CN110123675A - A kind of tea-seed oil water conservation skin care suncream and preparation method thereof - Google Patents
A kind of tea-seed oil water conservation skin care suncream and preparation method thereof Download PDFInfo
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/04—Topical preparations for affording protection against sunlight or other radiation; Topical sun tanning preparations
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- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
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- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/10—Production of fats or fatty oils from raw materials by extracting
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Abstract
The present invention provides a kind of tea-seed oil water conservation skin care suncream and preparation method thereof, the raw material including following parts by weight: exquisite tea-seed oil 15-25 parts, 5-7 parts of moringa seeds extracting solution, 3-5 parts of Folium Forsythia, 5-7 parts of flower extracting liquid, 2-4 parts of aloe, 1-3 parts of Poria cocos, 4-6 parts of water chestnut extracting solution, filler 20-30 parts of thickening, 1-2 parts of grape hydrochlorate, 0.5-1 parts of jojoba butter, 4-6 parts of auxiliary agent of increasing property.The present invention can effectively prevent skin by tanned, sunburn, and effective moisturizing can lighten the stain freckle, skin care, antiallergy, and ingredient is mostly plant extracts, avoids chemical substance stimulation caused by skin；Its raw material of preparation method of the invention are cheap simultaneously, and technique is distinct, do not add chemical preservative, and materials are convenient, practical value with higher and good application prospect.
Description
Technical field
The present invention relates to tea-seed oil deep process technology fields, and in particular to a kind of tea-seed oil water conservation skin care suncream and its system
Preparation Method.
Background technique
Suncream, the sun-screening agent of ultraviolet light can be obstructed or absorb to reach and prevent skin by tanned, sunburn by referring to be added to
Cosmetics.According to sun-proof principle, suncream can be divided into physical sunscreen frost, chemical sunscreen frost, added in suncream now
Olive oil price is more expensive, and raw material is less, while a large amount of chemical synthesis component and essence are being added in suncream to body
Body has a certain impact.
Tea-seed oil also known as camellia oil, tea pear oil (Fujian is commonly called as), Wild camellia seed oil, camellia seed oil, tea oil seeds of trees oil.Camellia is
The ground specialty such as Dabie Mountain of China, Fujian, Jiangxi, Hunan (Changning) can extract good camellia oil, i.e. tea-seed oil in fruit.
Camellia seed oil mainly contains the unsaturated fatty acids such as oleic acid, linoleic acid, and content of fatty acid, ratio and olive oil are very much like, element
The index of the title or even some nutritional ingredients that have " east olive oil " is higher than olive oil.Tea-seed oil is applied to sun-proof
Less discovery in frost, there is certain research significance.
Summary of the invention
In view of the drawbacks of the prior art, the object of the present invention is to provide a kind of tea-seed oils to be retained skin care suncream, this is sun-proof
Frost can effectively prevent skin by tanned, sunburn, and effective moisturizing can lighten the stain freckle, skin care, antiallergy, ingredient
It is mostly plant extracts, avoids chemical substance stimulation caused by skin；Its raw material of preparation method of the invention simultaneously
Cheap, technique is distinct, does not add chemical preservative, and materials are convenient, practical value with higher and good application prospect.
The present invention solves technical problem and adopts the following technical scheme that
The present invention provides a kind of tea-seed oils to be retained skin care suncream, the raw material including following parts by weight:
Exquisite tea-seed oil 15-25 parts, 5-7 parts of moringa seeds extracting solution, 3-5 parts of Folium Forsythia, 5-7 parts of flower extracting liquid, aloe
2-4 parts, 1-3 parts of Poria cocos, 4-6 parts of water chestnut extracting solution, thickening filler 20-30 parts, 1-2 parts of grape hydrochlorate, jojoba butter 0.5-1
Part, 4-6 parts of auxiliary agent of increasing property.
Preferably, the tea-seed oil water conservation skin care suncream includes the raw material of following parts by weight:
20 parts of exquisite tea-seed oil, 6 parts of moringa seeds extracting solution, 4 parts of Folium Forsythia, 6 parts of flower extracting liquid, 3 parts of aloe, Poria cocos 2
Part, 5 parts of water chestnut extracting solution, 25 parts of filler of thickening, 1.5 parts of grape hydrochlorate, 0.8 part of jojoba butter, 5 parts of auxiliary agent of increasing property.
Preferably, the exquisite tea-seed oil the preparation method comprises the following steps: by the camellia oleifera fruit of harvesting ripe, remove mildew, pest and disease damage
The seed of damage at, first stack 5-7 angel camellia oleifera fruit after-ripening, then after tea seed is removed the peel, it is evenly laid out on material disc, carry out
Heated-air drying, drying temperature are controlled at 60-80 DEG C, its water content is made to drop to 8% hereinafter, the tea seed after drying is put into tea seed
Broken shell in decorticator realizes Kernel-hull separation by pneumatic separating, the camellia seed kernel after shelling is crushed, is added relative to tea seed
The ethyl alcohol that the determining alcohol of 2-4 times of benevolence quality is 95%, first ultrasonic power is 200-300W, temperature is 65 DEG C of constant temperature processing 10-
20 minutes, reflux 1-2h is reheated, filters to obtain filter residue, determining alcohol filter residue being added again relative to 2-4 times of filter residue quality is
95% ethyl alcohol, is heated to reflux 1-2h, filtering and impurity removing, merges filtered fluid, be recovered under reduced pressure ethyl alcohol to get.
