CN103520280A - Healthcare litsea cubeba essential oil foot bath liquid and preparation method thereof - Google Patents
Healthcare litsea cubeba essential oil foot bath liquid and preparation method thereof Download PDFInfo
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- CN103520280A CN103520280A CN201310488988.6A CN201310488988A CN103520280A CN 103520280 A CN103520280 A CN 103520280A CN 201310488988 A CN201310488988 A CN 201310488988A CN 103520280 A CN103520280 A CN 103520280A
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Abstract
The invention discloses healthcare litsea cubeba essential oil foot bath liquid and a preparation method thereof, belonging to the technical field of foot bath liquid. The healthcare litsea cubeba essential oil foot bath liquid is technically characterized by being mainly prepared from the following raw materials in parts by weight: 3-15 parts of litsea cubeba essential oil, 1-8 parts of glycerin, 3-15 parts of an emulsifier and 60-100 parts of water; the preparation method comprises the following steps: (1) weighing the litsea cubeba essential oil and the emulsifier according to the formula amount, mixing the litsea cubeba essential oil and the emulsifier and uniformly stirring to obtain a solution A for standby application; (2) weighing water and glycerin according to the formula amount, mixing water and glycerin and uniformly stirring to obtain a solution B for standby application; (3) in a stirring state, heating the solution B to 38-55 DEG C, and dropwise adding the solution A into the solution B; and after the dropwise adding, continuously stirring for 20-30 minutes, and standing to obtain stable emulsion; and (4) sterilizing and separately packaging the stable emulsion. The invention aims at providing healthcare litsea cubeba essential oil foot bath liquid which is natural and non-toxic and has the functions of sterilization and disinfection and fungal infection prevention and is used for foot bath.
Description
Technical field
The present invention relates to a kind of health-care foot bath solution, more particularly, relate in particular to a kind of Fructus Litseae essential oil health-care foot bath solution.The invention still further relates to the preparation method of this foot bath liquid.
Background technology
Fructus Litseae essential oil (being conventionally called for short litsea cubeba oil) is the natural plant essential oils being obtained by vapor distillation by the grey seed in mountain, has pleasant citrus scented, and its main component is citral.Litsea cubeba oil have wide spectrum, efficient antifungic action, it has very strong inhibitory action to multiple mycetes such as penicillium, Candida albicans, Aspergillus niger, Aspergillus flavus, Aspergillus fumigatus, and the dermatophytosises such as acrothesium floccosum, trichophyton, alpha fungus, Sabouraudites lanosus are had to good insect killing effect.Litsea cubeba oil is a kind of natural medicinal plants of anti-fungal infection of rare high-efficiency low-toxicity.
Ten thousand power, Zhu Jingshan etc. are by setting up Murine Systemic Candidiasis model, observe mice median survival time after litsea cubeba oil effect, and have detected mouse kidney numbers of CFU.Result shows that litsea cubeba oil can obviously extend the median survival time of mice, reduces kidney numbers of CFU.Illustrate that Lisea Cubeba Oil on disseminated candidiasis of mice has therapeutical effect.
The employing trace liquid diluting methods such as Rong Li have been measured litsea cubeba oil the MIC value of 4 kinds of dermatophytosises (acrothesium floccosum, trichophyton, alpha fungus, Sabouraudites lanosus) have been to 312.5 μ g/ml, and with reference to MIC value, litsea cubeba oil is made to 3% cream, clinical practice is in the treatment of tinea pedis, total effective rate is up to 96%, especially evident in efficacy to vesicle, dipping erosive type tinea pedis, all cases are all without obvious adverse reaction.
No.1 Hospital Attached to Kunming Medical College has good curative effect using litsea cubeba oil as anti-candida infection medicine.The emerging grade of the Nie Chong of Ji'nan University, using litsea cubeba oil as primary raw material, has been prepared a kind of medicine for external use for the treatment of trichomonal vaginitis, and therapeutic effect is remarkable.
Above-mentioned document shows that litsea cubeba oil is a kind of natural drug with the anti-fungal infection of good DEVELOPMENT PROSPECT.
Domestic ten thousand people's foot fungus situations generaI investigations in 2002 find, closely the people of half has foot affliction, and fungal infection accounts for first place in foot dermatosis, and sickness rate is high, and with easy infection between toe, 79.01% is due to trichophyton; Secondly be Candida albicans, so the primary work of control foot dermatosis is prevent fungal infections.And use Fructus Litseae essential oil to carry out foot bath, just can reach the effect of good prevent fungal infections.
