CN103469577A - Stiffening agent used for crease finishing of jean clothes - Google Patents
Stiffening agent used for crease finishing of jean clothes Download PDFInfo
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- CN103469577A CN103469577A CN2013104640233A CN201310464023A CN103469577A CN 103469577 A CN103469577 A CN 103469577A CN 2013104640233 A CN2013104640233 A CN 2013104640233A CN 201310464023 A CN201310464023 A CN 201310464023A CN 103469577 A CN103469577 A CN 103469577A
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- polyvinyl alcohol
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- resin
- stiffening agent
- emulsion
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Abstract
The invention relates to a stiffening agent and resin finishing liquid used for crease finishing of jean clothes. The stiffening agent used for crease finishing of the jean clothes comprises the following components, by weight percentage or weight, 60-67% of polyvinyl alcohol emulsion, 33-40% of polyurethane emulsion, and a buffer system of which the weight is 0.006 time of the total weight of the polyvinyl alcohol emulsion and the polyurethane emulsion. The resin finishing liquid used for crease finishing of the jean clothes comprises the following component, by weight percentage or weight, 3-6% of the stiffening agent, 6-18% of crease pressing resin, catalysts with use amount being 1/5-1/4 of the crease pressing resin, and the balance water. By the adoption of the stiffening agent and resin finishing liquid used for crease finishing of the jean clothes, the elastic recovery performance and crease resistant performance of jeans can be improved; the stereoscopic impression of cat whiskers and three-dimensional cat whiskers of creases is achieved, and durability is also achieved; the color retaining performance and dry and wet friction fastness are improved, a soft feeling is achieved, the cost performance is high, and the requirement for fashionable elements of the jean clothes is met.
Description
Technical field
The present invention relates to cowboy's dress ornament washing processing (style) finishing field, be specifically related to crumple for cowboy's dress ornament the stiffening agent of arrangement.
Background technology
In recent years, a kind of fashion trend has appearred in cowboy's dress ornament---solid crumples cat's whisker and arranges.Arrange out the flat and circular natural wrinkle that clothes produce in taking process at positions such as the trouser legs of clothes, trousers bodies, and its wrinkle form stable is got off, because of its shape as cat's whisker, therefore claim three-dimensional cat's whisker to crumple arrangement, this style enjoys consumers in general to like because of its nature, novelty, fashion.
Cowboy crumples finishing technique becomes one of the most conventional technique of denim industry gradually.Its effect is to make cowboy improve its elastic recovery properties after the arrangement of RESIN FINISH liquid crumples, thereby improve the wrinkle resistance of cowboy clothing trousers, give cowboy's dress ornament simultaneously and crumple cat's whisker, 3D cat's whisker third dimension and persistence, improve its guarantee the minimum performance and dry fastness to wet rubbing, thereby improve the class of cowboy clothing trousers.Cowboy, crumple in the RESIN FINISH formula of liquid of cat's whisker, the three-dimensional cat's whisker of 3D, adding of stiffening agent is absolutely necessary, and is also very important.
With regard to stiffening agent in the market, normal having of using: acrylic acid and acrylate emulsifying liquid stiffening agent.Cowboy's dress ornament after the RESIN FINISH liquid with above-mentioned stiffening agent is processed, the cat's whisker stereoeffect and guarantee the minimum performance still can, but elasticity is poor, feel is really up to the mark.Also have and use polyvinyl acetate emulsion or PVA emulsion as stiffening agent, after the RESIN FINISH liquid through having this stiffening agent is processed, the feel of cowboy's dress ornament comparatively speaking still can, but cat's whisker stereoeffect defect to some extent.
Therefore, in order to improve the competitiveness of cowboy's product, meet the growing fashion clothing needs of people, study a kind of elasticity, raising that had both improved cowboy's fabric and crumple stereoeffect, the performance of guaranteeing the minimum is preferably arranged again, soft, reduce the loss to powerful tearing power, the stiffening agent that the cloth cover glossiness is improved becomes the task of top priority of the industry! Thereby improve the competitiveness that cowboy's product, meet the growing fashion clothing needs of people.
Summary of the invention
For the deficiencies in the prior art, the purpose of this invention is to provide a kind of stiffening agent and RESIN FINISH liquid that crumples arrangement for cowboy, improve cowboy's elastic recovery properties, thereby improve the wrinkle resistance of cowboy clothing trousers; Give and crumple cat's whisker, 3D cat's whisker third dimension, persistence; Improve its unfading and dry wet-milling rubbing fastness; Soft, reduce powerful tearing power loss, cost performance is high, and stay in grade meets environmental protection concept, meets the requirement of cowboy's dress ornament fashionable element.
