CN103143312A - Method for extracting rose extract by utilizing a pot-type ultrasonic equipment - Google Patents
Method for extracting rose extract by utilizing a pot-type ultrasonic equipment Download PDFInfo
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- CN103143312A CN103143312A CN2013101052600A CN201310105260A CN103143312A CN 103143312 A CN103143312 A CN 103143312A CN 2013101052600 A CN2013101052600 A CN 2013101052600A CN 201310105260 A CN201310105260 A CN 201310105260A CN 103143312 A CN103143312 A CN 103143312A
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- rose
- organic solvent
- extract
- flos rosae
- rosae rugosae
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Abstract
The invention provides a method for extracting rose extract by utilizing pot-type ultrasonic equipment. The method comprises the following steps of: drying fresh rose petals in shade and crushing the dried rose petals into 10-40 meshes; mixing the dried rose petals with an organic solvent in a mass ratio of 1:(5-10), putting the mixture to the a pot-type ultrasonic extractor for extracting for 20 minutes to 40 minutes under 25 DEG C to 50 DEG C to obtain a rose organic solvent mixture; putting the rose organic solvent mixture to a melt cinder extruding-separating device, separating the slag charge, squeezing and separating the slag charge at the speed of 20kg-100kg/h to obtain the rose extract organic solvent mixture; and putting the rose extract organic solvent mixture to a dynamic circulating low-temperature evaporation concentrator, reducing the pressure of the dynamic circulating low-temperature evaporation concentrator to -0.08MPa, and recycling the organic solvent at 20 DEG C to 40 DEG C to obtain the rose extract, wherein the yield of the rose extract is not lower than 9%.
Description
Technical field
The present invention relates to the technique of Flos Rosae Rugosae extract, especially adopt hyperacoustic extraction, the method has significant effect to improving the recovery rate of plant live part composition.
Background technology
Traditional rose extracting method: (1) steam distillation makes aromatic ester and the aromatic alcohol that single rose ethereal oil main component is effumability.Rose ethereal oil recovery rate≤0.03%.In this spices type of rose plant, except containing rose ethereal oil, also contain a large amount of to human body is very useful but the compositions such as not volatile plant wax, protein, glucoside, carbohydrate only can't be realized extraction and application by traditional way of distillation; (2) CO
2The resulting Flos Rosae Rugosae extract recovery rate of supercritical extraction≤1.6%.
The invention provides supersonic extracting method, not only extract rose ethereal oil, compositions such as not volatile plant wax, protein, glucoside, carbohydrate in a large number (account for extract total amount 15～20%) can also be extracted, and the high composition of these values can't be realized by traditional extraction method.The material that employing the method is obtained has wide market sale prospect for the production of the chemical industry consumer goods provides abundant raw material and additive resource, must be subject to consumer's favor.
Summary of the invention
The object of the invention is to: adopt ultrasonic method to extract Flos Rosae Rugosae extract, shortened extraction time, reduced the extraction temperature, the heat-sensitive substance that adequately protected improves effective component content and quality.
The object of the present invention is achieved like this: a kind of method of utilizing the pot type ultrasonic equipment to extract Flos Rosae Rugosae extract, step by step:
1) will pluck high-quality, without the fresh-rose petal that rots, be placed in the rear pulverizing of drying in the shade under natural conditions, wherein the water content of comminuting matter≤20%, granularity 10～40 orders;
2) rose of pulverizing is mixed with the mass ratio of organic solvent by 1:5～10, be placed in the pot type ultrasonic extractor and extract, extract 20～40min under 25～50 ℃ of conditions, get the rose ORGANIC SOLVENT MIXTURES;
3) the rose ORGANIC SOLVENT MIXTURES is placed in melt cinder and extracts separator, separate slag charge, carry out expression separation by 20～100kg/h, get the Flos Rosae Rugosae extract ORGANIC SOLVENT MIXTURES;
4) the Flos Rosae Rugosae extract ORGANIC SOLVENT MIXTURES is placed in dynamic circulation low-temperature evaporation inspissator, decompression is arrived-0.08MPa, reclaims organic solvent under 20～40 ℃ of conditions, namely gets Flos Rosae Rugosae extract;
The organic solvent that wherein adopts is ethanol or ethyl acetate;
The yield of the Flos Rosae Rugosae extract of described method is 〉=9%.