Foot bath is accepted extensively by people as a kind of leisure way of fashion, the foot bath of natural essence oil, and the project that foot bath industry especially is extremely praised highly, it has been generally acknowledged that quintessence oil foot bath has warm flesh internal organs, the effect of dredging the meridian reaches the effect of disease-relieving and physique enhancing.Can play allaying tiredness, the effect that profit is slept, also can remove the horn cell coming off in time, avoids advising the accumulation of raw horn cell, can prevent that foot is dry and cracked, callosity etc.Different quintessence oil foot baths, has different health-care effects, common are oil of ginger, lavandula angustifolia etc.But litsea cubeba oil is also rarely found in the application of foot bath industry, and it is different from the effect of the anti-fungal infection of other quintessence oils and is not paid attention to.
Use quintessence oil foot bath, in occupation mode, have for a long time certain mistaken ideas.Normally quintessence oil is directly added in hot water and carry out foot bath, quintessence oil is oil soluble material, can not be dissolved in equably in water, and it will swim on the water surface.If Fructus Litseae essential oil is kept afloat when foot bath, just can not reach the valid density for the treatment of, defence fungal infection.
Wuhan Inst. of Botany, Chinese Academy of Sciences shows in the patent of " litsea cubeba oil is being killed the ectozoal effect of people and animals ": litsea cubeba oil is nontoxic, and intact skin and eye are not had to stimulation; Damaged skin is had to slight stimulation, after stopping using, can automatically recover.Litsea cubeba oil is directly coated on damaged skin, and stimulation is slightly strong, but with insecticidal solution containing the reduction of litsea cubeba oil concentration, its stimulation reduces, and even disappears.
At present, in foot bath city, carry out more than quintessence oil foot bath, and that what adopt is the plants essential oils such as Fructus Citri Limoniae, lavandula angustifolia, Flos Rosae Rugosae is more, expensive because of it, also only have at present only a few people to enjoy.Fructus Litseae plants essential oil extracts with Fructus Litseae seed, and because Fructus Litseae seed is high containing quintessence oil rate, the extraction ratio of quintessence oil is high, so Fructus Litseae essential oil low price.If prepare foot bath liquid with it, can obtain cheap and good-quality product, it had both had pleasant citrus scented, had again the health-care effect of control foot dermatosis.Than the lemon type essential oil using at present, more there is the market competitiveness, be more suitable for mass consumption, be easier to promote.
Summary of the invention
The object of the present invention is to provide a kind of Nantural non-toxic, there is sterilizing, prevent fungal infections and can prevent and treat the Fructus Litseae essential oil health-care foot bath solution of foot dermatosis.
Another object of the present invention is to provide a kind of method of preparing above-mentioned health-care foot bath solution.
Last technical scheme of the present invention is achieved in that a kind of Fructus Litseae essential oil health-care foot bath solution, and it is that raw material by following weight parts is prepared from: 60～100 parts, 3～15 parts of Fructus Litseae essential oil, 1～8 part of glycerol, 3～15 parts of emulsifying agents and water.
In above-mentioned Fructus Litseae essential oil health-care foot bath solution, be that the raw material by following weight parts is prepared from: 70～90 parts, 3～10 parts of Fructus Litseae essential oil, 1～5 part of glycerol, 3～10 parts of emulsifying agents and water.
In above-mentioned Fructus Litseae essential oil health-care foot bath solution, described emulsifying agent is tween 80.
After of the present invention, a technical scheme is achieved in that a kind of method of preparing the Fructus Litseae essential oil health-care foot bath solution described in above-mentioned arbitrary claim, it is characterized in that, the method comprises the steps: that (1) takes Fructus Litseae essential oil and emulsifying agent by formula ratio, by both mixing and stirring, obtain solution A, stand-by; (2) by formula ratio, take water, glycerol, by both mixing and stirring, obtain solution B, stand-by; (3) under stirring, solution B is heated to 38～55 ℃, then keep stirring that solution A is dropped in solution B, drip off rear continuation and stir 20～30 minutes, standing, obtain stable emulsion; (4) stable emulsion is carried out to sterilizing, packing, obtain Fructus Litseae essential oil health-care foot bath solution.
In the method for above-mentioned Fructus Litseae essential oil health-care foot bath solution, the heating-up temperature of the solution B that step (3) is described is 40～50 ℃.
In the method for above-mentioned Fructus Litseae essential oil health-care foot bath solution, the described time of repose of step (3) is 24 hours.
