CN103469577B - Stiffening agent used for crease finishing of jean clothes - Google Patents
Stiffening agent used for crease finishing of jean clothes Download PDFInfo
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- CN103469577B CN103469577B CN201310464023.3A CN201310464023A CN103469577B CN 103469577 B CN103469577 B CN 103469577B CN 201310464023 A CN201310464023 A CN 201310464023A CN 103469577 B CN103469577 B CN 103469577B
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Abstract
The invention relates to a stiffening agent and resin finishing liquid used for crease finishing of jean clothes. The stiffening agent used for crease finishing of the jean clothes comprises the following components, by weight percentage or weight, 60-67% of polyvinyl alcohol emulsion, 33-40% of polyurethane emulsion, and a buffer system of which the weight is 0.006 time of the total weight of the polyvinyl alcohol emulsion and the polyurethane emulsion. The resin finishing liquid used for crease finishing of the jean clothes comprises the following component, by weight percentage or weight, 3-6% of the stiffening agent, 6-18% of crease pressing resin, catalysts with use amount being 1/5-1/4 of the crease pressing resin, and the balance water. By the adoption of the stiffening agent and resin finishing liquid used for crease finishing of the jean clothes, the elastic recovery performance and crease resistant performance of jeans can be improved; the stereoscopic impression of cat whiskers and three-dimensional cat whiskers of creases is achieved, and durability is also achieved; the color retaining performance and dry and wet friction fastness are improved, a soft feeling is achieved, the cost performance is high, and the requirement for fashionable elements of the jean clothes is met.
Description
Technical field
The present invention relates to cowboy's dress ornament washing processing (style) finishing field, be specifically related to the stiffening agent crumpling arrangement for cowboy's dress ornament.
Background technology
In recent years, there is a kind of fashion trend in cowboy's dress ornament---solid crumples cat's whisker and arranges.Arrange out clothes at the position such as trouser legs, trousers body of clothes and take the natural wrinkle of flat and circle produced in process, and its wrinkle form stable is got off, because its shape is as cat's whisker, therefore claiming three-dimensional cat's whisker to crumple arrangement, this style is because of its nature, novel, fashion and enjoy consumers in general to like.
Cowboy crumples finishing technique becomes one of the most conventional technique of denim industry gradually.Its effect makes cowboy improve its elastic recovery properties after the arrangement of RESIN FINISH liquid crumples, thus improve the wrinkle resistance of cowboy clothing trousers, give cowboy's dress ornament simultaneously and crumple cat's whisker, 3D cat's whisker third dimension and persistence, improve its guarantee the minimum performance and and dry fastness to wet rubbing, thus improve the class of cowboy clothing trousers.Crumple cowboy in the RESIN FINISH formula of liquid of cat's whisker, the three-dimensional cat's whisker of 3D, adding of stiffening agent is absolutely necessary, and is also very important.
With regard to stiffening agent in the market, having of normal use: acrylic acid and acrylate emulsifying liquid stiffening agent.Cowboy's dress ornament after the RESIN FINISH liquid process with above-mentioned stiffening agent, cat's whisker stereoeffect and guarantee the minimum performance still can, but elasticity is poor, and feel is really up to the mark.Also have and use polyvinyl acetate emulsion or PVA emulsion as stiffening agent, after the RESIN FINISH liquid process with this stiffening agent, the feel of cowboy's dress ornament comparatively speaking still can, but cat's whisker stereoeffect defect to some extent.
Therefore, in order to improve the competitiveness of cowboy's product, meet the fashion clothing needs that people are growing, study a kind of both improved denim fabric elasticity, improve and crumple stereoeffect, there is again performance of guaranteeing the minimum preferably, soft, reduce the loss to powerful tensile force, the stiffening agent that cloth cover glossiness is improved becomes the task of top priority of the industry! Thus improve the competitiveness cowboy's product, meet the fashion clothing needs that people are growing.