Preferably, the moringa seeds extracting solution the preparation method comprises the following steps: take appropriate moringa seeds volumetric concentration be 70% ethyl alcohol
It is 24 DEG C of -28 DEG C of extractions processing in temperature, ethanol extract is obtained, then ethanol extract is crossed into AB-8 macroporous resin column, with distillation
Water washing is transparent to efflux, then with volumetric concentration is 3-5 times of column volume of 55%-65% ethanol elution, obtains ethanol eluate, most
Moringa seeds extracting solution is obtained with ethanol eluate recycling ethyl alcohol afterwards.
Preferably, the flower extracting liquid the preparation method comprises the following steps: by weight by 4-6 parts of chrysanthemum, 2-4 parts of honeysuckle, jasmine
1-3 parts of jasmine, 2-4 parts of violet rinsed well with clear water, be added pulverizer in crush, add 10-12 times of water to be heated to 90-100
Degree Celsius, it decocts 2-4 hours, solid and liquid separation；Residue after first time water is mentioned again adds 8-10 times to measure water second of water of progress
It mentions, extracts 1-3 hours, solid and liquid separation；Residue after second of water is mentioned again adds 4-6 times to measure water progress ultrasonic extraction, extracts 1-
2 hours, merge extracting solution three times, is concentrated to get flower extracting liquid.
Preferably, the water chestnut extracting solution the preparation method comprises the following steps: by water chestnut remove the peel be added juice extractor in, juicing, be added fruit
Glue enzyme controls temperature at 15 DEG C, stands 10-16 hours, obtain clear water chestnut juice, is concentrated under reduced pressure, then 1-3 DEG C of low-temperature preservation is standby
With.
Preferably, it is described thickening filler the preparation method comprises the following steps: by attapulgite, bentonite, conch meal according to weight ratio 2: 1
: 3 be 480-520 DEG C in temperature at calcine 1-2h, after cooling, ball milling crosses 100-200 mesh, then in the acetic acid solution of 8-10%
It after middle immersion 2-4h, takes out, deionized water is washed to neutrality, and the smooth single oleic acid of sorb for being equivalent to diatom powder weight 2-4% is added
Ester, after mixing, drying, be ground into nanometer powder to get.
Preferably, the gluconate is zinc gluconate, copper gluconate, managanese gluconate are formed according to weight ratio 1: 3: 2
Mixture.
The increasing property auxiliary agent is zinc sulfate, lysine, nano-titanium dioxide, methyl hydroxybenzoate according to again than 2: 1: 3: 1 composition
Mixture.
The present invention also provides a kind of preparation methods of tea-seed oil water conservation skin care suncream, comprising the following steps:
Step 1 weighs prepare each component raw material as required；
Step 2 after cleaning Folium Forsythia, aloe, Poria cocos with clear water, is sent into microtome, is then added in boiling water and floats
It scalds 6-8 minutes, picks up to be sent into extruding-desiccation machine and remove moisture removal, be re-fed into crushing in pulverizer and obtain mixed-powder A；
Step 3 moringa seeds extracting solution, flower extracting liquid, water chestnut extracting solution, grape hydrochlorate is added in blender, in temperature
Degree is to stir 10-20 minutes, speed of agitator 100-200r/min obtains mixed liquid B at 40-50 DEG C；
Exquisite tea-seed oil, jojoba butter, increasing property auxiliary agent are added in reaction kettle step 4, are 70-80 DEG C in temperature, stir
It mixes 20-30 minutes, the mix powder A of step 2 preparation is added, continue stirring 15-25 minutes, cooling to 30-40 DEG C, adding
The mixed liquid B and thickening filler for entering step 3 preparation, continue stirring 5-15 minutes, obtain thick paste mixture C；
Step 5 the thick paste mixture C of step 4 preparation is added in homogenizer, homogenizer revolving speed 5500-7500r/
Min, the homogenization 8-10min under 50-60 DEG C, the pressure of 18-22MPa, then taken off under 40-50 DEG C, 80-90kPa vacuum degree
Gas 10-12min, then ultra-high temperature sterilization 40-50 seconds at 130-150 DEG C, the tea-seed oil water conservation invented after aseptic canning is protected
Skin suncream.
Preferably, the preparation step of the tea-seed oil water conservation skin care suncream are as follows:
Step 1 weighs prepare each component raw material as required；
Step 2 after cleaning Folium Forsythia, aloe, Poria cocos with clear water, is sent into microtome, is then added in boiling water and floats
It scalds 7 minutes, picks up to be sent into extruding-desiccation machine and remove moisture removal, be re-fed into crushing in pulverizer and obtain mixed-powder A；
Step 3 moringa seeds extracting solution, flower extracting liquid, water chestnut extracting solution, grape hydrochlorate is added in blender, in temperature
Degree is to stir 15 minutes, speed of agitator 150r/min obtains mixed liquid B at 45 DEG C；
Exquisite tea-seed oil, jojoba butter, increasing property auxiliary agent are added in reaction kettle step 4, are 75 DEG C in temperature, stirring 25
Minute, the mix powder A of step 2 preparation is added, continues stirring 20 minutes, is cooling to 35 DEG C, step 3 preparation is added
Mixed liquid B and thickening filler, continue stirring 10 minutes, obtain thick paste mixture C；
Step 5 the thick paste mixture C of step 4 preparation is added in homogenizer, homogenizer revolving speed 6500r/min,
55 DEG C, homogenization 9min under the pressure of 20MPa, then the 11min that deaerates under 45 DEG C, 85kPa vacuum degree, then surpass at 140 DEG C
High-temperature sterilization 45 seconds, the tea-seed oil water conservation skin care suncream invented after aseptic canning.