In order to solve the problems of the technologies described above, the present invention is achieved by the following technical solutions:
A kind of stiffening agent that crumples arrangement for cowboy's dress ornament, it is characterized in that, by polyvinyl alcohol emulsion, polyurethane emulsion and buffering composing system, the mixed liquor weight of polyvinyl alcohol emulsion and polyurethane emulsion of take is benchmark, weight percent content or the consumption of each component are as follows: polyvinyl alcohol emulsion 60%～67%, polyurethane emulsion 33%～40%, the consumption of buffer system is 0.006 times of mixed liquor weight of polyvinyl alcohol emulsion and polyurethane emulsion.
Preferably, it is 1750 that described polyvinyl alcohol emulsion is selected the degree of polymerization, and the polyvinyl alcohol raw material that alcoholysis degree is 99.5% is prepared from.
Further, described polyvinyl alcohol emulsion is selected the polyvinyl alcohol emulsion that weight content is 14%; Described polyurethane emulsion is selected the polyurethane emulsion that weight content is 23%.
Further, the preparation method of described 14% polyvinyl alcohol emulsion is: in the gross weight of polyvinyl alcohol emulsion, add 86% water in reactor, start kneading mill, slowly add again 14% cotton-shaped polyvinyl alcohol, while polyvinyl alcohol add rear stir to tremble be warming up to 90-95 ℃, after fully dissolving, discharging, then stirring cools to indoor temperature;
Further, the preparation method of described 23% polyurethane emulsion is: in the gross weight of polyurethane emulsion, add 6.5% emulsifying agent TX-10 in reactor, 6.5% paregal O, inject 64% water, while stir the polyurethane that adds 23%, be warming up to 70 ℃, insulation 90min, blowing is filtered in cooling.
Preferably, described buffer system by 98% acetic acid, 99% sodium acetate and water with weight ratio acetic acid: sodium acetate: water=3:5:13 is formulated.
A kind of RESIN FINISH liquid that crumples arrangement for cowboy's dress ornament, it is characterized in that, comprise described stiffening agent, crumple resin and catalyst, wherein the weight percent content of each component or consumption are: stiffening agent 3～6%, crumple resin 6～18%, catalyst amount is described 1/5～1/4 of the resin that crumples, and surplus is water.
Further, the described resin that crumples is selected from any one in etherificate dihydroxymethyl dihydroxy ethylidene-urea resin, N-methylol dihydroxymethyl ethylene urea, Lauxite, melamine resin, dihydroxymethyl urethanes, dihydroxymethyl triazinone, dihydroxymethyl oolong; Described catalyst can be MgCl
26H
2one or more in O, zinc chloride, crystallization zinc nitrate, ammonium chloride, ammonium nitrate, triethanol ammonium hydrochloride, ammonium phosphate, polyacid.
Use described RESIN FINISH liquid cowboy's dress ornament to be crumpled to the method for arrangement, it is characterized in that, comprise following step: (1) is done destarch with amylase to cowboy's dress ornament and is processed; (2) washing; (3) dry; (4) resin pickup dressing liquid; (5) upper three-dimensional cat's whisker mechanism is made cat's whisker, then preliminary drying; (6) Shang oven machines; (7) adding softener processes.
Further, the soak time of the RESIN FINISH liquid of step (4) is 15 minutes, then with Water Extraction Machinery dehydration 5 minutes; The preliminary drying temperature of step (5) is 100 ℃, preliminary drying 12 minutes; (6) ovens are Li Shi oven machine to step, baked 25 minutes of temperature 145 ℃; The silicone oil that the softener of step (7) is 3g/L and 3g/L consistent lubricant, the processing time is 5 minutes.
