CN103468553A - Method for producing cordyceps sinensis health-preserving liquor - Google Patents

Method for producing cordyceps sinensis health-preserving liquor Download PDF

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CN103468553A
CN103468553A CN201310476031XA CN201310476031A CN103468553A CN 103468553 A CN103468553 A CN 103468553A CN 201310476031X A CN201310476031X A CN 201310476031XA CN 201310476031 A CN201310476031 A CN 201310476031A CN 103468553 A CN103468553 A CN 103468553A
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wine
diacolation
caterpillar fungus
chinese caterpillar
preserving
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CN103468553B (en
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易彬
周军
李云辉
黄张君
代汉聪
陈永利
代小雪
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Luzhou Pinchuang Technology Co Ltd
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Abstract

The invention discloses a method for producing cordyceps sinensis health-preserving liquor, and belongs to the field of health-care liquor. The method comprises the following steps of: a, treating raw materials, namely crushing cordyceps sinensis; b, extracting cordyceps sinensis percolation crude solution from the crushed cordyceps sinensis by virtue of a circulating percolation technology, and settling to obtain cordyceps sinensis percolation stock solution; c, performing liquor body design on the cordyceps sinensis percolation stock solution to obtain the cordyceps sinensis health-preserving liquor. According to the method, a chemical reagent is not added, so that the cordyceps sinensis health-preserving liquor has a better sense and is more suitable for consumer drinking, and a new choice is provided to preparation of cordyceps sinensis liquor.