Summary of the invention
For the deficiencies in the prior art, the object of this invention is to provide a kind of stiffening agent and the RESIN FINISH liquid that crumple arrangement for cowboy, improve the elastic recovery properties of cowboy, thus improve the wrinkle resistance of cowboy clothing trousers; Imparting crumples cat's whisker, 3D cat's whisker third dimension, persistence; Improve its unfading and dry wet-milling rubbing fastness; Soft, reduce the loss of powerful tensile force, cost performance is high, stay in grade, meets environmental protection concept, meets the requirement of cowboy's dress ornament fashionable element.
In order to solve the problems of the technologies described above, the present invention is achieved by the following technical solutions:
A kind of stiffening agent crumpling arrangement for cowboy's dress ornament, it is characterized in that, be made up of polyvinyl alcohol emulsions, polyurethane emulsion and buffer system, with the mixed liquor weight of polyvinyl alcohol emulsions and polyurethane emulsion for benchmark, weight percent content or the consumption of each component are as follows: polyvinyl alcohol emulsions 60% ~ 67%, polyurethane emulsion 33% ~ 40%, the consumption of buffer system is 0.006 times of the mixed liquor weight of polyvinyl alcohol emulsions and polyurethane emulsion.
Preferably, described polyvinyl alcohol emulsions selects the degree of polymerization to be 1750, alcoholysis degree be 99.5% polyvinyl alcohol raw material be prepared from.
Further, described polyvinyl alcohol emulsions select weight content be 14% polyvinyl alcohol emulsions; Described polyurethane emulsion select weight content be 23% polyurethane emulsion.
Further, the preparation method of the polyvinyl alcohol emulsions of described 14% is: with the total weight of polyvinyl alcohol emulsions, the water of 86% is added in reactor, start kneading mill, slowly add the cotton-shaped polyvinyl alcohol of 14% again, polyvinyl alcohol add rear stir to tremble be warming up to 90-95 DEG C, after fully dissolving, discharging, then stirring cools to indoor temperature;
Further, the preparation method of the polyurethane emulsion of described 23% is: with the total weight of polyurethane emulsion, add the emulsifying agent TX-10 of 6.5% in a kettle., the paregal O of 6.5%, inject the water of 64%, stir the polyurethane adding 23%, be warming up to 70 DEG C, insulation 90min, blowing is filtered in cooling.
Preferably, described buffer system by 98% acetic acid, 99% sodium acetate and water with weight ratio acetic acid: sodium acetate: water=3:5:13 is formulated.
A kind of RESIN FINISH liquid crumpling arrangement for cowboy's dress ornament, it is characterized in that, comprise described stiffening agent, crumple resin and catalyst, wherein the weight percent content of each component or consumption are: stiffening agent 3 ~ 6%, crumple resin 6 ~ 18%, catalyst amount for described in crumple 1/5 ~ 1/4 of resin, surplus is water.
Further, crumple described in that resin is selected from etherificate dihydroxymethyl dihydroxy ethylidene-urea resin, N-methylol dihydroxymethyl ethylene urea, Lauxite, melamine resin, dihydroxymethyl urethanes, dihydroxymethyl triazinone, dihydroxymethyl oolong any one; Described catalyst can be MgCl
26H
2one or more in O, zinc chloride, crystallization zinc nitrate, ammonium chloride, ammonium nitrate, triethanol ammonium hydrochloride, ammonium phosphate, polyacid.
Use described RESIN FINISH liquid cowboy's dress ornament to be crumpled to the method for arrangement, it is characterized in that, comprise following step: (1) does destarch process with amylase to cowboy's dress ornament; (2) wash; (3) dry; (4) resin pickup dressing liquid; (5) upper three-dimensional cat's whisker mechanism makes cat's whisker, then preliminary drying; (oven machine Shang 6); (7) softener process is added.
Further, the soak time of the RESIN FINISH liquid of step (4) is 15 minutes, then dewaters 5 minutes with Water Extraction Machinery; The preliminary drying temperature of step (5) is 100 DEG C, preliminary drying 12 minutes; (6) ovens are Li Shi oven machine to step, baked 25 minutes of temperature 145 DEG C; The softener of step (7) is silicone oil and the 3g/L consistent lubricant of 3g/L, and the processing time is 5 minutes.