Stiffening agent and the RESIN FINISH liquid that crumples arrangement for cowboy of the present invention has reached following beneficial effect:
(1) because the alcoholysis degree of PVA is different with the degree of polymerization, its dissolubility, adhesiveness, moulding property have very large difference, TENSILE STRENGTH after the PVA film forming is with the degree of polymerization, the rising of alcoholysis degree and increasing, and the degree of polymerization and the high PVA of alcoholysis degree have higher adhesiveness and compatibility to hydrophilic fibre simultaneously.The present invention selectes a kind of PVA(polyvinyl alcohol that is conducive to cowboy's cat's whisker solid) as one of preparation raw material, its degree of polymerization is 1750, alcoholysis degree is 99.5%, can so that cowboy to crumple the film forming of cat's whisker, 3D cat's whisker very good, and " hard and tough ";
(2) concerning cowboy crumples cat's whisker, the three-dimensional cat's whisker of 3D, look after just having crumpled that third dimension is inadequate, also persistence must be arranged, quality softness, high resilience, the pliability had.Polyurethane belongs to emerging high-molecular organic material, the material be polymerized by the organic cellular chain of ethane, and it is good that it has ABRASION RESISTANCE, and hardness range adapts to strong, and mechanical strength is large, and adhesive property is good; Good springiness, have good restoration simultaneously, and it has low-temperature pliability in addition, the performances such as weather fastness is good, oil resistivity is good, anti-biological aging.The present invention is the PVA combination with certain degree of polymerization and alcoholysis degree by polyurethane, the novel stiffening agent of this combination is added in RESIN FINISH liquid, make cowboy crumple the cat's whisker solid, durability is strong, feel elasticity strengthens, there is good unfading, after the conjunctiva raising, thereby improve its environment and take performance, this novel stiffening agent is a kind of competitive novel product;
(3) through a large amount of cowboy clothing trousers bulk productions, produce, in the same process condition, at resin demand of the same race under identical prerequisite, by adding respectively the PVA of equivalent, polyvinyl acetate class stiffening agent, acrylic acid, esters of acrylic acid stiffening agent and stiffening agent of the present invention compare test, effect from product, stiffening agent of the present invention adds the various successfuls in resin to be better than other kind stiffening agent, not only crumple cat's whisker, the stereoeffect of 3D cat's whisker obviously strengthens, washability strengthens, improved the elastic recovery properties of fabric, simultaneously soft, the loss of powerful tearing power has reduced, glossiness, unfadings etc. are significantly improved.
The specific embodiment
Below in conjunction with specific embodiment, the present invention is further illustrated, but the present invention is not subject to the restriction of following embodiment.
Embodiment 1
(1) prepare 14% polyvinyl alcohol emulsion: selecting the degree of polymerization is 1750, the polyvinyl alcohol raw material that alcoholysis degree is 99.5%.In the gross weight of polyvinyl alcohol emulsion, add 86% water in reactor, start kneading mill, slowly add again 14% cotton-shaped polyvinyl alcohol, while polyvinyl alcohol add rear stir to tremble be warming up to 90-95 ℃, after fully dissolving, discharging, then stirring cools to indoor temperature.
(2) prepare 23% polyurethane emulsion: in the gross weight of polyurethane emulsion, add 6.5% emulsifying agent TX-10(Polyethylene Octylphenol Ether-10 in reactor), 6.5% paregal O (fatty alcohol-polyoxyethylene ether), inject 64% water, while stirring the polyurethane that adds 23%, be warming up to 70 ℃, insulation 90min, blowing is filtered in cooling.
(3) preparation of buffer system: due under usual condition, the best film forming pH value scope of cowboy clothing trousers RESIN FINISH is 4.2～4.8, in order to keep the pH value scope in resin liquid stable, therefore also add buffer system in stiffening agent.This buffer system is comprised of acetic acid (content 98%), sodium acetate (content 99%) and water.Thereby make the pH value in stiffening agent constant in 4.5 left and right.Acetic acid: sodium acetate: water=3:5:13.(mass ratio)
(4) take the mixed liquor weight of polyvinyl alcohol emulsion and polyurethane emulsion is benchmark, choose the component of following weight percentage: polyvinyl alcohol emulsion 60%, polyurethane emulsion 40%, add again buffer system after mixing, the consumption of buffer system is 0.006 times of mixed liquor weight of polyvinyl alcohol emulsion and polyurethane emulsion, obtains the stiffening agent of the present embodiment.
Embodiment 2
Step (1) (2) (3) is identical with embodiment 1, polyvinyl alcohol emulsion 67% in step (4), and polyurethane emulsion 33%, all the other are identical, prepare the stiffening agent of the present embodiment.
Embodiment 3
Step (1) (2) (3) is identical with embodiment 1, polyvinyl alcohol emulsion 63.5% in step (4), and polyurethane emulsion 36.5%, all the other are identical, prepare the stiffening agent of the present embodiment.