Know-why of the present invention and effect: Flos Rosae Rugosae extract is owing to having adopted ultrasonic technology, by ultrasonic wave stretching shaking force can the rose compact tissue is loose, broken, plant cell wall is broken, the compositions such as the stronger plant wax of the fragrant effective ingredients such as rose tissue space and intracellular ester class, alcohols and adhesive force, protein, glucoside, carbohydrate are fully freed rear by organic solvent dissolution, high extraction reaches more than 9%; Next has guaranteed to use the solvent of minimum to reach best extraction effect; Adopting traditional way of distillation to extract the Flos Rosae Rugosae extract yield is only 0.03%; Adopt CO
2It is only also 1.6% that supercritical extraction extracts the Flos Rosae Rugosae extract yield.
The present invention adopts ultrasonic method to extract Flos Rosae Rugosae extract, has shortened extraction time, and the heat-sensitive substance that adequately protected improves effective component content and quality.Ultrasonic wave extracts the method for Flos Rosae Rugosae extract, will extract, the functions such as the melt cinder extruding separates, filter, concentrate, residual solvent Distillation recovery organically combine, and highlight technique effect, show technological progress.
Description of drawings
The present invention is described further by reference to the accompanying drawings.
Accompanying drawing is the process flow diagram that the pot type ultrasonic equipment extracts Flos Rosae Rugosae extract;
As shown in the figure: pulverize rose--mix with organic solvent in ultrasonic extractor and extract--the rose ORGANIC SOLVENT MIXTURES--input is extracted melt cinder and is extracted separator--separates slag charge--get mixture and input dynamic circulation low-temperature evaporation inspissator---organic solvent reclaims-gets Flos Rosae Rugosae extract.
The specific embodiment:
The present invention is described further in conjunction with the embodiments.
Embodiment
Raw material is disposed: will pluck high-quality, without rotten fresh-rose petal, and dry in the shade under field conditions (factors), during its water content≤20%, it be pulverized 20 mesh sieves;
Preparation scheme 1
Get the rose 10kg that pulverized 20 mesh sieves, put into the organic solvent ethanol (95%) that the clean general happy bio tech ltd in Xinjiang is produced the pot type ultrasonic extractor that meets JB/T 20126-2009 national standard by the mass ratio of 1:8, keeping extracting 35min at 40 ℃ of ultrasonic extractor temperature, get the rose alcohol mixture; After this mixture input extraction melt cinder is extracted separator, isolate slag charge and extract mixture, to extract mixture input dynamic circulation low-temperature reduced-pressure (0.08MPa) in the evaporation concentrator, keep 35 ℃ of temperature, recycling after the organic solvent ethanol evaporation reclaims, collect residue extract 1.0kg, be Flos Rosae Rugosae extract, yield is 10%.
Preparation scheme 2
Get the rose 10kg that pulverized 20 mesh sieves, put into the organic solvent ethyl acetate that Tianjin Fu Yu Fine Chemical Co., Ltd produces the pot type ultrasonic extractor that meets JB/T 20126-2009 national standard by the mass ratio of 1:10, keeping extracting 40min under ultrasonic extractor temperature 45 C, get the rose ethyl acetate mixture; After this mixture input extraction melt cinder is extracted separator, isolate slag charge and extract mixture, to extract mixture input dynamic circulation low-temperature reduced-pressure (0.08MPa) in the evaporation concentrator, keep 40 ℃ of temperature, recycling after the evaporation of organic solvent ethyl acetate is reclaimed, collect residue extract 0.9kg, be Flos Rosae Rugosae extract, yield is 9%.
This method obtains the effect of extract:
Production example 1
The interpolation of rose Manual perfumed soap:
During Manual perfumed soap was made, after the saponification process was completed, the saponification liquor temperature added rose extract 1.0 or 3.0%(kg/kg when remaining on 60 or 80 ℃), that constant temperature stirs is cooling in the injection moulding mould, cut apart, pack and to get the rose Manual perfumed soap.This rose extract is applied in the making of Manual perfumed soap, has replaced the use of chemical essence and pigment in common perfumed soap, after using more than the lasting 24h of body surface lasting, can play the effects such as tender white, moisturizing, moisturizing.
Production example 2
The interpolation of cosmetics creme class skin care item rose hand lotion:
When making skin care item hand lotion emulsification process and finish, add rose extract 0.9 or 1.5%(kg/kg when keeping temperature 40 or 60 ℃), be down to room temperature after constant temperature stirs, after packing, packing both the rose hand lotion.This rose extract is applied to the use that hand lotion has replaced chemical essence and pigment in common perfumed soap, and the sustainable lasting of body surface after using can play the effects such as tender white, moisturizing, moisturizing.