Stiffening agent and the RESIN FINISH liquid crumpling arrangement for cowboy of the present invention, reaches following beneficial effect:
(1) alcoholysis degree due to PVA is different with the degree of polymerization, its dissolubility, adhesiveness, moulding property have very large difference, TENSILE STRENGTH after PVA film forming is with the degree of polymerization, and the rising of alcoholysis degree and increasing, the degree of polymerization and the high PVA of alcoholysis degree have higher adhesiveness and compatibility to hydrophilic fibre simultaneously.The present invention selectes a kind of PVA(polyvinyl alcohol being conducive to cowboy's cat's whisker solid) as one of preparation raw material, its degree of polymerization is 1750, alcoholysis degree is 99.5%, can make cowboy crumple cat's whisker, 3D cat's whisker film forming very good, and " hard and tough ";
(2) concerning cowboy crumples cat's whisker, the three-dimensional cat's whisker of 3D, look after just crumpling that third dimension is inadequate, also must have persistence, quality is soft, high resilience, the pliability had.Polyurethane belongs to emerging high-molecular organic material, and by the material of ethane organo units chain polymerization, it is good that it has ABRASION RESISTANCE, and hardness range adapts to strong, and mechanical strength is large, and adhesive property is good; Good springiness simultaneously, have excellent restoration, it has low-temperature pliability in addition, the performances such as weather fastness is good, oil resistivity is good, resistance to biological aging.The PVA of polyurethane and certain degree of polymerization and alcoholysis degree combines by the present invention, the novel stiffening agent of this combination is added in RESIN FINISH liquid, make cowboy crumple cat's whisker solid, durability is strong, feel elasticity strengthens, there is good unfading, after conjunctiva improves, thus improve its environment and wearability, this novel stiffening agent is a kind of competitive novel product;
(3) produce through a large amount of cowboy clothing trousers bulk productions, in same process condition, under the prerequisite that homogenous resins consumption is identical, by adding the PVA of equivalent respectively, polyvinyl acetate class stiffening agent, acrylic acid, esters of acrylic acid stiffening agent and stiffening agent of the present invention compare test, from the effect of product, the stiffening agent of the present invention various successfuls added in resin are better than other kind stiffening agent, not only crumple cat's whisker, the stereoeffect of 3D cat's whisker obviously strengthens, washability strengthens, improve the elastic recovery properties of fabric, simultaneously soft, the loss of powerful tensile force decreases, glossiness, unfadings etc. are significantly improved.
Detailed description of the invention
Below in conjunction with specific embodiment, the present invention is further illustrated, but the present invention is not by the restriction of following embodiment.
Embodiment 1
(1) prepare the polyvinyl alcohol emulsions of 14%: select the degree of polymerization to be 1750, alcoholysis degree is the polyvinyl alcohol raw material of 99.5%.With the total weight of polyvinyl alcohol emulsions, in reactor, add the water of 86%, start kneading mill, slowly add the cotton-shaped polyvinyl alcohol of 14% again, polyvinyl alcohol add rear stir to tremble be warming up to 90-95 DEG C, after fully dissolving, discharging, then stirring cools to indoor temperature.
(2) the polyurethane emulsion of 23% is prepared: with the total weight of polyurethane emulsion, add the emulsifying agent TX-10(Polyethylene Octylphenol Ether-10 of 6.5% in a kettle .), the paregal O (fatty alcohol-polyoxyethylene ether) of 6.5%, inject the water of 64%, stir while add 23% polyurethane, be warming up to 70 DEG C, insulation 90min, blowing is filtered in cooling.