Embodiment 4～6: the following resin that crumples can be to be selected from any one in etherificate dihydroxymethyl dihydroxy ethylidene-urea resin, N-methylol dihydroxymethyl ethylene urea, Lauxite, melamine resin, dihydroxymethyl urethanes, dihydroxymethyl triazinone, dihydroxymethyl oolong; Catalyst can be MgCl
26H
2one or more in O, zinc chloride, crystallization zinc nitrate, ammonium chloride, ammonium nitrate, triethanol ammonium hydrochloride, ammonium phosphate, polyacid.
Embodiment 4
The RESIN FINISH liquid of the present embodiment, comprise embodiment 1 stiffening agent, crumple resin and catalyst, in percentage by weight or weight content, wherein stiffening agent 3%, crumples resin 12%, catalyst content is to crumple 1/5 of weight resin, surplus is water.
Embodiment 5
The RESIN FINISH liquid of the present embodiment, comprise embodiment 2 stiffening agent, crumple resin and catalyst, in percentage by weight or weight content, wherein stiffening agent 4.5%, crumples resin 6%, catalyst content is to crumple 1/4 of resin, surplus is water.
Embodiment 6
The RESIN FINISH liquid of the present embodiment, comprise embodiment 3 stiffening agent, crumple resin and catalyst, wherein stiffening agent 6%, crumples resin 18%, catalyst content is to crumple 1/4 of resin, surplus is water.
Embodiment 7
Material: 393g/m
2, the textile indigo jeans of 60kg
Equipment: 630 pounds of industry washers, drum-type industrial drier (YG2-300P), the resin pickup liquid container, Italy produces the three-dimensional cat's whisker Ji ， oven machine (YCF-120 type) of Tonello3D
1. choose different resins dressing liquid formula
Choose respectively the RESIN FINISH liquid of following three kinds of different formulations, wherein fill a prescription 3 for RESIN FINISH liquid of the present invention, following modification dihydroxymethyl dihydroxy ethylidene-urea resin is selected from the holding SERIREZ AP-ECLF of Co., Ltd of Yorkshire chemical industry, polyvinyl acetate class stiffening agent is produced by the red textile technology of Dongguan City ten thousand Co., Ltd, the ebonite KDM-T35 that the acrylic compounds stiffening agent is Guangzhou Jin Demeng biological material Co., Ltd:
2, the three-dimensional cat's whisker technique of 3D:
Flow process: amylase destarch → washing → oven dry → resin pickup liquid → upper three-dimensional cat's whisker machine preliminary drying → oven → add softener (silicone oil, consistent lubricant)
To fill a prescription and 1,2,3 soak respectively trousers 20kg, soak 15 minutes, respectively with same centrifugal dehydrator dehydration 5 minutes.Go up respectively the three-dimensional cat's whisker machine of Tonello3D and do into same three-dimensional cat's whisker, 100 ℃ of pre-ovens 12 minutes, then all with 145 ℃ of ovens of vertical formula oven machine 25 minutes, all add organic silicone oil 3g/L, consistent lubricant 3g/L, normal temperature * 5min after finally.Compare its stylistic effects after drying.
3, the cowboy's dress ornament after 1,2,3 the RESIN FINISH liquid of filling a prescription is processed respectively, relatively form is as follows for effectiveness indicator:
Embodiment 8
Material: 368g/m
2, the cotton of content 98%, 2% spandex, 60kg blue-black jeans.
Device therefor is identical with embodiment 7.
1. choose different resins dressing liquid formula
Choose respectively the RESIN FINISH liquid of following three kinds of different formulations, wherein fill a prescription 3 for RESIN FINISH liquid of the present invention, following N-methylol dihydroxymethyl ethyl urea resin is selected from the Superlow Formaldehyde Resin PM-50 of Lian Sheng chemical plant, Shantou City Co., Ltd, polyvinyl acetate class stiffening agent is produced by the red textile technology of Dongguan City ten thousand Co., Ltd, the ebonite KDM-T35 that the acrylic compounds stiffening agent is Guangzhou Jin Demeng biological material Co., Ltd:
2, the three-dimensional cat's whisker technological process of 3D is identical with embodiment 7 with process.