Description

The production method of cordyceps health-preserving wine
Technical field
The invention belongs to the health promoting wine field, be specifically related to a kind of production method of cordyceps health-preserving wine.
Background technology
Chinese caterpillar fungus is a kind of traditional rare traditional Chinese medicine, with natural ginseng, pilose antler, is listed as three large tonics.Property of medicine gentleness, old and young sick and weak all suitable, compare other tonic and there is higher pharmaceutical use.
Along with the development in epoch, Chinese caterpillar fungus obtains greatly effectively utilizing, and the cordycepin contained in Chinese caterpillar fungus, Cordyceps polysaccharide have high utility value, more and more are subject to human consumer's approval.Although Chinese caterpillar fungus, cordyceps militaris liquor, cordycepin, Cordyceps polysaccharide market potential are huge, be subject to the restriction of Chinese caterpillar fungus wild resource, it is extremely unpractical utilizing merely the products such as wild Chinese caterpillar fungus process for processing cordyceps militaris liquor, Cordyceps polysaccharide to meet the growing needs of the mankind.
Cordyceps militaris (L.) Link. is the example that artificial culture is the most successful, be Chinese caterpillar fungus belong to the xenogenesis fungi together, the two chemical composition, nutritive ingredient and medicinal function are extremely similar, it is the best substitute of Chinese caterpillar fungus, owing to can manually bringing up, Cordyceps militaris (L.) Link. progresses into people's the visual field, and is effectively utilized.
At present, about the patent that is prepared with of cordyceps militaris liquor: CN102604804A, by the method for fermenting, prepare cordyceps militaris liquor; CN93103815.4, compound " hot dipping method " is processed and is obtained cordyceps militaris liquor.Nowadays the Chinese caterpillar fungus raw material is mainly the Cordyceps militaris (L.) Link. of artificial culture, on quality and output, is protected, and treatment process is mainly that infusion method obtains cordyceps militaris liquor.Present method is to extract the effective constituent in Cordyceps militaris (L.) Link. by Digital Extraction technology-percolation, and a kind of pure natural extracting method obtains percolate, utilizes modern wine body designing technique, obtains being applicable to the cordyceps health-preserving wine that the human consumer drinks happily.
Summary of the invention
Technical problem to be solved by this invention be to provide a kind of sense organ better, be more suitable for the cordyceps health-preserving method for preparing wine that the human consumer drinks.
The technical solution adopted for the present invention to solve the technical problems is: the production method of cordyceps health-preserving wine comprises the steps:
A, raw material are processed: Chinese caterpillar fungus is pulverized;
B, the Chinese caterpillar fungus after pulverizing is extracted and obtains the thick liquid of Chinese caterpillar fungus diacolation by the circulatory displacement technology, then process and obtain Chinese caterpillar fungus diacolation stoste through sedimentation;
C, Chinese caterpillar fungus diacolation stoste is carried out to wine body design obtain cordyceps health-preserving wine.
Chinese caterpillar fungus of the present invention can be wild Chinese caterpillar fungus, can be also the Cordyceps militaris (L.) Link. of artificial culture.
Wine body design is blent Chinese caterpillar fungus diacolation stoste and base wine exactly, and teacher of the sampling wine by specialty determines best mouthfeel and ratio.
Wherein, in aforesaid method step a, the granularity that Chinese caterpillar fungus is pulverized is-20 orders.
Wherein, in aforesaid method step b, the solid-liquid ratio that diacolation extracts is 1 ︰ 15~25.
Wherein, in aforesaid method step b, the time that diacolation extracts is that 50~70 hours, base wine concentration are 55~65%vol.
Wherein, in aforesaid method step b, the temperature that sedimentation is processed is 10~14 hours for-4~0 ℃, time.
Wherein, in aforesaid method step c, the scheme of wine body design is Chinese caterpillar fungus diacolation stoste 0.01~0.1%, base wine 99.9~99.99%.
Wherein, in aforesaid method step c, in the design of wine body, the concentration of base wine is 60~65%vol.
Further, in step c, wine body design is the former liquid hold-up 0.05% of Chinese caterpillar fungus diacolation, base wine content 99.95%; Concentration 60~the 65%vol of described base wine, total acid content 0.40~0.50%, total ester content 2.30~2.50%, ethyl acetate content 0.50~0.60%.
Further, the wine of base described in step c giving off a strong fragrance is outstanding, mellow, pure and sweet.
Wherein, in aforesaid method step c, Chinese caterpillar fungus diacolation stoste is carried out after the design of wine body at-4~0 ℃ of temperature to sedimentation 10~14 hours, refilter and obtain cordyceps health-preserving wine.
The present invention specifically can implement in such a way: the production method of cordyceps health-preserving wine comprises the steps:
A, raw material are processed: Chinese caterpillar fungus is crushed to-20 orders;
B, the Chinese caterpillar fungus after pulverizing is extracted and obtains the thick liquid of Chinese caterpillar fungus diacolation by the circulatory displacement technology, then process and obtain Chinese caterpillar fungus diacolation stoste through sedimentation; The solid-liquid ratio that diacolation extracts is 1 ︰ 15~25, and the time that diacolation extracts is that 50~70 hours, base wine concentration are 55~65%vol; The temperature that sedimentation is processed is 10~14 hours for-4~0 ℃, time;
C, Chinese caterpillar fungus diacolation stoste is carried out after the design of wine body at-4~0 ℃ of temperature to sedimentation 10~14 hours, refilter and obtain cordyceps health-preserving wine, wine body design is the former liquid hold-up 0.05% of Chinese caterpillar fungus diacolation, base wine content 99.95%; Concentration 60~the 65%vol of described base wine, total acid content 0.40~0.50%, total ester content 2.30~2.50%, ethyl acetate content 0.50~0.60%.
Further, the wine of base described in step c giving off a strong fragrance is outstanding, mellow, pure and sweet.
The invention has the beneficial effects as follows: the present invention effectively extracts the functional component (cordycepin, Cordyceps polysaccharide etc.) in Chinese caterpillar fungus by the circulatory displacement technology, thereby then by modern liquor wine body designing technique obtain sense organ better, be more suitable for the cordyceps health-preserving wine that the human consumer drinks; The inventive method is the process of a pure ecology, does not add any chemical reagent, and the preparation that the present invention is cordyceps militaris liquor provides a kind of new selection.
