic is 0.2% to 0.3% and the deionized water of surplus; Wherein the compound house oil skin care item of this Semen Vitis viniferae are undertaken by following preparation method: the first step is dissolve under 80 ℃ to 90 ℃ conditions and be mixed into oil phase in temperature after Oleum Vitis viniferae, house oil, glyceryl monostearate and hexadecanol are mixed; Second step is dissolve under 80 ℃ to 90 ℃ conditions and be mixed into water in temperature after glycerol, triethanolamine, tween 80, xanthan gum, grape pip procyanidin and deionized water are mixed; The 3rd step, be, under 80 ℃ to 90 ℃ conditions, oil phase is added to water in temperature, and be that under 800r/min to 1000r/min condition, emulsifying 30min to 60min obtains emulsion in stir speed (S.S.); The 4th step after emulsion is cooled to 40 ℃ to 45 ℃, obtains the compound house oil skin care item of Semen Vitis viniferae after adding essence and antiseptic mix homogeneously in emulsion.
below the further optimization and/or improvements to the foregoing invention technical scheme:
the above-mentioned meter of percent by weight, Oleum Vitis viniferae is 12%, house oil is 5.5%, glyceryl monostearate is 2.9%, hexadecanol is 1.5%, glycerol is 9%, triethanolamine is 1.2%, tween 80 is 1.9%, xanthan gum is 0.3%, grape pip procyanidin is 0.2%, essence is 0.2%, antiseptic is 0.2%.
above-mentioned is under 300r/min to 600r/min condition, emulsion to be cooled to 40 ℃ to 45 ℃ in stir speed (S.S.).
foregoing preservatives is potassium sorbate.
production technology of the present invention is simple and convenient, is a kind of natural skin care product that are applicable to industrial safe and high quality, and adopting Oleum Vitis viniferae and house oil is raw material, can make sliding tender, the high resilience of skin moisturizing, slow down aging, and play the formation that prevents acne and freckle etc.
The accompanying drawing explanation
fig. 1 is for being used the skin care item that obtain according to the embodiment of the present invention and the guarantor's moisture curve that uses basic skin care item, experimental group is for being used guarantor's moisture curve of the skin care item that obtain according to the above embodiment of the present invention, and matched group is for being used guarantor's moisture curve of basic skin care item.
The specific embodiment
the present invention is not subject to the restriction of following embodiment, can determine concrete embodiment according to technical scheme of the present invention and practical situation.
below in conjunction with embodiment, the invention will be further described:
embodiment 1, the compound house oil skin care item of this Semen Vitis viniferae, raw material is the percent meter by weight: Oleum Vitis viniferae is 10% to 13%, house oil is 5% to 7%, glyceryl monostearate is 2% to 3%, hexadecanol is 0.5% to 2%, glycerol is 8% to 10%, triethanolamine is 1% to 3%, tween 80 is 1% to 3%, xanthan gum is 0.2% to 0.5%, grape pip procyanidin is 0.2% to 0.5%, essence is 0.2% to 0.3%, antiseptic is 0.2% to 0.3% and the deionized water of surplus; Wherein the compound house oil skin care item of this Semen Vitis viniferae obtain by following preparation method: the first step is dissolve under 80 ℃ to 90 ℃ conditions and be mixed into oil phase in temperature after Oleum Vitis viniferae, house oil, glyceryl monostearate and hexadecanol are mixed; Second step is dissolve under 80 ℃ to 90 ℃ conditions and be mixed into water in temperature after glycerol, triethanolamine, tween 80, xanthan gum, grape pip procyanidin and deionized water are mixed; The 3rd step, be, under 80 ℃ to 90 ℃ conditions, oil phase is added to water in temperature, and be that under 800r/min to 1000r/min condition, emulsifying 30min to 60min obtains emulsion in stir speed (S.S.); The 4th step after emulsion is cooled to 40 ℃ to 45 ℃, obtains the compound house oil skin care item of Semen Vitis viniferae after adding essence and antiseptic mix homogeneously in emulsion.Adopting Oleum Vitis viniferae and house oil after refining is raw material, can make sliding tender, the high resilience of skin moisturizing, slow down aging, and play the formation that prevents acne and freckle etc.