The present invention be take Fructus Litseae essential oil as primary raw material, add a small amount of nontoxic additive, by it, composite for Fructus Litseae essential oil content is 3%～10%, stable emulsion---be Fructus Litseae essential oil health-care foot bath solution, this Fructus Litseae essential oil foot bath liquid has dispersive property preferably in water.When foot bath is used, use amount is only 2～5mL, and Fructus Litseae essential oil can be evenly distributed in the water of foot bath, reaches the valid density of sterilization, defence fungal infection, and pedal skin is not had to stimulation, thereby reach the effect of control foot dermatosis.
The collocation of the present invention formula, makes every effort to make the stable emulsion of high concentration Fructus Litseae essential oil, and foot bath liquid, is allowed to condition at while using, and Fructus Litseae essential oil can be dispersed in water uniformly, reaches effective bacteriocidal concentration, has significant health-care effect.This formula is compared with other bath lotion, its essential oil content is other bath lotion tens times.
The specific embodiment
Below in conjunction with specific embodiment, the present invention is described in further detail, but do not form any limitation of the invention.
A kind of Fructus Litseae essential oil health-care foot bath solution of the present invention, it is that raw material by following weight parts is prepared from: 60～100 parts, 3～15 parts of Fructus Litseae essential oil, 1～8 part of glycerol, 3～15 parts of emulsifying agents and water.Preferably, it is that raw material by following weight parts is prepared from: 70～90 parts, 3～10 parts of Fructus Litseae essential oil, 1～5 part of glycerol, 3～10 parts of emulsifying agents and water.Wherein, described emulsifying agent is preferably tween 80.Tween 80 is nonionic surfactant, little to skin irritation, nontoxic, has minimum haemolysis and the strongest emulsification in tween series.The more important thing is that the present invention shows through many experiments: tween 80 can make to be dissolved in water liquid after Fructus Litseae essential oil emulsifying, plays a role completely.Certainly, select different surfactants to make emulsifying agent, also can make to be dissolved in water liquid after Fructus Litseae essential oil emulsifying, just effect can be weak.
The method of a kind of Fructus Litseae essential oil health-care foot bath solution of the present invention, the method comprises the steps:
(1) by formula ratio, take Fructus Litseae essential oil and emulsifying agent, by both mixing and stirring, obtain solution A, stand-by;
(2) by formula ratio, take water, glycerol, by both mixing and stirring, obtain solution B, stand-by;
(3) under stirring, solution B is heated to 38～55 ℃, being preferably heating-up temperature is 40～50 ℃, then keeps stirring that solution A is dropped in solution B, drips off rear continuation and stirs 20～30 minutes, standing 24 hours, obtains stable emulsion; Suitable heating, is in order to form the stable emulsion of high concentration Fructus Litseae essential oil, and this emulsion adds in foot-immersing water, and Fructus Litseae essential oil can disperse uniformly;
(4) stable emulsion is carried out to sterilizing, packing, obtain Fructus Litseae essential oil health-care foot bath solution.
Embodiment 1
Formula: Fructus Litseae essential oil 3kg, glycerol 1kg, emulsifying agent 3kg, water 60kg.
Preparation method: (1) takes Fructus Litseae essential oil and emulsifying agent by formula ratio, by both mixing and stirring, obtains solution A, stand-by; (2) by formula ratio, take water, glycerol, by both mixing and stirring, obtain solution B, stand-by; (3) under stirring, solution B is heated to 38 ℃, then keep stirring that solution A is dropped in solution B, drip off rear continuation and stir 20～30 minutes, standing 24 hours, obtain stable emulsion; (4) stable emulsion is carried out to sterilizing, packing, obtain Fructus Litseae essential oil health-care foot bath solution.
Embodiment 2
Formula: Fructus Litseae essential oil 3kg, glycerol 1kg, emulsifying agent 3kg, water 70kg.
Preparation method: (1) takes Fructus Litseae essential oil and emulsifying agent by formula ratio, by both mixing and stirring, obtains solution A, stand-by; (2) by formula ratio, take water, glycerol, by both mixing and stirring, obtain solution B, stand-by; (3) under stirring, solution B is heated to 40 ℃, then keep stirring that solution A is dropped in solution B, drip off rear continuation and stir 20～30 minutes, standing 24 hours, obtain stable emulsion; (4) stable emulsion is carried out to sterilizing, packing, obtain Fructus Litseae essential oil health-care foot bath solution.
Embodiment 3
Formula: Fructus Litseae essential oil 6kg, glycerol 3kg, emulsifying agent 6kg, water 80kg.