Compared with prior art, the present invention have it is following the utility model has the advantages that
(1) a kind of tea-seed oil of the invention water conservation skin care suncream uses a large amount of tea-seed oil, the molecular structure of tea oil
It is very thin or even also thinner than olive oil, there are desalinationization color spot freckle, skin care, antiallergy sterilization and enhancing immunization,
Than existing olive oil there are also better sun-proof result, cost is also substantially reduced than olive oil, while being provided in the present invention
The preparation method of exquisite tea-seed oil, the tea-seed oil impurity that, drying ripe by heap, ultrasonic extraction, organic solvent extraction, reflux obtain
Less, purity is higher, and fat clarification quality is higher, is more suitable for sun-proof component and uses, while can efficiently use raw material,
Oil yield is higher, reduces costs.
(2) the moringa seeds extracting solution added in a kind of tea-seed oil of the invention water conservation skin care suncream, has preferable
Uvioresistant, moisturizing effect, while there are also preferable moisture-keeping functions, extracting method provided by the invention can effectively save peppery
Active constituent in the wooden seed effectively increases the sun-proof water retention property of suncream.
(3) flower extracting liquid of a kind of tea-seed oil of the invention water conservation skin care suncream addition, on the one hand improves sun-proof
The fragrance of frost, avoids damage of the chemical synthesis essence to human body, another aspect chrysanthemum, honeysuckle, Jasmine, violet are also
Certain sterilizing skin moistening effect.
(4) a kind of water chestnut extracting solution of tea-seed oil of the invention water conservation skin care suncream addition is retained with stronger moisturizing
Effect, there are also certain whitening performances.
(5) the thickening filler that the present invention adds is processed by the calcining and grinding to attapulgite, bentonite, conch meal, and one
Aspect makes the ultraviolet resistance of suncream more preferable, on the other hand makes sense of touch excellent, can effectively adsorb skin oil and fat, kill
Bacterium adsorption effect is excellent.
(6) homogenization has been used in a kind of preparation method of tea-seed oil of the invention water conservation skin care suncream, after mashing
Slurry mixing after again through high-pressure homogeneous processing, material can be more evenly mutually mixed, product particle extremely refine, sense of touch is more
It is good, substantially increase the efficiency that effective component absorbs in suncream.
(7) jojoba butter of a kind of tea-seed oil of the invention water conservation skin care suncream addition, texture is more slim and graceful, can be fast
Fast ground drawout on the skin, and to skin leave it is soft use not stickyly after feel, improve the quality of suncream.
(8) a kind of tea-seed oil of the invention water conservation skin care suncream can effectively prevent skin by tanned, sunburn, effectively protect
It is wet, freckle, skin care, antiallergy can be lightened the stain, ingredient is mostly plant extracts, avoids chemical substance to skin
It is stimulated caused by skin；Its raw material of preparation method of the invention are cheap simultaneously, and technique is distinct, do not add chemical preservative, draw materials
It is convenient, practical value with higher and good application prospect.
Specific embodiment
Combined with specific embodiments below, technical scheme in the embodiment of the invention is clearly and completely described, shows
So, described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.Based on the reality in the present invention
Example is applied, every other embodiment obtained by those of ordinary skill in the art without making creative efforts all belongs to
In the scope of protection of the invention.
Embodiment 1.
A kind of tea-seed oil of the present embodiment is retained skin care suncream, the raw material including following parts by weight:
15 parts of exquisite tea-seed oil, 5 parts of moringa seeds extracting solution, 3 parts of Folium Forsythia, 5 parts of flower extracting liquid, 2 parts of aloe, Poria cocos 1
Part, 4 parts of water chestnut extracting solution, 20 parts of filler of thickening, 1 part of grape hydrochlorate, 0.5 part of jojoba butter, 4 parts of auxiliary agent of increasing property.
Exquisite tea-seed oil in the present embodiment the preparation method comprises the following steps: by the camellia oleifera fruit of harvesting ripe, remove mildew, pest and disease damage
The seed of damage at, first stack 5 angel's camellia oleifera fruit after-ripening, then after tea seed is removed the peel, it is evenly laid out on material disc, carry out heat
Air-dry it is dry, drying temperature control at 60 DEG C, so that its water content is dropped to 8% and peel off hereinafter, the tea seed after drying is put into tea seed
Broken shell in machine realizes Kernel-hull separation by pneumatic separating, the camellia seed kernel after shelling is crushed, is added relative to camellia seed kernel matter
The ethyl alcohol that the determining alcohol of 2 times of amount is 95% reheats first ultrasonic power is 200W, temperature is that 65 DEG C of constant temperature are handled 10 minutes
Flow back 1h, filters to obtain filter residue, and filter residue is added to the ethyl alcohol for being 95% relative to 2 times of filter residue quality of determining alcohol again, is heated back
Flow 1h, filtering and impurity removing, merge filtered fluid, be recovered under reduced pressure ethyl alcohol to get.