(3) preparation of buffer system: due under normal conditions, the best film forming pH value range of cowboy clothing trousers RESIN FINISH is 4.2 ~ 4.8, in order to keep the pH value range in resin liquid to stablize, therefore also adds buffer system in stiffening agent.This buffer system is made up of acetic acid (content 98%), sodium acetate (content 99%) and water.Thus make the pH value in stiffening agent constant in about 4.5.Acetic acid: sodium acetate: water=3:5:13.(mass ratio)
(4) with the mixed liquor weight of polyvinyl alcohol emulsions and polyurethane emulsion for benchmark, choose the component of following weight percentage: polyvinyl alcohol emulsions 60%, polyurethane emulsion 40%, buffer system is added again after mixing, the consumption of buffer system is 0.006 times of the mixed liquor weight of polyvinyl alcohol emulsions and polyurethane emulsion, obtains the stiffening agent of the present embodiment.
Embodiment 2
Step (1) (2) (3) are identical with embodiment 1, and polyvinyl alcohol emulsions 67% in step (4), polyurethane emulsion 33%, all the other are identical, prepare the stiffening agent of the present embodiment.
Embodiment 3
Step (1) (2) (3) are identical with embodiment 1, and polyvinyl alcohol emulsions 63.5% in step (4), polyurethane emulsion 36.5%, all the other are identical, prepare the stiffening agent of the present embodiment.
Embodiment 4 ~ 6: following crumple resin can be selected from etherificate dihydroxymethyl dihydroxy ethylidene-urea resin, N-methylol dihydroxymethyl ethylene urea, Lauxite, melamine resin, dihydroxymethyl urethanes, dihydroxymethyl triazinone, dihydroxymethyl oolong any one; Catalyst can be MgCl
26H
2one or more in O, zinc chloride, crystallization zinc nitrate, ammonium chloride, ammonium nitrate, triethanol ammonium hydrochloride, ammonium phosphate, polyacid.
Embodiment 4
The RESIN FINISH liquid of the present embodiment, comprises the stiffening agent of embodiment 1, crumples resin and catalyst, and in percentage by weight or weight content, wherein stiffening agent 3%, crumples resin 12%, and catalyst content is crumple weight resin 1/5, and surplus is water.
Embodiment 5
The RESIN FINISH liquid of the present embodiment, comprises the stiffening agent of embodiment 2, crumples resin and catalyst, and in percentage by weight or weight content, wherein stiffening agent 4.5%, crumples resin 6%, and catalyst content is crumple resin 1/4, and surplus is water.
Embodiment 6
The RESIN FINISH liquid of the present embodiment, comprises the stiffening agent of embodiment 3, crumples resin and catalyst, wherein stiffening agent 6%, crumple resin 18%, and catalyst content is crumple resin 1/4, and surplus is water.
Embodiment 7
Material: 393g/m
2, the textile indigo jeans of 60kg
Equipment: 630 pounds of industry washers, drum-type industrial drier (YG2-300P), resin pickup liquid container, Italy produces three-dimensional cat's whisker Ji ， oven machine (YCF-120 type) of Tonello3D
1. choose different resins dressing liquid formula
Choose the RESIN FINISH liquid of following three kinds of different formulations respectively, wherein formula 3 is RESIN FINISH liquid of the present invention, following modification dihydroxymethyl dihydroxy ethylidene-urea resin is selected from Yorkshire chemical industry Pty Ltd SERIREZ AP-ECLF, polyvinyl acetate class stiffening agent is produced by the red textile technology Co., Ltd of Dongguan City ten thousand, and acrylic compounds stiffening agent is the ebonite KDM-T35 of Guangzhou Jin Demeng biological material Co., Ltd:
2, the three-dimensional cat's whisker technique of 3D:
Flow process: amylase destarch → washing → oven dry → resin pickup liquid → upper three-dimensional cat's whisker machine preliminary drying → oven → add softener (silicone oil, consistent lubricant)
To fill a prescription and 1,2,3 soak trousers 20kg respectively, and soak 15 minutes, dewater 5 minutes with same centrifugal dehydrator respectively.Go up the three-dimensional cat's whisker machine of Tonello3D respectively and do into same three-dimensional cat's whisker, 100 DEG C of pre-ovens 12 minutes, then all with vertical formula oven machine 145 DEG C of ovens 25 minutes, finally, all add organic silicone oil 3g/L, consistent lubricant 3g/L, normal temperature × 5min.Its stylistic effects is compared after drying.