Preparation method: (1) takes Fructus Litseae essential oil and emulsifying agent by formula ratio, by both mixing and stirring, obtains solution A, stand-by; (2) by formula ratio, take water, glycerol, by both mixing and stirring, obtain solution B, stand-by; (3) under stirring, solution B is heated to 45 ℃, then keep stirring that solution A is dropped in solution B, drip off rear continuation and stir 20～30 minutes, standing 24 hours, obtain stable emulsion; (4) stable emulsion is carried out to sterilizing, packing, obtain Fructus Litseae essential oil health-care foot bath solution.
Embodiment 4
Formula: Fructus Litseae essential oil 10kg, glycerol 5kg, emulsifying agent 10kg, water 90kg.
Preparation method: (1) takes Fructus Litseae essential oil and emulsifying agent by formula ratio, by both mixing and stirring, obtains solution A, stand-by; (2) by formula ratio, take water, glycerol, by both mixing and stirring, obtain solution B, stand-by; (3) under stirring, solution B is heated to 50 ℃, then keep stirring that solution A is dropped in solution B, drip off rear continuation and stir 20～30 minutes, standing 24 hours, obtain stable emulsion; (4) stable emulsion is carried out to sterilizing, packing, obtain Fructus Litseae essential oil health-care foot bath solution.
Embodiment 5
Formula: Fructus Litseae essential oil 15kg, glycerol 8kg, emulsifying agent 15kg, water 100kg.
Preparation method: (1) takes Fructus Litseae essential oil and emulsifying agent by formula ratio, by both mixing and stirring, obtains solution A, stand-by; (2) by formula ratio, take water, glycerol, by both mixing and stirring, obtain solution B, stand-by; (3) under stirring, solution B is heated to 55 ℃, then keep stirring that solution A is dropped in solution B, drip off rear continuation and stir 20～30 minutes, standing 24 hours, obtain stable emulsion; (4) stable emulsion is carried out to sterilizing, packing, obtain Fructus Litseae essential oil health-care foot bath solution.
The present invention tests the antibiotic property of the prepared Fructus Litseae essential oil health-care foot bath solution of embodiment 1, dispersibility in water, and its result is as follows:
1. microbiological test and result
First, two kinds of mycetes activation culture in potato dextrose agar (PDA) culture medium, then two kinds of mycetes of picking embrace sub-supending (10 respectively
5individual armful of son/mL must be used in 24h).Get Fructus Litseae essential oil health-care foot bath solution and be respectively 0.4mL, 0.8mL, 1.2mL, 1.6mL, 2mL and in 25mL volumetric flask, use distilled water standardize solution, standby.
With aseptic straw, draw each 1mL of Fructus Litseae essential oil health-care foot bath solution serial dilutions, inject respectively sterile petri dish.After potato sucrose medium sterilization, be cooled to 50 ℃ of left and right, then measure respectively 15mL with graduated cylinder, in impouring sterile petri dish, fully mix also cooling.After solidifying, add 0.1mL bacteria suspension, with spreading rod coating evenly.Cover plate lid, be placed in calorstat, observe fungus growth situation (three plates of every kind of parallel work of situation) cultivate 48h at 28 ℃ ± 1 ℃ after; With three plates, do blank experiment simultaneously.Its result of the test is as table 1:
The antibacterial result of table 1 Fructus Litseae essential oil health-care foot bath solution to mycete
As can be seen from Table 1, adopt the prepared Fructus Litseae essential oil health-care foot bath solution of the present invention to there is significant inhibition to the growth of several typical mycetes.
2. dispersivity test and result
The present invention to the prepared Fructus Litseae essential oil health-care foot bath solution of embodiment 1 dispersibility in water test, dispersion effect uses the oil content in the water in different depth (upper, middle and lower layer) to characterize.Concrete testing program is: get the separatory funnel of two 250mL, respectively add 100mL water.One merely hits adds 0.1g litsea cubeba oil, another to add Fructus Litseae essential oil health-care foot bath solution 2mL(made in above-described embodiment approximately containing Fructus Litseae essential oil 0.1g), shake well, standing.Observe the deployment conditions of Fructus Litseae essential oil in two separatory funnels, record.Then from separatory funnel, take successively respectively 40mL solution (lower floor), 30mL solution (middle level) in different conical flasks, remaining solution 30mL(upper strata) from separatory funnel is suitable for reading, pour into another conical flask.Measure the content of different layers solution Fructus Litseae essential oil.During mensuration, after shake well, sample immediately.Result of the test is in Table 2
The deployment conditions of table 2 Fructus Litseae essential oil in water
As can be seen from Table 2, the Fructus Litseae essential oil health-care foot bath solution that the present invention prepares has dispersive property preferably in water.During actual use, its amount that adds water is 10 times of left and right of above-mentioned experiment.During foot bath, get foot bath liquid 2～5mL of the present invention, add 5L water, Fructus Litseae essential oil can be evenly distributed in water, can reach > concentration of effective sterilization of 0.1mg/mL, defence fungal infection.