Moringa seeds extracting solution in the present embodiment the preparation method comprises the following steps: taking appropriate moringa seeds volumetric concentration is 70% ethyl alcohol
It is 24 DEG C of extraction processing in temperature, obtains ethanol extract, then ethanol extract is crossed into AB-8 macroporous resin column, be washed with distilled water
It is transparent to efflux, then with volumetric concentration be 55% ethanol elution, 3 times of column volumes, obtain ethanol eluate, finally use ethanol elution
Liquid recycling ethyl alcohol obtains moringa seeds extracting solution.
Flower extracting liquid in the present embodiment the preparation method comprises the following steps: by weight by 4 parts of chrysanthemum, 2 parts of honeysuckle, Jasmine
1 part, 2 parts of violet is rinsed well with clear water, is added in pulverizer and is crushed, and 10 times of water is added to be heated to 90 degrees Celsius, and it is small to decoct 2
When, solid and liquid separation；Residue after first time water is mentioned again adds 8 times of amount water second of water of progress to mention, and extracts 1 hour, solid, liquid point
From；Residue after second of water is mentioned again adds 4 times of amount water to carry out ultrasonic extraction, extracts 1 hour, merges extracting solution three times, is concentrated,
Up to flower extracting liquid.
Water chestnut extracting solution in the present embodiment is added in juice extractor the preparation method comprises the following steps: water chestnut is removed the peel, and fruit is added in juicing
Glue enzyme controls temperature at 15 DEG C, stands 10 hours, obtain clear water chestnut juice, is concentrated under reduced pressure, then 1 DEG C of low-temperature preservation is spare i.e.
It can.
In the present embodiment thickening filler the preparation method comprises the following steps: by attapulgite, bentonite, conch meal according to weight ratio 2:
1: 3 be 480 DEG C in temperature at calcine 1h, after cooling, ball milling is sieved with 100 mesh sieve, after then impregnating 2h in 8% acetic acid solution,
It takes out, deionized water is washed to neutrality, the sorbitan monooleate for being equivalent to diatom powder weight 2% is added, after mixing, drying,
Be ground into nanometer powder to get.
Gluconate in the present embodiment is zinc gluconate, copper gluconate, managanese gluconate are formed according to weight ratio 1: 3: 2
Mixture；
The increasing property auxiliary agent is zinc sulfate, lysine, nano-titanium dioxide, methyl hydroxybenzoate according to again than 2: 1: 3: 1 composition
Mixture.
A kind of preparation method of the tea-seed oil water conservation skin care suncream of the present embodiment, comprising the following steps:
Step 1 weighs prepare each component raw material as required；
Step 2 after cleaning Folium Forsythia, aloe, Poria cocos with clear water, is sent into microtome, is then added in boiling water and floats
It scalds 6 minutes, picks up to be sent into extruding-desiccation machine and remove moisture removal, be re-fed into crushing in pulverizer and obtain mixed-powder A；
Step 3 moringa seeds extracting solution, flower extracting liquid, water chestnut extracting solution, grape hydrochlorate is added in blender, in temperature
Degree is to stir 10 minutes, speed of agitator 100r/min obtains mixed liquid B at 40 DEG C；
Exquisite tea-seed oil, jojoba butter, increasing property auxiliary agent are added in reaction kettle step 4, are 70 DEG C in temperature, stirring 20
Minute, the mix powder A of step 2 preparation is added, continues stirring 15 minutes, is cooling to 30 DEG C, step 3 preparation is added
Mixed liquid B and thickening filler, continue stirring 5 minutes, obtain thick paste mixture C；
Step 5 the thick paste mixture C of step 4 preparation is added in homogenizer, homogenizer revolving speed 5500r/min,
50 DEG C, homogenization 8min under the pressure of 18MPa, then the 10min that deaerates under 40 DEG C, 80kPa vacuum degree, then surpass at 130 DEG C
High-temperature sterilization 40 seconds, the tea-seed oil water conservation skin care suncream invented after aseptic canning.
Embodiment 2.
A kind of tea-seed oil of the present embodiment is retained skin care suncream, the raw material including following parts by weight:
25 parts of exquisite tea-seed oil, 7 parts of moringa seeds extracting solution, 5 parts of Folium Forsythia, 7 parts of flower extracting liquid, 4 parts of aloe, Poria cocos 3
Part, 6 parts of water chestnut extracting solution, 30 parts of filler of thickening, 2 parts of grape hydrochlorate, 1 part of jojoba butter, 6 parts of auxiliary agent of increasing property.
