CN103519318A - Antioxidant - Google Patents
Antioxidant Download PDFInfo
- Publication number
- CN103519318A CN103519318A CN201310512827.6A CN201310512827A CN103519318A CN 103519318 A CN103519318 A CN 103519318A CN 201310512827 A CN201310512827 A CN 201310512827A CN 103519318 A CN103519318 A CN 103519318A
- Authority
- CN
- China
- Prior art keywords
- parts
- antioxidant
- concentrated
- absolute ethyl
- rosemary
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
- 239000003963 antioxidant agent Substances 0.000 title claims abstract description 20
- 230000003078 antioxidant effect Effects 0.000 title claims abstract description 20
- 241000196324 Embryophyta Species 0.000 claims abstract description 8
- 235000014360 Punica granatum Nutrition 0.000 claims abstract description 8
- 244000178231 Rosmarinus officinalis Species 0.000 claims abstract description 8
- 239000002994 raw material Substances 0.000 claims abstract description 7
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 30
- HEDRZPFGACZZDS-UHFFFAOYSA-N Chloroform Chemical compound ClC(Cl)Cl HEDRZPFGACZZDS-UHFFFAOYSA-N 0.000 claims description 10
- 239000008236 heating water Substances 0.000 claims description 10
- 241000245240 Lonicera Species 0.000 claims description 7
- 241000219991 Lythraceae Species 0.000 claims description 7
- 235000009569 green tea Nutrition 0.000 claims description 7
- 238000004821 distillation Methods 0.000 claims description 5
- 235000019441 ethanol Nutrition 0.000 claims description 5
- 239000000706 filtrate Substances 0.000 claims description 5
- 238000010438 heat treatment Methods 0.000 claims description 5
- 238000000643 oven drying Methods 0.000 claims description 5
- 239000000843 powder Substances 0.000 claims description 5
- 238000002360 preparation method Methods 0.000 claims description 5
- 238000011084 recovery Methods 0.000 claims description 5
- 238000010992 reflux Methods 0.000 claims description 5
- 238000010898 silica gel chromatography Methods 0.000 claims description 5
- 239000007787 solid Substances 0.000 claims description 5
- 238000003756 stirring Methods 0.000 claims description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 5
- 244000167230 Lonicera japonica Species 0.000 abstract 1
- 235000017617 Lonicera japonica Nutrition 0.000 abstract 1
- 244000294611 Punica granatum Species 0.000 abstract 1
- 235000013305 food Nutrition 0.000 description 3
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000002537 cosmetic Substances 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000003203 everyday effect Effects 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L3/00—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs
- A23L3/34—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals
- A23L3/3454—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals in the form of liquids or solids
- A23L3/3463—Organic compounds; Microorganisms; Enzymes
- A23L3/3472—Compounds of undetermined constitution obtained from animals or plants
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Abstract
The invention discloses an antioxidant, which comprises the following components in parts by weight: 20 to 25 parts of green tealeaf, 10 to 16 parts of rosemary plant, 20 to 26 parts of lonicera japonica and 10 to 15 parts of pomegranate seed. The antioxidant is prepared from natural and readily-available raw materials according to a reasonable proportion, and is wide in application range.
Description
Technical field
The present invention relates to a kind of cosmetics of everyday use, be specifically related to a kind of antioxidant.
Background technology
Antioxidant is to stop or postpone Food Oxidation after making an addition to food, improves the stability and the material that extends storage period of food quality, and it is artificial synthetic that the antioxidant in market mostly is.
Summary of the invention
Goal of the invention: in order to overcome the deficiencies in the prior art, the object of this invention is to provide a kind of antioxidant.
Technical scheme: a kind of antioxidant of the present invention, comprises following component according to parts by weight: 20～25 parts of green teas, 10～16 parts of rosemary, Xue MingRosma rinus officinalis plant, 20～26 parts of honeysuckles, 10～15 parts of seed of pomegranate.
As preferably, 21～24.5 parts of described green teas, 11.5～14.5 parts of rosemary, Xue MingRosma rinus officinalis plant, 22～25.5 parts of honeysuckles, 11.5～14.5 parts of seed of pomegranate.
The preparation method of a kind of antioxidant of the present invention, comprises the steps:
(1) each component of extracting is by weight pulverized, then added 6 times to the absolute ethyl alcohol of raw material volume, stir and soak after 60min with the heating water bath 50min that refluxes, filter after being cooled to room temperature;
(2) gained filtrate water in above-mentioned steps is bathed to heating Distillation recovery ethanol, be concentrated into dark brown solid and occurred position, move into oven drying;
(3) the dry thing of gained in step (2) is ground as powder, add the anhydrous alcohol solution of 8 times of amounts, by silica gel column chromatography, first use chloroform give mobile phase, the rear absolute ethyl alcohol wash-out of using, collects brown efflux, concentrated, dry with heating water bath.
Beneficial effect: a kind of antioxidant of the present invention, raw material is natural to be easy to get, reasonable mixture ratio applied range.
The specific embodiment
Below in conjunction with embodiment, the present invention is further described.
Embodiment 1:
A kind of antioxidant of the present invention, comprises following component according to parts by weight; 21 parts of green teas, 11.5 parts of rosemary, Xue MingRosma rinus officinalis plant, 22 parts of honeysuckles, 11.5 parts of seed of pomegranate.
A preparation method for antioxidant, comprises the steps:
(1) each component of extracting is by weight pulverized, then added 6 times to the absolute ethyl alcohol of raw material volume, stir and soak after 60min with the heating water bath 50min that refluxes, filter after being cooled to room temperature;
(2) gained filtrate water in above-mentioned steps is bathed to heating Distillation recovery ethanol, be concentrated into dark brown solid and occurred position, move into oven drying;
(3) the dry thing of gained in step (2) is ground as powder, add the anhydrous alcohol solution of 8 times of amounts, by silica gel column chromatography, first use chloroform give mobile phase, the rear absolute ethyl alcohol wash-out of using, collects brown efflux, concentrated, dry with heating water bath.