3, through fill a prescription 1,2,3 RESIN FINISH liquid process respectively after cowboy's dress ornament, it is as follows that effectiveness indicator compares form:
Embodiment 8
Material: 368g/m
2, the cotton of content 98%, the spandex of 2%, 60kg blue-black jeans.
Device therefor is identical with embodiment 7.
1. choose different resins dressing liquid formula
Choose the RESIN FINISH liquid of following three kinds of different formulations respectively, wherein formula 3 is RESIN FINISH liquid of the present invention, following N-methylol dihydroxymethyl ethyl urea resin is selected from the Superlow Formaldehyde Resin PM-50 of Lian Sheng chemical plant, Shantou City Co., Ltd, polyvinyl acetate class stiffening agent is produced by the red textile technology Co., Ltd of Dongguan City ten thousand, and acrylic compounds stiffening agent is the ebonite KDM-T35 of Guangzhou Jin Demeng biological material Co., Ltd:
2, the three-dimensional cat's whisker technological process of 3D is identical with embodiment 7 with process.
3, through fill a prescription 1,2,3 RESIN FINISH liquid process respectively after cowboy's dress ornament, it is as follows that effectiveness indicator compares form:
As can be seen from embodiment 7 ~ 8, by stiffening agent of the present invention, after joining various RESIN FINISH, be that the flat deflection of denim fabric is improved, elastic recovery capability obtains obvious reinforcement, finished tensile loss that is powerful and tearing brute force obtains obvious improvement, and performance of guaranteeing the minimum improves, overall soft, glossiness is good, cat's whisker stereoeffect is more obvious, and improve product specification, the present invention is a kind of desirable cowboy's RESIN FINISH stiffening agent.
Last it is noted that these are only the preferred embodiments of the present invention; be not limited to the present invention; although with reference to embodiment to invention has been detailed description; for a person skilled in the art; it still can be modified to the technical scheme described in previous embodiment; or equivalent replacement is carried out to wherein portion of techniques feature; but it is within the spirit and principles in the present invention all; any amendment of doing, equivalent replacement, improvement etc., all should be included within protection scope of the present invention.
Claims (10)
1. one kind crumples the stiffening agent of arrangement for cowboy's dress ornament, it is characterized in that, be made up of polyvinyl alcohol emulsions, polyurethane emulsion and buffer system, with the mixed liquor weight of polyvinyl alcohol emulsions and polyurethane emulsion for benchmark, weight percent content or the consumption of each component are as follows:
Polyvinyl alcohol emulsions 60% ~ 67%,
Polyurethane emulsion 33% ~ 40%,
The consumption of buffer system is 0.006 times of the mixed liquor weight of polyvinyl alcohol emulsions and polyurethane emulsion.
2. the stiffening agent crumpling arrangement for cowboy's dress ornament according to claim 1, is characterized in that, described polyvinyl alcohol emulsions selects the degree of polymerization to be 1750, alcoholysis degree be 99.5% polyvinyl alcohol raw material be prepared from.
3. the stiffening agent crumpling arrangement for cowboy's dress ornament according to claim 1, is characterized in that, described polyvinyl alcohol emulsions select weight content be 14% polyvinyl alcohol emulsions; Described polyurethane emulsion select weight content be 23% polyurethane emulsion.
4. the stiffening agent crumpling arrangement for cowboy's dress ornament according to claim 3, it is characterized in that, the preparation method of the polyvinyl alcohol emulsions of described 14% is: with the total weight of polyvinyl alcohol emulsions, in reactor, add the water of 86%, start kneading mill, more slowly add the cotton-shaped polyvinyl alcohol of 14%, polyvinyl alcohol adds rear stirring and trembles while be warming up to 90-95 DEG C, after fully dissolving, discharging, then stirring cools to indoor temperature.