Exquisite tea-seed oil in the present embodiment the preparation method comprises the following steps: by the camellia oleifera fruit of harvesting ripe, remove mildew, pest and disease damage
The seed of damage at, first stack 7 angel's camellia oleifera fruit after-ripening, then after tea seed is removed the peel, it is evenly laid out on material disc, carry out heat
Air-dry it is dry, drying temperature control at 80 DEG C, so that its water content is dropped to 8% and peel off hereinafter, the tea seed after drying is put into tea seed
Broken shell in machine realizes Kernel-hull separation by pneumatic separating, the camellia seed kernel after shelling is crushed, is added relative to camellia seed kernel matter
The ethyl alcohol that the determining alcohol of 4 times of amount is 95% reheats first ultrasonic power is 300W, temperature is that 65 DEG C of constant temperature are handled 20 minutes
Flow back 2h, filters to obtain filter residue, and filter residue is added to the ethyl alcohol for being 95% relative to 4 times of filter residue quality of determining alcohol again, is heated back
Flow 2h, filtering and impurity removing, merge filtered fluid, be recovered under reduced pressure ethyl alcohol to get.
Moringa seeds extracting solution in the present embodiment the preparation method comprises the following steps: taking appropriate moringa seeds volumetric concentration is 70% ethyl alcohol
It is 28 DEG C of extraction processing in temperature, obtains ethanol extract, then ethanol extract is crossed into AB-8 macroporous resin column, be washed with distilled water
It is transparent to efflux, then with volumetric concentration be 65% ethanol elution, 5 times of column volumes, obtain ethanol eluate, finally use ethanol elution
Liquid recycling ethyl alcohol obtains moringa seeds extracting solution.
Flower extracting liquid in the present embodiment the preparation method comprises the following steps: by weight by 6 parts of chrysanthemum, 4 parts of honeysuckle, Jasmine
3 parts, 4 parts of violet are rinsed well with clear water, are added in pulverizer and are crushed, and 12 times of water is added to be heated to 100 degrees Celsius, and it is small to decoct 4
When, solid and liquid separation；Residue after first time water is mentioned again adds 10 times of amount water second of water of progress to mention, and extracts 3 hours, solid, liquid point
From；Residue after second of water is mentioned again adds 6 times of amount water to carry out ultrasonic extraction, extracts 2 hours, merges extracting solution three times, is concentrated,
Up to flower extracting liquid.
Water chestnut extracting solution in the present embodiment is added in juice extractor the preparation method comprises the following steps: water chestnut is removed the peel, and fruit is added in juicing
Glue enzyme controls temperature at 15 DEG C, stands 16 hours, obtain clear water chestnut juice, is concentrated under reduced pressure, then 3 DEG C of low-temperature preservations are spare i.e.
It can.
In the present embodiment thickening filler the preparation method comprises the following steps: by attapulgite, bentonite, conch meal according to weight ratio 2:
1: 3 be 520 DEG C in temperature at calcine 2h, after cooling, ball milling crosses 200 meshes, after then impregnating 4h in 10% acetic acid solution,
It takes out, deionized water is washed to neutrality, the sorbitan monooleate for being equivalent to diatom powder weight 4% is added, after mixing, drying,
Be ground into nanometer powder to get.
Gluconate in the present embodiment is zinc gluconate, copper gluconate, managanese gluconate are formed according to weight ratio 1: 3: 2
Mixture；
The increasing property auxiliary agent is zinc sulfate, lysine, nano-titanium dioxide, methyl hydroxybenzoate according to again than 2: 1: 3: 1 composition
Mixture.
A kind of preparation method of the tea-seed oil water conservation skin care suncream of the present embodiment, comprising the following steps:
Step 1 weighs prepare each component raw material as required；
Step 2 after cleaning Folium Forsythia, aloe, Poria cocos with clear water, is sent into microtome, is then added in boiling water and floats
It scalds 8 minutes, picks up to be sent into extruding-desiccation machine and remove moisture removal, be re-fed into crushing in pulverizer and obtain mixed-powder A；
Step 3 moringa seeds extracting solution, flower extracting liquid, water chestnut extracting solution, grape hydrochlorate is added in blender, in temperature
Degree is to stir 20 minutes, speed of agitator 200r/min obtains mixed liquid B at 50 DEG C；
Exquisite tea-seed oil, jojoba butter, increasing property auxiliary agent are added in reaction kettle step 4, are 80 DEG C in temperature, stirring 30
Minute, the mix powder A of step 2 preparation is added, continues stirring 25 minutes, is cooling to 40 DEG C, step 3 preparation is added
Mixed liquid B and thickening filler, continue stirring 15 minutes, obtain thick paste mixture C；
Step 5 the thick paste mixture C of step 4 preparation is added in homogenizer, homogenizer revolving speed 7500r/min,
60 DEG C, homogenization 10min under the pressure of 22MPa, then the 12min that deaerates under 50 DEG C, 90kPa vacuum degree, then surpass at 150 DEG C
High-temperature sterilization 50 seconds, the tea-seed oil water conservation skin care suncream invented after aseptic canning.
Embodiment 3.
A kind of tea-seed oil of the present embodiment is retained skin care suncream, the raw material including following parts by weight:
20 parts of exquisite tea-seed oil, 6 parts of moringa seeds extracting solution, 4 parts of Folium Forsythia, 6 parts of flower extracting liquid, 3 parts of aloe, Poria cocos 2
Part, 5 parts of water chestnut extracting solution, 25 parts of filler of thickening, 1.5 parts of grape hydrochlorate, 0.8 part of jojoba butter, 5 parts of auxiliary agent of increasing property.