3, the cowboy's dress ornament after 1,2,3 the RESIN FINISH liquid of filling a prescription is processed respectively, relatively form is as follows for effectiveness indicator:
From embodiment 7～8, can find out, by stiffening agent of the present invention, after joining various RESIN FINISH, be that the flat deflection of cowboy's fabric is improved, elastic recovery capability has obtained obvious reinforcement, the loss of fabric ultimate strength and tearing brute force has obtained obvious improvement, and the performance of guaranteeing the minimum improves, whole soft, glossiness is good, the cat's whisker stereoeffect is more obvious, has improved product specification, and the present invention is a kind of desirable cowboy's RESIN FINISH stiffening agent.
Finally it should be noted that: these are only the preferred embodiments of the present invention; be not limited to the present invention; although with reference to embodiment, the present invention is had been described in detail; for a person skilled in the art; its technical scheme that still can put down in writing previous embodiment is modified; perhaps part technical characterictic wherein is equal to replacement; but within the spirit and principles in the present invention all; any modification of doing, be equal to replacement, improvement etc., within protection scope of the present invention all should be included in.
Claims (10)
1. a stiffening agent that crumples arrangement for cowboy's dress ornament, it is characterized in that, by polyvinyl alcohol emulsion, polyurethane emulsion and buffering composing system, the mixed liquor weight of polyvinyl alcohol emulsion and polyurethane emulsion of take is benchmark, and weight percent content or the consumption of each component are as follows:
Polyvinyl alcohol emulsion 60%～67%,
Polyurethane emulsion 33%～40%,
The consumption of buffer system is 0.006 times of mixed liquor weight of polyvinyl alcohol emulsion and polyurethane emulsion.
2. the stiffening agent that crumples arrangement for cowboy's dress ornament according to claim 1, is characterized in that, it is 1750 that described polyvinyl alcohol emulsion is selected the degree of polymerization, and the polyvinyl alcohol raw material that alcoholysis degree is 99.5% is prepared from.
3. the stiffening agent that crumples arrangement for cowboy's dress ornament according to claim 1, is characterized in that, described polyvinyl alcohol emulsion is selected the polyvinyl alcohol emulsion that weight content is 14%; Described polyurethane emulsion is selected the polyurethane emulsion that weight content is 23%.
4. the stiffening agent that crumples arrangement for cowboy's dress ornament according to claim 3, it is characterized in that, the preparation method of described 14% polyvinyl alcohol emulsion is: in the gross weight of polyvinyl alcohol emulsion, add 86% water in reactor, start kneading mill, more slowly add 14% cotton-shaped polyvinyl alcohol, polyvinyl alcohol adds and while stirring to tremble, is warming up to 90-95 ℃ afterwards, after fully dissolving, discharging, then stirring cools to indoor temperature.
5. the stiffening agent that crumples arrangement for cowboy's dress ornament according to claim 3, it is characterized in that, the preparation method of described 23% polyurethane emulsion is: in the gross weight of polyurethane emulsion, add 6.5% emulsifying agent TX-10 in reactor, 6.5% paregal O, the water of injection 64%, first stir, then add 23% polyurethane, stir, be warming up to 70 ℃, insulation 90min, blowing is filtered in cooling.
6. the stiffening agent that crumples arrangement for cowboy's dress ornament according to claim 1, is characterized in that, described buffer system by 98% acetic acid, 99% sodium acetate and water with weight ratio 98% acetic acid: 99% sodium acetate: water=3:5:13 is formulated.
7. a RESIN FINISH liquid that crumples arrangement for cowboy's dress ornament, is characterized in that, comprises the arbitrary described stiffening agent of claim 1～6, crumples resin and catalyst, and wherein the weight percent content of each component or consumption are:
8. the RESIN FINISH liquid that crumples arrangement for cowboy's dress ornament according to claim 7, it is characterized in that, the described resin that crumples is selected from any one in etherificate dihydroxymethyl dihydroxy ethylidene-urea resin, N-methylol dihydroxymethyl ethylene urea, Lauxite, melamine resin, dihydroxymethyl urethanes, dihydroxymethyl triazinone, dihydroxymethyl oolong; Described catalyst can be MgCl
26H
2one or more in O, zinc chloride, crystallization zinc nitrate, ammonium chloride, ammonium nitrate, triethanol ammonium hydrochloride, ammonium phosphate, polyacid.
9. right to use requires 7 or 8 described RESIN FINISH liquid cowboy's dress ornament to be crumpled to the method for arrangement, it is characterized in that, comprises following step:
(1) with amylase, cowboy's dress ornament being done to destarch processes;
(2) washing;
(3) dry;
(4) resin pickup dressing liquid;
(5) upper three-dimensional cat's whisker mechanism is made cat's whisker, then preliminary drying;
(6) Shang oven machines;
(7) adding softener processes.