embodiment 2, the compound house oil skin care item of this Semen Vitis viniferae, raw material is the percent meter by weight: Oleum Vitis viniferae is 10% or 13%, house oil is 5% or 7%, glyceryl monostearate is 2% or 3%, hexadecanol is 0.5% or 2%, glycerol is 8% or 10%, triethanolamine is 1% or 3%, tween 80 is 1% or 3%, xanthan gum is 0.2% or 0.5%, grape pip procyanidin is 0.2% or 0.5%, essence is 0.2% or 0.3%, antiseptic is 0.2% or 0.3% and the deionized water of surplus; Wherein the compound house oil skin care item of this Semen Vitis viniferae obtain by following preparation method: the first step, and dissolve under temperature is 80 ℃ or 90 ℃ of conditions after Oleum Vitis viniferae, house oil, glyceryl monostearate and hexadecanol are mixed and be mixed into oil phase; Second step dissolves after glycerol, triethanolamine, tween 80, xanthan gum, grape pip procyanidin and deionized water are mixed and is mixed into water under temperature is 80 ℃ or 90 ℃ of conditions; The 3rd step is added to water by oil phase under temperature is 80 ℃ or 90 ℃ of conditions, and is that under 800r/min or 1000r/min condition, emulsifying 30min or 60min obtain emulsion in stir speed (S.S.); The 4th step after emulsion is cooled to 40 ℃ or 45 ℃, obtains the compound house oil skin care item of Semen Vitis viniferae after adding essence and antiseptic mix homogeneously in emulsion.
embodiment 3, as above-described embodiment preferably, percent meter by weight, Oleum Vitis viniferae is 12%, house oil is 5.5%, glyceryl monostearate is 2.9%, hexadecanol is 1.5%, glycerol is 9%, triethanolamine is 1.2%, tween 80 is 1.9%, xanthan gum is 0.3%, grape pip procyanidin is 0.2%, essence is 0.2%, antiseptic is 0.2%.
embodiment 4, with the difference of above-described embodiment, is, and in stir speed (S.S.), be under 300r/min to 600r/min condition, emulsion to be cooled to 40 ℃ to 45 ℃.Emulsion carried out cooling by stirring, to accelerate except making the emulsion cooldown rate, simultaneously, the viscosity by stirring cooled emulsion is not than good by the viscosity that stirs cooling emulsion.
embodiment 3, as above-described embodiment preferably, antiseptic is potassium sorbate.Potassium sorbate is a kind of antiseptic safely and effectively commonly used in the skin care item industry.
below experimental data and contrast effect
one, the skin care item that obtain according to the above embodiment of the present invention and the controlled trial of basic skin care item
the basis skin care item refer to the skin care item that obtain according to the above embodiment of the present invention method, but wherein neither add Oleum Vitis viniferae, also do not add house oil.
choose 20 ages in the 20-50 female volunteers in year, emulsion of the present invention is applied to a hands, the another hands is smeared basic skin care item in contrast, smear every day 2 times, totally 12 days, skin is moist has substantial connection with elasticity and epidermis contained humidity, the excessive loss of moisture of skin can cause xerosis cutis, elasticity reduces, even chap, every day, (skin was electric non-conductor by conductivity meter, when moisture content of skin increases, resistance descends, the descend bright moisturizing degree of more speaking more of resistance is better) measure the moisturizing degree of dauber's both hands, be determined at temperature 22-24 ℃, carry out the indoor of relative humidity 35-45%, (Fig. 1 is for being used the skin care item that obtain according to the above embodiment of the present invention and the guarantor's moisture curve that uses basic skin care item as shown in Figure 1 for the meansigma methods result, experimental group is for being used guarantor's moisture curve of the skin care item that obtain according to the above embodiment of the present invention, matched group is for being used guarantor's moisture curve of basic skin care item).
by upper figure, can find out: the skin care item that obtain according to the above embodiment of the present invention and basic skin care item relatively have remarkable increase skin moisture-keeping degree and elastic effect, and the skin moisture-keeping degree is effective delay skin aging speed well.