Exquisite tea-seed oil in the present embodiment the preparation method comprises the following steps: by the camellia oleifera fruit of harvesting ripe, remove mildew, pest and disease damage
The seed of damage at, first stack 6 angel's camellia oleifera fruit after-ripening, then after tea seed is removed the peel, it is evenly laid out on material disc, carry out heat
Air-dry it is dry, drying temperature control at 70 DEG C, so that its water content is dropped to 8% and peel off hereinafter, the tea seed after drying is put into tea seed
Broken shell in machine realizes Kernel-hull separation by pneumatic separating, the camellia seed kernel after shelling is crushed, is added relative to camellia seed kernel matter
The ethyl alcohol that the determining alcohol of 3 times of amount is 95% reheats first ultrasonic power is 250W, temperature is that 65 DEG C of constant temperature are handled 15 minutes
Flow back 1.5h, filters to obtain filter residue, and filter residue is added to the ethyl alcohol for being 95% relative to 3 times of filter residue quality of determining alcohol, heating again
Flow back 1.5h, filtering and impurity removing, merge filtered fluid, be recovered under reduced pressure ethyl alcohol to get.
Moringa seeds extracting solution in the present embodiment the preparation method comprises the following steps: taking appropriate moringa seeds volumetric concentration is 70% ethyl alcohol
It is 26 DEG C of extraction processing in temperature, obtains ethanol extract, then ethanol extract is crossed into AB-8 macroporous resin column, be washed with distilled water
It is transparent to efflux, then with volumetric concentration be 3-5 times of column volume of 60% ethanol elution, obtain ethanol eluate, finally washed with ethyl alcohol
De- liquid recycling ethyl alcohol obtains moringa seeds extracting solution.
Flower extracting liquid in the present embodiment the preparation method comprises the following steps: by weight by 5 parts of chrysanthemum, 3 parts of honeysuckle, Jasmine
2 parts, 3 parts of violet are rinsed well with clear water, are added in pulverizer and are crushed, and 11 times of water is added to be heated to 95 degrees Celsius, and it is small to decoct 3
When, solid and liquid separation；Residue after first time water is mentioned again adds 9 times of amount water second of water of progress to mention, and extracts 2 hours, solid, liquid point
From；Residue after second of water is mentioned again adds 5 times of amount water to carry out ultrasonic extraction, extracts 1.5 hours, merges extracting solution three times, dense
Contracting is to get flower extracting liquid.
Water chestnut extracting solution in the present embodiment is added in juice extractor the preparation method comprises the following steps: water chestnut is removed the peel, and fruit is added in juicing
Glue enzyme controls temperature at 15 DEG C, stands 13 hours, obtain clear water chestnut juice, is concentrated under reduced pressure, then 2 DEG C of low-temperature preservations are spare i.e.
It can.
In the present embodiment thickening filler the preparation method comprises the following steps: by attapulgite, bentonite, conch meal according to weight ratio 2:
1: 3 be 500 DEG C in temperature at calcine 1.5h, after cooling, ball milling crosses 150 meshes, then impregnates 3h in 9% acetic acid solution
Afterwards, it takes out, deionized water is washed to neutrality, and the sorbitan monooleate for being equivalent to diatom powder weight 3% is added, and after mixing, is dried
It is dry, be ground into nanometer powder to get.
Gluconate in the present embodiment is zinc gluconate, copper gluconate, managanese gluconate are formed according to weight ratio 1: 3: 2
Mixture；
The increasing property auxiliary agent is zinc sulfate, lysine, nano-titanium dioxide, methyl hydroxybenzoate according to again than 2: 1: 3: 1 composition
Mixture.
A kind of preparation method of the tea-seed oil water conservation skin care suncream of the present embodiment, comprising the following steps:
Step 1 weighs prepare each component raw material as required；
Step 2 after cleaning Folium Forsythia, aloe, Poria cocos with clear water, is sent into microtome, is then added in boiling water and floats
It scalds 7 minutes, picks up to be sent into extruding-desiccation machine and remove moisture removal, be re-fed into crushing in pulverizer and obtain mixed-powder A；
Step 3 moringa seeds extracting solution, flower extracting liquid, water chestnut extracting solution, grape hydrochlorate is added in blender, in temperature
Degree is to stir 15 minutes, speed of agitator 150r/min obtains mixed liquid B at 45 DEG C；
Exquisite tea-seed oil, jojoba butter, increasing property auxiliary agent are added in reaction kettle step 4, are 75 DEG C in temperature, stirring 25
Minute, the mix powder A of step 2 preparation is added, continues stirring 20 minutes, is cooling to 35 DEG C, step 3 preparation is added
Mixed liquid B and thickening filler, continue stirring 10 minutes, obtain thick paste mixture C；
Step 5 the thick paste mixture C of step 4 preparation is added in homogenizer, homogenizer revolving speed 6500r/min,
55 DEG C, homogenization 9min under the pressure of 20MPa, then the 11min that deaerates under 45 DEG C, 85kPa vacuum degree, then surpass at 140 DEG C
High-temperature sterilization 45 seconds, the tea-seed oil water conservation skin care suncream invented after aseptic canning.
A kind of tea-seed oil water conservation skin care suncream of the invention can effectively prevent skin by tanned, sunburn, effective moisturizing, energy
Freckle, skin care, antiallergy are enough lightened the stain, ingredient is mostly plant extracts, avoids chemical substance and makes to skin
At stimulation；Its raw material of preparation method of the invention are cheap simultaneously, and technique is distinct, do not add chemical preservative, and materials are convenient,
Practical value with higher and good application prospect.
