CN103468378B - A kind of multi-usage magnalium wire drawing oil - Google Patents
A kind of multi-usage magnalium wire drawing oil Download PDFInfo
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- CN103468378B CN103468378B CN201310372391.5A CN201310372391A CN103468378B CN 103468378 B CN103468378 B CN 103468378B CN 201310372391 A CN201310372391 A CN 201310372391A CN 103468378 B CN103468378 B CN 103468378B
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Abstract
A multi-usage magnalium wire drawing oil, is made up of the raw material of following weight part: 2-mercaptobenzimidazole 1-2, hydrogenated castor oil 12-14, tritolyl phosphate 2-3, benzotriazole 1-2, dibutyl terephthalate 2-3, the acid of pungent certain herbaceous plants with big flowers 1-2, sodium lauryl sulphate 1-2, ethyl acetate 4-5, tertbutyl peroxide 1-2, modification aluminium nitride powder 2-3, water 1200.
Description
Technical field
The present invention relates to magnalium wire wire-drawing technology field, is a kind of multi-usage magnalium wire drawing oil and preparation method thereof.
Background technology
In existing drawing process, the lubricating oil that adopts as wire drawing medium more, and the conductive line surfaces that drawing goes out is mellow and full, fine and smooth, smooth, bright, no-sundries is detained, and wire broken rate reduces, and quality product improves greatly.But lubricating oil heat radiation is slow, damage mould, affect quality product, while high temperature easily to ignite oil product or oil evaporation is smoldered cause site environment to worsen.
Summary of the invention
The object of this invention is to provide a kind of multi-usage magnalium wire drawing oil, it has, and film forming properties is good, lubricant effect is good, feature.
Technical scheme of the present invention is as follows:
A multi-usage magnalium wire drawing oil, is characterized in that being made up of the raw material of following weight part: 2-mercaptobenzimidazole 1-2, hydrogenated castor oil 12-14, tritolyl phosphate 2-3, benzotriazole 1-2, dibutyl terephthalate 2-3, the acid of pungent certain herbaceous plants with big flowers 1-2, sodium lauryl sulphate 1-2, ethyl acetate 4-5, tertbutyl peroxide 1-2, modification aluminium nitride powder 2-3, water 1200;
Modification aluminium nitride powder is made up of the raw material of following weight part:
Wintergreen oil 2.1-3.2, dioctyl sebacate 0.2-0.4, nitrocellulose 1.5-1.8, Sodium Persulfate 1-1.2, di-n-octyl-4-isothiazoline-3-ketone 0.1-0.2, citric acid 2.1-2.3, morpholine 1.2-1.4, nano-sized carbon 0.1-0.2, nano aluminum nitride powder 3.0-3.5, silane coupling agent KH7920.7-1.3, Sodium dodecylbenzene sulfonate 0.4-0.6, polyvinylpyrrolidone 1.2-1.4, water 40-50;
The preparation method of described modification aluminium nitride powder is as follows: nitrocellulose, citric acid, morpholine are dissolved in the water, are heated to 80-85 DEG C, then add Sodium Persulfate, stirring reaction 15-20 minute, then, then add wintergreen oil, Sodium dodecylbenzene sulfonate, 1200-1500 rev/min is stirred 30-45 minute, then, add other surplus stock, be warming up to 90-95 DEG C, 1200-1500 rev/min of stirring reaction 40-50 minute, dry, abrasive dust and get final product.
Described multi-usage magnalium wire drawing oil, is characterized in that, preparation method is as follows: first hydrogenated castor oil, tritolyl phosphate are added to the water, are heated to 45-55 DEG C, stirring reaction 20-30 minute, then, then add dibutyl terephthalate, pungent certain herbaceous plants with big flowers acid, stir 10-15 minute at 35-42 DEG C after, drip tertbutyl peroxide, stirring reaction 20-30 minute, then add all the other raw materials, be warming up to 60-70 DEG C, 700-800 rev/min is continued stirring reaction 1-2 hour, to obtain final product.
Beneficial effect of the present invention is:
The present invention adds modified nano aluminum nitride powder and plays promotion thermolysis, adds film-forming properties, and product oil product volatility of the present invention is little, flash-point is higher, and antioxidant property is fabulous, not only improves oil product processing characteristics after adding multiple additives, not easily catch fire simultaneously, improve safety in utilization.