two, the skin care item that obtain according to the above embodiment of the present invention and the controlled trial that contrasts skin care item
the contrast skin care item refer to the skin care item that obtain according to the above embodiment of the present invention method, but wherein do not add house oil.
choose 20 ages in the 20-50 female volunteers (freckle as well as acne is in various degree arranged) in year, the skin care item that will obtain according to the above embodiment of the present invention and contrast skin care item first are applied to half of face after ear after allergy test, face is smeared the skin care item that obtain according to the above embodiment of the present invention method on one side, another half of face is smeared the contrast skin care item, smear every day 2 times, totally 20 days, result means to use the position of the skin care item that obtain according to the above embodiment of the present invention from the 7th day, the acne freckle starts to reduce gradually, average minimizing 40% in the 15th day, with the freckle as well as acne of decreased average 50% to the 20th day, the freckle as well as acne minimizing is not obvious to use the position that contrasts skin care item.The emulsion that hence one can see that adds house oil has the effect that reduces freckle as well as acne.
Claims (10)
1. compound house oil skin care item of Semen Vitis viniferae is characterized in that raw material percent meter by weight: Oleum Vitis viniferae is 10% to 13%, house oil is 5% to 7%, glyceryl monostearate is 2% to 3%, hexadecanol is 0.5% to 2%, glycerol is 8% to 10%, triethanolamine is 1% to 3%, tween 80 is 1% to 3%, xanthan gum is 0.2% to 0.5%, grape pip procyanidin is 0.2% to 0.5%, essence is 0.2% to 0.3%, antiseptic is 0.2% to 0.3% and the deionized water of surplus; Wherein the compound house oil skin care item of this Semen Vitis viniferae obtain as follows: the first step is dissolve under 80 ℃ to 90 ℃ conditions and be mixed into oil phase in temperature after Oleum Vitis viniferae, house oil, glyceryl monostearate and hexadecanol are mixed; Second step is dissolve under 80 ℃ to 90 ℃ conditions and be mixed into water in temperature after glycerol, triethanolamine, tween 80, xanthan gum, grape pip procyanidin and deionized water are mixed; The 3rd step, be, under 80 ℃ to 90 ℃ conditions, oil phase is added to water in temperature, and be that under 800r/min to 1000r/min condition, emulsifying 30min to 60min obtains emulsion in stir speed (S.S.); The 4th step after emulsion is cooled to 40 ℃ to 45 ℃, obtains the compound house oil skin care item of Semen Vitis viniferae after adding essence and antiseptic mix homogeneously in emulsion.
2. compound house oil skin care item of Semen Vitis viniferae according to claim 1, it is characterized in that percent meter by weight, Oleum Vitis viniferae is 12%, house oil is 5.5%, glyceryl monostearate is 2.9%, hexadecanol is 1.5%, glycerol is 9%, triethanolamine is 1.2%, tween 80 is 1.9%, xanthan gum is 0.3%, grape pip procyanidin is 0.2%, essence is 0.2%, antiseptic is 0.2%.
3. the compound house oil skin care item of Semen Vitis viniferae according to claim 1 and 2, is characterized in that in stir speed (S.S.) being under 300r/min to 600r/min condition, emulsion to be cooled to 40 ℃ to 45 ℃.
4. the compound house oil skin care item of Semen Vitis viniferae according to claim 1 and 2, is characterized in that antiseptic is potassium sorbate.
5. the compound house oil skin care item of Semen Vitis viniferae according to claim 3, is characterized in that antiseptic is potassium sorbate.