Claims (2)
1. method of utilizing the pot type ultrasonic equipment to extract Flos Rosae Rugosae extract is characterized in that: step by step:
1) will pluck high-quality, without the fresh-rose petal that rots, be placed in the rear pulverizing of drying in the shade under natural conditions, wherein the water content of comminuting matter≤20%, granularity 10～40 orders;
2) rose of pulverizing is mixed with the mass ratio of organic solvent by 1:5～10, be placed in the pot type ultrasonic extractor and extract, at 25～50 ℃, extract 20～40min, get the rose ORGANIC SOLVENT MIXTURES;
3) the rose ORGANIC SOLVENT MIXTURES is placed in melt cinder and extracts separator, separate slag charge, carry out expression separation by 20～100kg/h, get the Flos Rosae Rugosae extract ORGANIC SOLVENT MIXTURES;
4) the Flos Rosae Rugosae extract ORGANIC SOLVENT MIXTURES is placed in dynamic circulation low-temperature evaporation inspissator, decompression is arrived-0.08MPa, reclaims organic solvents at 20～40 ℃, namely gets Flos Rosae Rugosae extract;
The organic solvent that wherein adopts is ethanol or ethyl acetate.
2. method according to claim 1, it is characterized in that: the yield of Flos Rosae Rugosae extract is 〉=9%.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310105260.0A CN103143312B (en) | 2013-03-28 | 2013-03-28 | Method for extracting rose extract by utilizing a pot-type ultrasonic equipment |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201310105260.0A CN103143312B (en) | 2013-03-28 | 2013-03-28 | Method for extracting rose extract by utilizing a pot-type ultrasonic equipment |
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| CN103143312A true CN103143312A (en) | 2013-06-12 |
| CN103143312B CN103143312B (en) | 2015-07-08 |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107099803A (en) * | 2017-06-29 | 2017-08-29 | 西南石油大学 | A kind of preparation method and purposes of the carbon steel pickling corrosion inhibitor containing Flos Rosae Rugosae extract |
| CN112175776A (en) * | 2020-11-03 | 2021-01-05 | 茅台学院 | Preparation method of rose and jasmine Maotai-flavor liquor |
| CN114403448A (en) * | 2022-02-17 | 2022-04-29 | 北京鲜汽十族食品科技有限公司 | Rose tangerine peel water and preparation method thereof |
-
2013
- 2013-03-28 CN CN201310105260.0A patent/CN103143312B/en active Active
Non-Patent Citations (1)
| Title |
|---|
| 王晓林等: "玫瑰花总黄酮的超声提取工艺", 《食品研究与开发》 * |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107099803A (en) * | 2017-06-29 | 2017-08-29 | 西南石油大学 | A kind of preparation method and purposes of the carbon steel pickling corrosion inhibitor containing Flos Rosae Rugosae extract |
| CN112175776A (en) * | 2020-11-03 | 2021-01-05 | 茅台学院 | Preparation method of rose and jasmine Maotai-flavor liquor |
| CN114403448A (en) * | 2022-02-17 | 2022-04-29 | 北京鲜汽十族食品科技有限公司 | Rose tangerine peel water and preparation method thereof |
| CN114403448B (en) * | 2022-02-17 | 2024-03-22 | 北京鲜汽十族食品科技有限公司 | Rose and dried orange peel water and preparation method thereof |
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| Publication number | Publication date |
|---|---|
| CN103143312B (en) | 2015-07-08 |
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Effective date of registration: 20150910 Address after: 835000 Bayan Dai village, Dai Town, Yining, Yili Kazakh Autonomous Prefecture, the Xinjiang Uygur Autonomous Region, Bayan Patentee after: Yili lavender products Co. Ltd. Mayila St. Address before: 835000 the Xinjiang Uygur Autonomous Region Yili Kazak Autonomous Prefecture of Yining City, Bayan Dai Zhen Yili lavender products Co. Ltd. Mayila St. Patentee before: Zheng Gang Patentee before: Wang Yubiao |
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| EE01 | Entry into force of recordation of patent licensing contract |
Application publication date: 20130612 Assignee: Yili lavender products Co. Ltd. Mayila St. Assignor: Zheng Gang|Wang Yubiao Contract record no.: 2015650000037 Denomination of invention: Method for extracting rose extract by utilizing a pot-type ultrasonic equipment Granted publication date: 20150708 License type: Exclusive License Record date: 20150831 |
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