Embodiment 2:
A kind of antioxidant of the present invention, comprises following component according to parts by weight; 4.5 parts of green teas, 14.5 parts of rosemary, Xue MingRosma rinus officinalis plant, 25.5 parts of honeysuckles, 14.5 parts of seed of pomegranate.
A preparation method for antioxidant, is characterized in that comprising the steps:
(1) each component of extracting is by weight pulverized, then added 6 times to the absolute ethyl alcohol of raw material volume, stir and soak after 60min with the heating water bath 50min that refluxes, filter after being cooled to room temperature;
(2) gained filtrate water in above-mentioned steps is bathed to heating Distillation recovery ethanol, be concentrated into dark brown solid and occurred position, move into oven drying;
(3) the dry thing of gained in step (2) is ground as powder, add the anhydrous alcohol solution of 8 times of amounts, by silica gel column chromatography, first use chloroform give mobile phase, the rear absolute ethyl alcohol wash-out of using, collects brown efflux, concentrated, dry with heating water bath.
Embodiment 3:
A kind of antioxidant of the present invention, comprises following component according to parts by weight; 23 parts of green teas, 12 parts of rosemary, Xue MingRosma rinus officinalis plant, 22.5 parts of honeysuckles, 12.5 parts of seed of pomegranate.
The preparation method of a kind of antioxidant of the present invention, comprises the steps:
(1) each component of extracting is by weight pulverized, then added 6 times to the absolute ethyl alcohol of raw material volume, stir and soak after 60min with the heating water bath 50min that refluxes, filter after being cooled to room temperature;
(2) gained filtrate water in above-mentioned steps is bathed to heating Distillation recovery ethanol, be concentrated into dark brown solid and occurred position, move into oven drying;
(3) the dry thing of gained in step (2) is ground as powder, add the anhydrous alcohol solution of 8 times of amounts, by silica gel column chromatography, first use chloroform give mobile phase, the rear absolute ethyl alcohol wash-out of using, collects brown efflux, concentrated, dry with heating water bath.
The above is only the preferred embodiment of the present invention; be noted that for those skilled in the art; under the premise without departing from the principles of the invention, can also make some improvements and modifications, these improvements and modifications also should be considered as protection scope of the present invention.
Claims (3)
1. an antioxidant, is characterized in that comprising following component according to parts by weight: 20～25 parts of green teas, 10～16 parts of rosemary, Xue MingRosma rinus officinalis plant, 20～26 parts of honeysuckles, 10～15 parts of seed of pomegranate.
2. antioxidant according to claim 1, is characterized in that: 21～24.5 parts of described green teas, 11.5～14.5 parts of rosemary, Xue MingRosma rinus officinalis plant, 22～25.5 parts of honeysuckles, 11.5～14.5 parts of seed of pomegranate.
3. a preparation method for the antioxidant based on described in claim 1 or 2 any one, is characterized in that comprising the steps:
(1) each component of extracting is by weight pulverized, then added 6 times to the absolute ethyl alcohol of raw material volume, stir and soak after 60min with the heating water bath 50min that refluxes, filter after being cooled to room temperature;
(2) gained filtrate water in above-mentioned steps is bathed to heating Distillation recovery ethanol, be concentrated into dark brown solid and occurred position, move into oven drying;
(3) the dry thing of gained in step (2) is ground as powder, add the anhydrous alcohol solution of 8 times of amounts, by silica gel column chromatography, first use chloroform give mobile phase, the rear absolute ethyl alcohol wash-out of using, collects brown efflux, concentrated, dry with heating water bath.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310512827.6A CN103519318A (en) | 2013-10-25 | 2013-10-25 | Antioxidant |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310512827.6A CN103519318A (en) | 2013-10-25 | 2013-10-25 | Antioxidant |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN103519318A true CN103519318A (en) | 2014-01-22 |
Family
ID=49921953
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201310512827.6A Withdrawn CN103519318A (en) | 2013-10-25 | 2013-10-25 | Antioxidant |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN103519318A (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104172432A (en) * | 2014-07-30 | 2014-12-03 | 谢松芬 | Passion fruit seed oil antioxidant |
| CN104323397A (en) * | 2014-10-14 | 2015-02-04 | 合肥庭索环保材料有限公司 | Exterior wall coating antioxidant |
| CN104397827A (en) * | 2014-12-04 | 2015-03-11 | 梁亨 | Preparation method of food antioxidant |
| CN104856188A (en) * | 2015-04-25 | 2015-08-26 | 安徽蜂献蜂业有限公司 | Natural honey antioxidant and preparation method thereof |
-
2013
- 2013-10-25 CN CN201310512827.6A patent/CN103519318A/en not_active Withdrawn
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104172432A (en) * | 2014-07-30 | 2014-12-03 | 谢松芬 | Passion fruit seed oil antioxidant |
| CN104323397A (en) * | 2014-10-14 | 2015-02-04 | 合肥庭索环保材料有限公司 | Exterior wall coating antioxidant |
| CN104397827A (en) * | 2014-12-04 | 2015-03-11 | 梁亨 | Preparation method of food antioxidant |
| CN104856188A (en) * | 2015-04-25 | 2015-08-26 | 安徽蜂献蜂业有限公司 | Natural honey antioxidant and preparation method thereof |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C04 | Withdrawal of patent application after publication (patent law 2001) | ||
| WW01 | Invention patent application withdrawn after publication |
Application publication date: 20140122 |