Claims (6)
1. a Fructus Litseae essential oil health-care foot bath solution, is characterized in that, is that the raw material by following weight parts is prepared from: 60～100 parts, 3～15 parts of Fructus Litseae essential oil, 1～8 part of glycerol, 3～15 parts of emulsifying agents and water.
2. a kind of Fructus Litseae essential oil health-care foot bath solution according to claim 1, is characterized in that, is that the raw material by following weight parts is prepared from: 70～90 parts, 3～10 parts of Fructus Litseae essential oil, 1～5 part of glycerol, 3～10 parts of emulsifying agents and water.
3. Fructus Litseae essential oil health-care foot bath solution according to claim 1 and 2, is characterized in that, described emulsifying agent is tween 80.
4. a method of preparing the Fructus Litseae essential oil health-care foot bath solution described in above-mentioned arbitrary claim, is characterized in that, the method comprises the steps: that (1) takes Fructus Litseae essential oil and emulsifying agent by formula ratio, by both mixing and stirring, obtains solution A, stand-by; (2) by formula ratio, take water, glycerol, by both mixing and stirring, obtain solution B, stand-by; (3) under stirring, solution B is heated to 38～55 ℃, then keep stirring that solution A is dropped in solution B, drip off rear continuation and stir 20～30 minutes, standing, obtain stable emulsion; (4) stable emulsion is carried out to sterilizing, packing, obtain Fructus Litseae essential oil health-care foot bath solution.
5. the method for Fructus Litseae essential oil health-care foot bath solution according to claim 4, is characterized in that, the heating-up temperature of the solution B that step (3) is described is 40～50 ℃.
6. the method for Fructus Litseae essential oil health-care foot bath solution according to claim 4, is characterized in that, the described time of repose of step (3) is 24 hours.
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104562661A (en) * | 2014-12-23 | 2015-04-29 | 常熟市中宏针织厂 | Cotton and linen fabric finishing process |
| CN108034501A (en) * | 2017-12-30 | 2018-05-15 | 刘莹艳 | A kind of essential oil gel and preparation method thereof |
| CN113813304A (en) * | 2020-06-18 | 2021-12-21 | 陈信行 | Humic acid litsea cubeba compound and preparation process thereof |
| CN114504061A (en) * | 2022-03-17 | 2022-05-17 | 嘉应学院 | Chicken feed additive and preparation method and application thereof |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1064590A (en) * | 1992-03-30 | 1992-09-23 | 王金定 | The 4th generation vegetable germicide for agriculture |
| CN1561954A (en) * | 2004-04-22 | 2005-01-12 | 上海交通大学 | Skin external sterilizer |
-
2013
- 2013-10-17 CN CN201310488988.6A patent/CN103520280B/en not_active Expired - Fee Related
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1064590A (en) * | 1992-03-30 | 1992-09-23 | 王金定 | The 4th generation vegetable germicide for agriculture |
| CN1561954A (en) * | 2004-04-22 | 2005-01-12 | 上海交通大学 | Skin external sterilizer |
Non-Patent Citations (3)
| Title |
|---|
| 翟洪民: "防病健身话足浴", 《农业知识》, 31 December 2005 (2005-12-31), pages 55 * |
| 顾仁勇等: "山苍子精油抑菌及抗氧化作用的研究", 《食品科学》, vol. 27, no. 11, 31 December 2006 (2006-12-31), pages 86 - 89 * |
| 高辉华等: "山苍子精油杀菌谱及其制剂稳定性的研究", 《华中农业大学学报》, vol. 8, no. 4, 31 December 1989 (1989-12-31), pages 338 - 341 * |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104562661A (en) * | 2014-12-23 | 2015-04-29 | 常熟市中宏针织厂 | Cotton and linen fabric finishing process |
| CN108034501A (en) * | 2017-12-30 | 2018-05-15 | 刘莹艳 | A kind of essential oil gel and preparation method thereof |
| CN113813304A (en) * | 2020-06-18 | 2021-12-21 | 陈信行 | Humic acid litsea cubeba compound and preparation process thereof |
| CN114504061A (en) * | 2022-03-17 | 2022-05-17 | 嘉应学院 | Chicken feed additive and preparation method and application thereof |
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