6. the preparation method of the compound house oil skin care item of Semen Vitis viniferae is characterized in that raw material percent meter by weight: Oleum Vitis viniferae is 10% to 13%, house oil is 5% to 7%, glyceryl monostearate is 2% to 3%, hexadecanol is 0.5% to 2%, glycerol is 8% to 10%, triethanolamine is 1% to 3%, tween 80 is 1% to 3%, xanthan gum is 0.2% to 0.5%, grape pip procyanidin is 0.2% to 0.5%, essence is 0.2% to 0.3%, antiseptic is 0.2% to 0.3% and the deionized water of surplus; Wherein the compound house oil skin care item of this Semen Vitis viniferae are undertaken by following preparation method: the first step is dissolve under 80 ℃ to 90 ℃ conditions and be mixed into oil phase in temperature after Oleum Vitis viniferae, house oil, glyceryl monostearate and hexadecanol are mixed; Second step is dissolve under 80 ℃ to 90 ℃ conditions and be mixed into water in temperature after glycerol, triethanolamine, tween 80, xanthan gum, grape pip procyanidin and deionized water are mixed; The 3rd step, be, under 80 ℃ to 90 ℃ conditions, oil phase is added to water in temperature, and be that under 800r/min to 1000r/min condition, emulsifying 30min to 60min obtains emulsion in stir speed (S.S.); The 4th step after emulsion is cooled to 40 ℃ to 45 ℃, obtains the compound house oil skin care item of Semen Vitis viniferae after adding essence and antiseptic mix homogeneously in emulsion.
7. the preparation method of the compound house oil skin care item of Semen Vitis viniferae according to claim 6, it is characterized in that percent meter by weight, Oleum Vitis viniferae is 12%, house oil is 5.5%, glyceryl monostearate is 2.9%, hexadecanol is 1.5%, glycerol is 9%, triethanolamine is 1.2%, tween 80 is 1.9%, xanthan gum is 0.3%, grape pip procyanidin is 0.2%, essence is 0.2%, antiseptic is 0.2%.
8. according to the preparation method of the compound house oil skin care item of the described Semen Vitis viniferae of claim 6 or 7, it is characterized in that in stir speed (S.S.) being emulsion to be cooled to 40 ℃ to 45 ℃ under 300r/min to 600r/min condition.
9. according to the preparation method of the compound house oil skin care item of the described Semen Vitis viniferae of claim 6 or 7, it is characterized in that antiseptic is potassium sorbate.
10. the preparation method of the compound house oil skin care item of Semen Vitis viniferae according to claim 8, is characterized in that antiseptic is potassium sorbate.
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| CN103520023A (en) * | 2013-10-28 | 2014-01-22 | 西北农林科技大学 | Sunscreen cream rich in grape seed oil and procyanidine |
| CN103536495A (en) * | 2013-10-28 | 2014-01-29 | 西北农林科技大学 | Preparation method of grape seed procyanidin sun cream |
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| CN103536476A (en) * | 2013-10-17 | 2014-01-29 | 苏州威尔德工贸有限公司 | Grape seed oil skin protection cream and preparation method thereof |
| CN103767898A (en) * | 2014-01-26 | 2014-05-07 | 新疆亲努尔生物科技有限公司 | Horse-oil cold-dispelling foot cream |
| CN104606079A (en) * | 2015-02-06 | 2015-05-13 | 深圳唯美度生物科技有限公司 | Hand care product and preparation method thereof |
| CN104666126A (en) * | 2015-02-06 | 2015-06-03 | 深圳唯美度生物科技有限公司 | Liquid preparation employing horse oil as active component |
| CN105267090A (en) * | 2015-11-05 | 2016-01-27 | 山东润泽制药有限公司 | Skin care product with main components of horse oil and salvia sclarea essential oil and method for manufacturing skin care product |
| CN106420504A (en) * | 2016-12-01 | 2017-02-22 | 北京化工大学 | Antioxidant skin-care composition containing ocean collagen degradation product and its application |
| CN108078867A (en) * | 2018-02-01 | 2018-05-29 | 乌鲁木齐芊草汇生物科技有限公司 | A kind of skin-protection product and preparation method thereof |
| CN111166685A (en) * | 2018-10-24 | 2020-05-19 | 福建省梦娇兰日用化学品有限公司 | A children skin caring cream containing horse oil |
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| CN111166685A (en) * | 2018-10-24 | 2020-05-19 | 福建省梦娇兰日用化学品有限公司 | A children skin caring cream containing horse oil |
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