CN103505473A - Preparation method of deer blood powder - Google Patents
Preparation method of deer blood powder Download PDFInfo
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- CN103505473A CN103505473A CN201310480746.2A CN201310480746A CN103505473A CN 103505473 A CN103505473 A CN 103505473A CN 201310480746 A CN201310480746 A CN 201310480746A CN 103505473 A CN103505473 A CN 103505473A
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- deer blood
- sanguis cervi
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Abstract
The invention discloses a preparation method of deer blood powder. The preparation method comprises the following steps: using ethyl alcohol with concentration of 40% to warmly soak fresh deer blood, carrying out reflux extraction for several times, deproteinizing the deer blood with ethyl alcohol with concentration of 95% for three times, condensing the deproteinized blood, and carrying out spray drying to obtain the deer blood powder. The preparation method has the active effect of effectively separating out macromolecules such as flocculating protein generated from the collected deer blood. The obtained deer blood powder can be used for producing deer blood wine and deer blood oral liquid with bright color, which is not easy to generate sediment, reduce the risk of damage to effective components due to high temperature, effectively retain the components in the deer blood, and prolong the useful life of the deer blood powder. The technological process is simple; the extraction efficiency is high; the production cost is low; the preparation method is free from environment pollution; the method is suitable for industrialized production.
Description
Technical field
The invention belongs to pharmaceutical field, be specifically related to a kind of preparation of Sanguis cervi powder.
Background technology
Sanguis cervi refers to the blood of Cervidae Cervus nippon Temminck or Cervus elaphus linnaeus, is famous and precious simply Chinese medicine.Its sweet-salty, hot in nature, enter Liver and kidney two warps, have the benefit essence of nourishing blood, promoting the circulation of blood to dispel effect that paralysis, detumescence cure the wound.Curing mainly deficient lumbago, cardiopalmus, insomnia, lung spits blood repeatly; Metrorrhagia, leukorrhagia.
In recent years, along with the progress of modern medicine level and scientific and technological development, more and more deep to the research of the aspects such as the chemical composition of Sanguis cervi and pharmacological action thereof, field of health care food has not been limited in the application of Sanguis cervi.It is little that the product that the Sanguis cervi of take is development of raw materials has good amount, and market prospect is wide.But due to the limitation of Sanguis cervi resource, and its development is more single, only limit to the utilization of former blood and processing deep development and underutilization; Restriction on Zai You region, it is also limited that deer class is raised and train the development scale quantity of industry, makes its utilization and exploitation add to the difficulties.
At present, the many folk prescriptions of Sanguis cervi or compound recipe are prepared into various deer-blood wines, and it is that Raw material processing becomes capsule or tablet that portioned product is selected Sanguis cervi powder, cannot meet the need of market.Common Sanguis cervi powder preparation method is bake drying method, and this kind of preparation method, because temperature in the course of processing is high, makes the functional component loss of Sanguis cervi or destroy.Loss effective ingredient in Sanguis cervi being caused for fear of bake drying method, freeze-drying replaces oven drying method gradually.Adopt frozen drying legal system to be to preserve to greatest extent the nutritional labeling in raw material for the advantage of Sanguis cervi powder, especially to processing this class thermal sensitivity raw material of blood product, more can fully demonstrate its value.Adopt Freeze Drying Technique product cost expensive, drying time is longer.Storage test also shows, its good quality of freeze-dried food can not be lasting, and the change of quality also easily occurs in storage.
The present invention has used for reference traditional blood store method, in blood, add a certain amount of ethanol, by ethanol, carry out most nutrient substance in solidificating blood, and by reflux, extract, repeatedly, the effective ingredient in blood is diffused in ethanol and water to greatest extent, and processes by deproteinization, by gathering the wadding egg collection generating in Sanguis cervi, effectively separate in vain, utilize spray-dired method, can shorten the dry time, reduce the risk that high temperature destroys effective ingredient.Processed of the present invention is simple, and effectively production control cost, has effectively retained composition in Sanguis cervi in addition, can extend again the effect duration of Sanguis cervi powder.In addition, the Sanguis cervi powder that adopts the present invention to extract is prepared deer-blood wine, Sanguis cervi oral liquid color is vivid, is difficult for producing precipitation.The extensive use that the present invention can be Sanguis cervi lays the foundation.
Summary of the invention
The preparation method that the object of this invention is to provide a kind of Sanguis cervi powder, overcomes the aforementioned deficiency that existing oven drying method and lyophilization exist.
The inventive method comprises the following steps:
1, bright Sanguis cervi adds 6 times of volumes of ethanol of 40% concentration, and under 40-50 ℃ of condition, warm macerating is 12 hours, is heated to 100 ℃ and starts timing, and reflux, extract, 3 hours, filters.
2, in the filtrate of step 1 gained, add the alcohol heating reflux of 40% concentration to extract secondary, all after being heated to 100 ℃, start timing respectively, add for the first time 5 times of volumes of step 1 bright Sanguis cervi used, extract 3 hours, add for the second time 4 times of volumes of step 1 bright Sanguis cervi used, extract 2 hours, filter, the filtrate that merges extracted twice, reclaims ethanol, and is concentrated into 1/2 of former Sanguis cervi amount.
3, to the ethanol deproteinization 3 times that adds successively 5,6,7 times of amount 95% concentration of concentrated solution volume in the concentrated solution of step 2 gained, each standing 24 hours, reclaim ethanol, medicinal liquid is concentrated into 1/4 of former Sanguis cervi total amount, the spray-dried rear acquisition Sanguis cervi powder of concentrated solution.