Embodiment
A multi-usage magnalium wire drawing oil, is made up of the raw material of following weight part (kg): 2-mercaptobenzimidazole 1.2, hydrogenated castor oil 12, tritolyl phosphate 2, benzotriazole 1.4, dibutyl terephthalate 3, pungent certain herbaceous plants with big flowers acid 1, sodium lauryl sulphate 2, ethyl acetate 4, tertbutyl peroxide 2, modification aluminium nitride powder 3, water 1200;
Modification aluminium nitride powder is made up of the raw material of following weight part:
Wintergreen oil 2.1, dioctyl sebacate 0.4, nitrocellulose 1.8, Sodium Persulfate 1.2, di-n-octyl-4-isothiazoline-3-ketone 0.2, citric acid 2.3, morpholine 1.4, nano-sized carbon 0.2, nano aluminum nitride powder 3.1, silane coupling agent KH7920.7, Sodium dodecylbenzene sulfonate 0.6, polyvinylpyrrolidone 1.4, water 40;
The preparation method of described modification aluminium nitride powder is as follows: nitrocellulose, citric acid, morpholine are dissolved in the water, and is heated to 82 DEG C, then adds Sodium Persulfate, stirring reaction 15 minutes, then, then add wintergreen oil, Sodium dodecylbenzene sulfonate, 1200 revs/min are stirred 35 minutes, then, add other surplus stock, be warming up to 90 DEG C, 1500 revs/min of stirring reactions 50 minutes, dry, abrasive dust and get final product.
Described multi-usage magnalium wire drawing oil, preparation method is as follows: first hydrogenated castor oil, tritolyl phosphate are added to the water, and is heated to 45 DEG C, stirring reaction 30 minutes, then, then add dibutyl terephthalate, the acid of pungent certain herbaceous plants with big flowers, stir at 35 DEG C after 10 minutes, drip tertbutyl peroxide, stirring reaction 30 minutes, then add all the other raw materials, be warming up to 60 DEG C, 800 revs/min are continued stirring reaction 2 hours, to obtain final product.
Use the present embodiment, the highest drawing speed can reach 18m/sec.The copper wire rust prevention during manufacture time of producing is more than 6 days; Concentrate the oil sump drain period to be 3 years, the unit oil sump drain period is 8 months, decreases liquid waste disposal and discharge, protects environment.
Claims (2)
1. a multi-usage magnalium wire drawing oil, is made up of the raw material of following weight part: 2-mercaptobenzimidazole 1.2kg, hydrogenated castor oil 12kg, tritolyl phosphate 2kg, benzotriazole 1.4kg, dibutyl terephthalate 3kg, the acid of pungent certain herbaceous plants with big flowers 1kg, sodium lauryl sulphate 2kg, ethyl acetate 4kg, tertbutyl peroxide 2kg, modification aluminium nitride powder 3kg, water 1200kg;
Modification aluminium nitride powder is made up of the raw material of following weight part:
Wintergreen oil 2.1 parts, dioctyl sebacate 0.4 part, 1.8 parts, nitrocellulose, Sodium Persulfate 1.2 parts, di-n-octyl-4-isothiazoline-3-ketone 0.2 part, citric acid 2.3 parts, morpholine 1.4 parts, nano-sized carbon 0.2 part, nano aluminum nitride powder 3.1 parts, silane coupling agent KH7920.7 part, Sodium dodecylbenzene sulfonate 0.6 part, polyvinylpyrrolidone 1.4 parts, 40 parts, water;
The preparation method of described modification aluminium nitride powder is as follows: nitrocellulose, citric acid, morpholine are dissolved in the water, and is heated to 82 DEG C, then adds Sodium Persulfate, stirring reaction 15 minutes, then, then add wintergreen oil, Sodium dodecylbenzene sulfonate, 1200 revs/min are stirred 35 minutes, then, add other surplus stock, be warming up to 90 DEG C, 1500 revs/min of stirring reactions 50 minutes, dry, abrasive dust and get final product.
2. multi-usage magnalium wire drawing oil according to claim 1, it is characterized in that, preparation method is as follows: first hydrogenated castor oil, tritolyl phosphate are added to the water, be heated to 45-55 DEG C, stirring reaction 20-30 minute, then, add dibutyl terephthalate, the acid of pungent certain herbaceous plants with big flowers again, stir 10-15 minute at 35-42 DEG C after, drip tertbutyl peroxide, stirring reaction 20-30 minute, add all the other raw materials again, be warming up to 60-70 DEG C, 700-800 rev/min is continued stirring reaction 1-2 hour, to obtain final product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310372391.5A CN103468378B (en) | 2013-08-24 | 2013-08-24 | A kind of multi-usage magnalium wire drawing oil |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201310372391.5A CN103468378B (en) | 2013-08-24 | 2013-08-24 | A kind of multi-usage magnalium wire drawing oil |
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| CN103468378A CN103468378A (en) | 2013-12-25 |
| CN103468378B true CN103468378B (en) | 2016-03-09 |
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Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102925266A (en) * | 2012-11-13 | 2013-02-13 | 南宁飞日润滑科技有限公司 | Multipurpose aluminum-magnesium drawing oil and production method thereof |
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- 2013-08-24 CN CN201310372391.5A patent/CN103468378B/en active Active
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102925266A (en) * | 2012-11-13 | 2013-02-13 | 南宁飞日润滑科技有限公司 | Multipurpose aluminum-magnesium drawing oil and production method thereof |
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