Embodiment
Below by embodiment, the invention will be further described.
The production method of cordyceps health-preserving wine of the present invention, comprise the steps:
A, raw material are processed: Chinese caterpillar fungus is pulverized;
B, the Chinese caterpillar fungus after pulverizing is extracted and obtains the thick liquid of Chinese caterpillar fungus diacolation by the circulatory displacement technology, then process and obtain Chinese caterpillar fungus diacolation stoste through sedimentation;
C, Chinese caterpillar fungus diacolation stoste is carried out to wine body design obtain cordyceps health-preserving wine.
Under normal conditions, thinner to crushing material, it is all the extraction more be conducive to useful matter in material, but the contriver finds by research, Chinese caterpillar fungus is pulverized, in process that circulatory displacement extracts, pulverize too slightly or the too thin extraction that is unfavorable on the contrary the Chinese caterpillar fungus functional component, therefore, the present invention is preferably in aforesaid method step a, and the granularity that Chinese caterpillar fungus is pulverized is-20 orders.Under this granularity, than being easier to diacolation, in the thick liquid of Chinese caterpillar fungus diacolation obtained, functional component content is relatively the highest, has obtained unforeseeable technique effect.
Preferably, for the raising cordycepin that can try one's best, the recovery rate of Cordyceps polysaccharide, also can access the thick liquid of Chinese caterpillar fungus diacolation that concentration is higher in the diacolation process, in aforesaid method step b, the solid-liquid ratio that diacolation extracts is 1 ︰ 15~25 simultaneously.
Preferably, in aforesaid method step b, the time that diacolation extracts is that 50~70 hours, base wine concentration are 55~65%vol.
Preferably, in aforesaid method step b, the temperature that sedimentation is processed is 10~14 hours for-4~0 ℃, time.Temperature is too high, does not reach the effect of sedimentation, and temperature is too low, can make the thick liquid of Chinese caterpillar fungus diacolation freeze, under settling temperature of the present invention, minimum on the mouthfeel impact of wine sample.
Preferably, better for the cordyceps health-preserving wine sense organ that can make to obtain, in aforesaid method step c, the scheme of wine body design is Chinese caterpillar fungus diacolation stoste 0.01~0.1%, base wine 99.9~99.99%.
Further, in aforesaid method step c, in the design of wine body, the concentration of base wine is 60~65%vol.
Most preferred, in step c, wine body design is the former liquid hold-up 0.05% of Chinese caterpillar fungus diacolation, base wine content 99.95%; Concentration 60~the 65%vol of described base wine, total acid content 0.40~0.50%, total ester content 2.30~2.50%, ethyl acetate content 0.50~0.60%.
Preferably, for the cordyceps health-preserving wine that makes to obtain, more clarify, sense organ is better, in aforesaid method step c, Chinese caterpillar fungus diacolation stoste is carried out after the design of wine body at-4~0 ℃ of temperature to sedimentation 10~14 hours, refilters and obtains cordyceps health-preserving wine.
Below by embodiment, the specific embodiment of the invention is further described, but therefore protection scope of the present invention is not limited among embodiment.
Embodiment mono-use the inventive method is produced cordyceps health-preserving wine
Raw material is processed: utilize HX-200 type medicinal herb grinder to be pulverized dry raw material Chinese caterpillar fungus, the granularity that Chinese caterpillar fungus is pulverized is-20 orders.
Diacolation: at first utilize the base wine of 60%vol that Chinese caterpillar fungus raw material wetting (base wine and Chinese caterpillar fungus material rate are 1:2) is convenient to charging, the diacolation pipe of secondly wetting raw material slowly being packed into, have space in the prevention feed liquid.According to solid-liquid ratio 1:20, get the base wine 6000ml of 60%vol, utilize base wine that the Chinese caterpillar fungus raw material on the bottle wall is flushed in the diacolation pipe, charging completes.Again the diacolation pipe is placed at normal temperatures to diacolation after 60h, diacolation speed is 2-3ml/min, and by 3 circulatory displacements, the cordycepin yield is 85%, and the Cordyceps polysaccharide yield is 80%, and functional component extracts and reaches maximization, and the diacolation effect is good.
Sedimentation is processed: carry out the natural subsidence processing after the stoste of 3 diacolations is mixed, at first be placed on-4~0 ℃ of lower natural subsidence 12h, place 24h at normal temperatures after filtration.Again mixed solution is placed on to-4~0 ℃ of lower natural subsidence 12h, obtains the stoste of clarification after filtration.
Wine body design: main base wine has 3 kinds, and being respectively base wine 1(is base wine of the present invention), base wine 2, base wine 3, its physical and chemical index and sense organ appraise are in Table 1.Chinese caterpillar fungus stoste is carried out to the design of wine body, and scheme and appraise the results are shown in Table 2.
The index of each base wine of table 1 and sense organ appraise
The design of table 2 wine body and appraise result
The wine body that in the design of wine body, scheme 6 obtains is placed on to natural subsidence 12h in-4 ℃ of environment, recycles after small-sized chip filter filters the cordyceps health-preserving wine that can obtain clarification.
The impact of the different grinding particle size of comparative example one on diacolation
Adopt respectively two schemes: 1, do not pulverize diacolation, 2, fully pulverize after diacolation, be about to Chinese caterpillar fungus and be crushed to-100 orders.The diacolation mode adopts the mode of embodiment mono-, parameter constant.Diacolation after pulverizing fully, sense organ: almost without flavour of a drug, the functional component yield is on average 20%; Do not pulverize the processing mode of diacolation, no matter on wine sample mouthfeel and functional component extraction yield, do not reach requirement fully, yield on average only has 20% left and right.
The effect comparison of comparative example's two differing temps sedimentations
The stoste that embodiment is obtained is carried out sedimentation under differing temps, and effect is as shown in table 3:
Table 3 differing temps effect of settling contrast table
Figure BDA0000394599250000051