10. the method that cowboy's dress ornament is crumpled to arrangement according to claim 9, is characterized in that, the soak time of the RESIN FINISH liquid of step (4) is 15 minutes, then with Water Extraction Machinery dehydration 5 minutes; The preliminary drying temperature of step (5) is 100 ℃, preliminary drying 12 minutes; (6) ovens are Li Shi oven machine to step, baked 25 minutes of temperature 145 ℃; The silicone oil that the softener of step (7) is 3g/L and 3g/L consistent lubricant, the processing time is 5 minutes.
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| CN103757909A (en) * | 2013-12-21 | 2014-04-30 | 成都德美精英化工有限公司 | Non-ionic stiffening agent and preparation method thereof |
| CN104532609A (en) * | 2014-12-11 | 2015-04-22 | 江门市宝发纺织服饰制造有限公司 | Printing paste for locking jeans elasticity and preventing bleaching and application thereof |
| EP3009020A1 (en) * | 2014-10-17 | 2016-04-20 | COFEMEL - Sociedade de Vestuário S.A. | Garment and manufacturing method |
| CN105926295A (en) * | 2016-05-30 | 2016-09-07 | 太仓红桥服饰有限公司 | Finishing liquid applied to crumple finishing of jean costume |
| CN106400464A (en) * | 2016-11-24 | 2017-02-15 | 肇庆高新区飞越信息科技有限公司 | Green and environment-friendly stiffening agent for yarn fabric |
| CN107280099A (en) * | 2017-07-14 | 2017-10-24 | 上海喜眠服饰有限公司 | Rapid-curing cutback is perspired not catch a cold nightwear and its preparation technology |
| CN107558226A (en) * | 2016-07-01 | 2018-01-09 | 顾香 | Water-soluble wrinkle resistance finishing agent |
| CN107558227A (en) * | 2016-07-01 | 2018-01-09 | 顾香 | Silk broadcloth crease proofing agent |
| CN107558222A (en) * | 2016-07-01 | 2018-01-09 | 顾香 | Water-soluble finishing agent |
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Cited By (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103757909A (en) * | 2013-12-21 | 2014-04-30 | 成都德美精英化工有限公司 | Non-ionic stiffening agent and preparation method thereof |
| CN103757909B (en) * | 2013-12-21 | 2015-11-25 | 成都德美精英化工有限公司 | A kind of nonionic stiffening agent and preparation method thereof |
| EP3009020A1 (en) * | 2014-10-17 | 2016-04-20 | COFEMEL - Sociedade de Vestuário S.A. | Garment and manufacturing method |
| US11147321B2 (en) | 2014-10-17 | 2021-10-19 | COFEMEL—Sociedade de Vestuário, S.A. | Garment and manufacturing method |
| US10463084B2 (en) | 2014-10-17 | 2019-11-05 | COFEMEL—Sociedade de Vestuário, S.A. | Garment and manufacturing method |
| CN104532609A (en) * | 2014-12-11 | 2015-04-22 | 江门市宝发纺织服饰制造有限公司 | Printing paste for locking jeans elasticity and preventing bleaching and application thereof |
| CN105926295A (en) * | 2016-05-30 | 2016-09-07 | 太仓红桥服饰有限公司 | Finishing liquid applied to crumple finishing of jean costume |
| CN107558222A (en) * | 2016-07-01 | 2018-01-09 | 顾香 | Water-soluble finishing agent |
| CN107558227A (en) * | 2016-07-01 | 2018-01-09 | 顾香 | Silk broadcloth crease proofing agent |
| CN107558226A (en) * | 2016-07-01 | 2018-01-09 | 顾香 | Water-soluble wrinkle resistance finishing agent |
| CN106400464A (en) * | 2016-11-24 | 2017-02-15 | 肇庆高新区飞越信息科技有限公司 | Green and environment-friendly stiffening agent for yarn fabric |
| CN107280099B (en) * | 2017-07-14 | 2019-05-24 | 上海喜眠服饰有限公司 | Rapid-curing cutback is perspired not catch a cold nightwear and its preparation process |
| CN107280099A (en) * | 2017-07-14 | 2017-10-24 | 上海喜眠服饰有限公司 | Rapid-curing cutback is perspired not catch a cold nightwear and its preparation technology |
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