It is obvious to a person skilled in the art that invention is not limited to the details of the above exemplary embodiments, Er Qie
In the case where without departing substantially from spirit or essential attributes of the invention, the present invention can be realized in other specific forms.Therefore, no matter
From the point of view of which point, the present embodiments are to be considered as illustrative and not restrictive, and the scope of the present invention is by appended power
Benefit requires rather than above description limits, it is intended that all by what is fallen within the meaning and scope of the equivalent elements of the claims
Variation is included within the present invention.
In addition, it should be understood that although this specification is described in terms of embodiments, but not each embodiment is only wrapped
Containing an independent technical solution, this description of the specification is merely for the sake of clarity, and those skilled in the art should
It considers the specification as a whole, the technical solutions in the various embodiments may also be suitably combined, forms those skilled in the art
The other embodiments being understood that.
Claims (10)
1. a kind of tea-seed oil is retained skin care suncream, which is characterized in that the raw material including following parts by weight:
Exquisite tea-seed oil 15-25 parts, 5-7 parts of moringa seeds extracting solution, 3-5 parts of Folium Forsythia, 5-7 parts of flower extracting liquid, aloe 2-4
Part, filler 20-30 parts of thickening, 1-2 parts of grape hydrochlorate, 0.5-1 parts of jojoba butter, increases 1-3 parts of Poria cocos, 4-6 parts of water chestnut extracting solution
4-6 parts of auxiliary agent of property.
2. a kind of tea-seed oil according to claim 1 is retained skin care suncream, which is characterized in that the tea-seed oil water conservation shield
Skin suncream includes the raw material of following parts by weight:
20 parts of exquisite tea-seed oil, 6 parts of moringa seeds extracting solution, 4 parts of Folium Forsythia, 6 parts of flower extracting liquid, 3 parts of aloe, 2 parts of Poria cocos, water chestnut
5 parts of shepherd's purse extracting solution, 25 parts of filler of thickening, 1.5 parts of grape hydrochlorate, 0.8 part of jojoba butter, 5 parts of auxiliary agent of increasing property.
3. a kind of tea-seed oil according to claim 1 or 2 is retained skin care suncream, which is characterized in that the exquisiteness tea seed
Oil the preparation method comprises the following steps: by the camellia oleifera fruit of harvesting ripe, remove mildew, pest and disease damage damage seed at first stacking 5-7 angel oil
Tea fruit after-ripening, then after tea seed is removed the peel, it is evenly laid out on material disc, heated-air drying is carried out, drying temperature is controlled in 60-80
DEG C, so that its water content is dropped to 8% hereinafter, the tea seed after drying is put into broken shell in tea seed decorticator, it is real to pass through pneumatic separating
Existing Kernel-hull separation, the camellia seed kernel after shelling is crushed, and addition is 95% relative to 2-4 times of camellia seed kernel quality of determining alcohol
Ethyl alcohol, first ultrasonic power is 200-300W, temperature is that 65 DEG C of constant temperature are handled 10-20 minutes, reheating reflux 1-2h is filtered
The ethyl alcohol for being 95% relative to 2-4 times of filter residue quality of determining alcohol is added again, 1-2h is heated to reflux, filters by filter residue for filter residue
Removal of impurities, merge filtered fluid, be recovered under reduced pressure ethyl alcohol to get.
4. a kind of tea-seed oil according to claim 1 or 2 is retained skin care suncream, which is characterized in that the moringa seeds mention
Take liquid the preparation method comprises the following steps: it in temperature is 24 DEG C of -28 DEG C of extractions processing that take appropriate moringa seeds, which be 70% ethyl alcohol with volumetric concentration, is obtained
Ethanol extract, then ethanol extract is crossed into AB-8 macroporous resin column, it is transparent to be washed with distilled water to efflux, then dense with volume
Degree is 3-5 times of column volume of 55%-65% ethanol elution, obtains ethanol eluate, finally obtains Moringa with ethanol eluate recycling ethyl alcohol
Seed extracting solution.
5. a kind of tea-seed oil according to claim 1 or 2 is retained skin care suncream, which is characterized in that the flower extracts
Liquid the preparation method comprises the following steps: 4-6 parts of chrysanthemum, 2-4 parts of honeysuckle, 1-3 parts of Jasmine, 2-4 parts of violet are used clear water by weight
It rinses well, is added in pulverizer and crushes, 10-12 times of water is added to be heated to 90-100 degrees Celsius, decoct 2-4 hours, solid, liquid point
From；Residue after first time water is mentioned again add 8-10 times measure water carry out second of water mention, extract 1-3 hours, solid and liquid separation；Again
Residue after second of water is mentioned adds 4-6 times to measure water progress ultrasonic extraction, extracts 1-2 hours, merges extracting solution three times, is concentrated,
Up to flower extracting liquid.
6. a kind of tea-seed oil according to claim 1 or 2 is retained skin care suncream, which is characterized in that the water chestnut is extracted
Liquid is added in juice extractor the preparation method comprises the following steps: water chestnut is removed the peel, and pectase is added in juicing, controls temperature at 15 DEG C, stands 10-
16 hours, clear water chestnut juice is obtained, is concentrated under reduced pressure, then 1-3 DEG C of low-temperature preservation is spare.