Claims (9)

1. the production method of cordyceps health-preserving wine, is characterized in that comprising the steps:
A, raw material are processed: Chinese caterpillar fungus is pulverized;
B, the Chinese caterpillar fungus after pulverizing is extracted and obtains the thick liquid of Chinese caterpillar fungus diacolation by the circulatory displacement technology, then process and obtain Chinese caterpillar fungus diacolation stoste through sedimentation;
C, Chinese caterpillar fungus diacolation stoste is carried out to wine body design obtain cordyceps health-preserving wine.
2. the production method of cordyceps health-preserving wine according to claim 1 is characterized in that: in step a, the granularity that Chinese caterpillar fungus is pulverized is-20 orders.
3. the production method of cordyceps health-preserving wine according to claim 1 is characterized in that: in step b, the solid-liquid ratio that diacolation extracts is 1 ︰ 15~25.
4. the production method of cordyceps health-preserving wine according to claim 3 is characterized in that: in step b, the time that diacolation extracts is that 50~70 hours, base wine concentration are 55~65%vol.
5. the production method of cordyceps health-preserving wine according to claim 1 is characterized in that: in step b, the temperature that sedimentation is processed is 10~14 hours for-4~0 ℃, time.
6. according to the production method of the described cordyceps health-preserving wine of any one in claim 1 to 5, it is characterized in that: in step c, the scheme of wine body design is Chinese caterpillar fungus diacolation stoste 0.01~0.1%, base wine 99.9~99.99%.
7. the production method of cordyceps health-preserving wine according to claim 6 is characterized in that: in step c, in the design of wine body, the concentration of base wine is 60~65%vol.
8. the production method of cordyceps health-preserving wine according to claim 7, it is characterized in that: in step c, wine body design is the former liquid hold-up 0.05% of agate coffee diacolation, base wine content 99.95%; Concentration 60~the 65%vol of described base wine, total acid content 0.40~0.50%, total ester content 2.30~2.50%, ethyl acetate content 0.50~0.60%.
9. according to the production method of the described cordyceps health-preserving wine of any one in claim 1 to 5, it is characterized in that: in step c, Chinese caterpillar fungus diacolation stoste is carried out after the design of wine body at-4~0 ℃ of temperature to sedimentation 10~14 hours, refilter and obtain cordyceps health-preserving wine.
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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103865740A (en) * 2014-04-03 2014-06-18 泸州品创科技有限公司 Production method of yam wine
CN104593210A (en) * 2015-01-28 2015-05-06 王永新 Maca and cordyceps sinensis milk wine and making method thereof
CN107267348A (en) * 2017-08-24 2017-10-20 宜智萱(天津)生物科技有限公司 A kind of new aweto yellow wine preparation method

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103865740A (en) * 2014-04-03 2014-06-18 泸州品创科技有限公司 Production method of yam wine
CN103865740B (en) * 2014-04-03 2016-01-27 泸州品创科技有限公司 A kind of production method of yam wine
CN104593210A (en) * 2015-01-28 2015-05-06 王永新 Maca and cordyceps sinensis milk wine and making method thereof
CN107267348A (en) * 2017-08-24 2017-10-20 宜智萱(天津)生物科技有限公司 A kind of new aweto yellow wine preparation method

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