The present invention and existing method comparison, have following advantage:
The present invention has used for reference traditional blood store method, in blood, add a certain amount of ethanol, by ethanol, carry out most nutrient substance in solidificating blood, and by reflux, extract, repeatedly, the effective ingredient in blood is diffused in ethanol and water to greatest extent.In Sanguis cervi powder preparation process, with 5,6,7 times, measure ethanol deproteinization 3 times successively, can effectively by gathering the wadding egg collection generating in Sanguis cervi, wait in vain macromole effectively to separate.The Sanguis cervi powder that adopts the present invention's processing, the deer-blood wine of production and Sanguis cervi oral liquid solution colour are vivid, are difficult for producing precipitation.Utilize spray-dired method, can shorten the time of high temperature drying, reduce the risk that high temperature destroys effective ingredient, effectively retained composition in Sanguis cervi, can extend again the effect duration of Sanguis cervi powder.Technological process of the present invention is simple, extraction efficiency is high, production cost is low, non-environmental-pollution, is suitable for commercial production.
the specific embodiment
It is 40% ethanol 6L that 1L Sanguis cervi is added to concentration, and under 45 ℃ of conditions, warm macerating is 12 hours, is heated to 100 ℃ and starts timing, refluxes 3 hours, filters.In filtrate, add the alcohol heating reflux of 40% concentration to extract secondary again, all after being heated to 100 ℃, start timing respectively, add for the first time 5L, extract 3 hours, add for the second time 4L, extract 2 hours, filter, the filtrate that merges extracted twice, reclaims ethanol, and is concentrated into 0.5L.To the ethanol deproteinization 3 times that adds successively 2.5L, 3L, 3.5L concentration 95% in gained concentrated solution, each standing 24 hours, reclaim ethanol, be concentrated into 0.25L, after concentrated solution is spray-dried, can obtain 160g left and right Sanguis cervi powder.
Claims (1)
1. a preparation method for Sanguis cervi powder, is characterized in that:
(1) bright Sanguis cervi adds 6 times of volumes of ethanol of 40% concentration, and under 40 ~ 50 ℃ of conditions, warm macerating is 12 hours, is heated to 100 ℃ and starts timing, and reflux, extract, 3 hours, filters;
(2) in the filtrate of step (1) gained, add the alcohol heating reflux of 40% concentration to extract secondary, all after being heated to 100 ℃, start timing respectively, add for the first time 5 times of volumes of step (1) bright Sanguis cervi used, extract 3 hours, add for the second time 4 times of volumes of step (1) bright Sanguis cervi used, extract 2 hours, filter, the filtrate that merges extracted twice, reclaims ethanol, and is concentrated into 1/2 of former Sanguis cervi amount;
(3) to the ethanol deproteinization 3 times that adds successively 5,6,7 times of amount 95% concentration of concentrated solution volume in the concentrated solution of step (2) gained, each standing 24 hours, reclaim ethanol, medicinal liquid is concentrated into 1/4 of former Sanguis cervi total amount, the spray-dried rear acquisition Sanguis cervi powder of concentrated solution.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310480746.2A CN103505473A (en) | 2013-10-15 | 2013-10-15 | Preparation method of deer blood powder |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310480746.2A CN103505473A (en) | 2013-10-15 | 2013-10-15 | Preparation method of deer blood powder |
Publications (1)
| Publication Number | Publication Date |
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| CN103505473A true CN103505473A (en) | 2014-01-15 |
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| CN201310480746.2A Pending CN103505473A (en) | 2013-10-15 | 2013-10-15 | Preparation method of deer blood powder |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106359791A (en) * | 2016-08-29 | 2017-02-01 | 云南天佑熊业制药有限公司 | Deer blood tableted candy and production method thereof |
| CN107048323A (en) * | 2017-04-07 | 2017-08-18 | 江西莲花血鸭农业发展有限公司 | Duck blood powder and preparation method thereof |
| CN109331038A (en) * | 2018-08-24 | 2019-02-15 | 苏州红冠庄国药股份有限公司 | A kind of production technology of deer haemin and its preparation method of health care product |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101332243A (en) * | 2008-07-23 | 2008-12-31 | 黄涛 | Zigui jujube deer blood capsule capable of enriching blood and replenishing qi |
-
2013
- 2013-10-15 CN CN201310480746.2A patent/CN103505473A/en active Pending
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101332243A (en) * | 2008-07-23 | 2008-12-31 | 黄涛 | Zigui jujube deer blood capsule capable of enriching blood and replenishing qi |
Non-Patent Citations (1)
| Title |
|---|
| 陈晓燕等: "鹿血酒加工工艺研究", 《四川农业大学学报》 * |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106359791A (en) * | 2016-08-29 | 2017-02-01 | 云南天佑熊业制药有限公司 | Deer blood tableted candy and production method thereof |
| CN107048323A (en) * | 2017-04-07 | 2017-08-18 | 江西莲花血鸭农业发展有限公司 | Duck blood powder and preparation method thereof |
| CN109331038A (en) * | 2018-08-24 | 2019-02-15 | 苏州红冠庄国药股份有限公司 | A kind of production technology of deer haemin and its preparation method of health care product |
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| C05 | Deemed withdrawal (patent law before 1993) | ||
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Application publication date: 20140115 |