7. a kind of tea-seed oil according to claim 1 or 2 is retained skin care suncream, which is characterized in that the thickening filler
The preparation method comprises the following steps: by attapulgite, bentonite, conch meal according to weight ratio 2: 1: 3 temperature be 480-520 DEG C at calcine 1-
2h, after cooling, ball milling crosses 100-200 mesh, after then impregnating 2-4h in the acetic acid solution of 8-10%, takes out, deionized water
To neutrality the sorbitan monooleate for being equivalent to diatom powder weight 2-4% is added, after mixing, drying is ground into nano powder in washing
End to get.
8. a kind of tea-seed oil according to claim 1 or 2 is retained skin care suncream, which is characterized in that the gluconate
The mixture formed for zinc gluconate, copper gluconate, managanese gluconate according to weight ratio 1: 3: 2；
The increasing property auxiliary agent is zinc sulfate, lysine, nano-titanium dioxide, methyl hydroxybenzoate according to again more mixed than 2: 1: 3: 1 composition
Close object.
9. a kind of method for preparing tea-seed oil water conservation skin care suncream as claimed in claim 1 or 2, which is characterized in that including
Following steps:
Step 1 weighs prepare each component raw material as required；
Step 2 after cleaning Folium Forsythia, aloe, Poria cocos with clear water, is sent into microtome, is then added to blanching 6- in boiling water
It 8 minutes, picks up to be sent into extruding-desiccation machine and removes moisture removal, be re-fed into crushing in pulverizer and obtain mixed-powder A；
Moringa seeds extracting solution, flower extracting liquid, water chestnut extracting solution, grape hydrochlorate are added in blender, are in temperature by step 3
At 40-50 DEG C, stir 10-20 minutes, speed of agitator 100-200r/min obtains mixed liquid B；
Exquisite tea-seed oil, jojoba butter, increasing property auxiliary agent are added in reaction kettle step 4, are 70-80 DEG C in temperature, stir 20-
30 minutes, the mix powder A of step 2 preparation is added, continues stirring 15-25 minutes, is cooling to 30-40 DEG C, step is added
The mixed liquid B and thickening filler of three preparations, continue stirring 5-15 minutes, obtain thick paste mixture C；
Step 5 the thick paste mixture C of step 4 preparation is added in homogenizer, homogenizer revolving speed 5500-7500r/min,
The homogenization 8-10min under 50-60 DEG C, the pressure of 18-22MPa, then the 10- that deaerates under 40-50 DEG C, 80-90kPa vacuum degree
12min, then ultra-high temperature sterilization 40-50 seconds at 130-150 DEG C, the tea-seed oil water conservation skin care invented after aseptic canning is sun-proof
Frost.
10. a kind of preparation method of tea-seed oil water conservation skin care suncream according to claim 9, which is characterized in that described
Step are as follows:
Step 1 weighs prepare each component raw material as required；
Step 2 after cleaning Folium Forsythia, aloe, Poria cocos with clear water, is sent into microtome, is then added to blanching 7 in boiling water
Minute, it picks up to be sent into extruding-desiccation machine and removes moisture removal, be re-fed into crushing in pulverizer and obtain mixed-powder A；
Moringa seeds extracting solution, flower extracting liquid, water chestnut extracting solution, grape hydrochlorate are added in blender, are in temperature by step 3
At 45 DEG C, stir 15 minutes, speed of agitator 150r/min obtains mixed liquid B；
Exquisite tea-seed oil, jojoba butter, increasing property auxiliary agent are added in reaction kettle step 4, are 75 DEG C in temperature, stir 25 points
The mix powder A of step 2 preparation is added in clock, continues stirring 20 minutes, is cooling to 35 DEG C, and the mixed of step 3 preparation is added
Liquid B and thickening filler are closed, continues stirring 10 minutes, obtains thick paste mixture C；
Step 5 the thick paste mixture C of step 4 preparation is added in homogenizer, homogenizer revolving speed 6500r/min, 55
DEG C, homogenization 9min under the pressure of 20MPa, then the 11min that deaerates under 45 DEG C, 85kPa vacuum degree, then the superelevation at 140 DEG C
Temperature sterilizing 45 seconds, the tea-seed oil water conservation skin care suncream invented after aseptic canning.
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| CN110897966A (en) * | 2020-01-09 | 2020-03-24 | 伊尔瑞生物科技(江苏)有限公司 | Sunscreen cream based on traditional Chinese medicine natural extract and beneficial to avoiding pore blockage |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108210435A (en) * | 2018-03-02 | 2018-06-29 | 合肥仙之峰农业科技有限公司 | It is a kind of to sterilize the acne green spot eliminating skin care suncream and preparation method thereof that disappears |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN108210435A (en) * | 2018-03-02 | 2018-06-29 | 合肥仙之峰农业科技有限公司 | It is a kind of to sterilize the acne green spot eliminating skin care suncream and preparation method thereof that disappears |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110897966A (en) * | 2020-01-09 | 2020-03-24 | 伊尔瑞生物科技(江苏)有限公司 | Sunscreen cream based on traditional Chinese medicine natural extract and beneficial to avoiding pore blockage |
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