5. the stiffening agent crumpling arrangement for cowboy's dress ornament according to claim 3, it is characterized in that, the preparation method of the polyurethane emulsion of described 23% is: with the total weight of polyurethane emulsion, add the emulsifying agent TX-10 of 6.5% in a kettle., the paregal O of 6.5%, inject the water of 64%, first stir, then add the polyurethane of 23%, stir, be warming up to 70 DEG C, insulation 90min, blowing is filtered in cooling.
6. the stiffening agent crumpling arrangement for cowboy's dress ornament according to claim 1, is characterized in that, described buffer system by 98% acetic acid, 99% sodium acetate and water with weight ratio 98% acetic acid: 99% sodium acetate: water=3:5:13 is formulated.
7. crumple a RESIN FINISH liquid for arrangement for cowboy's dress ornament, it is characterized in that, comprise the arbitrary described stiffening agent of claim 1 ~ 6, crumple resin and catalyst, wherein the weight percent content of each component or consumption are:
8. the RESIN FINISH liquid crumpling arrangement for cowboy's dress ornament according to claim 7, it is characterized in that, described in crumple that resin is selected from etherificate dihydroxymethyl dihydroxy ethylidene-urea resin, N-methylol dihydroxymethyl ethylene urea, Lauxite, melamine resin, dihydroxymethyl urethanes, dihydroxymethyl triazinone, dihydroxymethyl oolong any one; Described catalyst is MgCl
26H
2one or more in O, zinc chloride, crystallization zinc nitrate, ammonium chloride, ammonium nitrate, triethanol ammonium hydrochloride, ammonium phosphate, polyacid.
9. use the RESIN FINISH liquid described in claim 7 or 8 cowboy's dress ornament to be crumpled to the method for arrangement, it is characterized in that, comprise following step:
(1) with amylase, destarch process is done to cowboy's dress ornament;
(2) wash;
(3) dry;
(4) resin pickup dressing liquid;
(5) upper three-dimensional cat's whisker mechanism makes cat's whisker, then preliminary drying;
(oven machine Shang 6);
(7) softener process is added.
10. method cowboy's dress ornament being crumpled to arrangement according to claim 9, is characterized in that, the soak time of the RESIN FINISH liquid of step (4) is 15 minutes, then dewaters 5 minutes with Water Extraction Machinery; The preliminary drying temperature of step (5) is 100 DEG C, preliminary drying 12 minutes; (6) ovens are Li Shi oven machine to step, baked 25 minutes of temperature 145 DEG C; The softener of step (7) is silicone oil and the 3g/L consistent lubricant of 3g/L, and the processing time is 5 minutes.
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| CN103469577B true CN103469577B (en) | 2015-04-29 |
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Families Citing this family (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103757909B (en) * | 2013-12-21 | 2015-11-25 | 成都德美精英化工有限公司 | A kind of nonionic stiffening agent and preparation method thereof |
| SI3009020T1 (en) | 2014-10-17 | 2018-11-30 | COFEMEL - Sociedade de Vestuario S.A. | Garment and manufacturing method |
| CN104532609B (en) * | 2014-12-11 | 2017-01-25 | 江门市宝发纺织服饰制造有限公司 | Printing paste for locking jeans elasticity and preventing bleaching and application thereof |
| CN105926295A (en) * | 2016-05-30 | 2016-09-07 | 太仓红桥服饰有限公司 | Finishing liquid applied to crumple finishing of jean costume |
| CN107558222A (en) * | 2016-07-01 | 2018-01-09 | 顾香 | Water-soluble finishing agent |
| CN107558226A (en) * | 2016-07-01 | 2018-01-09 | 顾香 | Water-soluble wrinkle resistance finishing agent |
| CN107558227A (en) * | 2016-07-01 | 2018-01-09 | 顾香 | Silk broadcloth crease proofing agent |
| CN106400464A (en) * | 2016-11-24 | 2017-02-15 | 肇庆高新区飞越信息科技有限公司 | Green and environment-friendly stiffening agent for yarn fabric |
| CN107280099B (en) * | 2017-07-14 | 2019-05-24 | 上海喜眠服饰有限公司 | Rapid-curing cutback is perspired not catch a cold nightwear and its preparation process |
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