CN104046455B - A kind of anti-corrosion, scale-inhibiting magnadure wire drawing liquid - Google Patents

A kind of anti-corrosion, scale-inhibiting magnadure wire drawing liquid Download PDF

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Publication number
CN104046455B
CN104046455B CN201410122607.7A CN201410122607A CN104046455B CN 104046455 B CN104046455 B CN 104046455B CN 201410122607 A CN201410122607 A CN 201410122607A CN 104046455 B CN104046455 B CN 104046455B
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stir
wire drawing
drawing liquid
sodium
deionized water
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CN104046455A (en
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鲍熊
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Anhui Shuo Li Industrial Co Ltd
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Anhui Shuo Li Industrial Co Ltd
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Abstract

The present invention relates to a kind of wire drawing liquid, be specifically related to a kind of anti-corrosion, scale-inhibiting magnadure wire drawing liquid, wire drawing liquid of the present invention is made up of the raw material of following weight portion: rilanit special 28-32, benzotriazole sodium 2-3, algal polysaccharides 2-3, trimethylolpropane tris oleate 15-18, butylated hydroxy anisole 4-6, sodium lactate 2-3, coptis extract 1-2, potassium dihydrogen phosphate 1-2, laurate polyoxyethylene ester 6-8, Rosmarinic acid 1-2, sulfuration paraffin 2-3, auxiliary agent 4-5, deionized water 800-1000; The base oil of wire drawing liquid of the present invention has good high temperature lubricating, add algal polysaccharides can effectively slow down Oxidation of Fat and Oils, can also with complexing of metal ion, avoid Integrated Chip on mould, coptis extract, Rosmarinic acid are the bioactivators of two class natural environmental-protectives, have antibacterial anticorrosion, oxidation resistant effect, wire drawing liquid wire-drawing effect of the present invention is good, wire surface no marking, and peace and quiet power is high, mould is difficult for incrustation, under normal temperature, be difficult for putrid and deteriorated, long service life.

Description

A kind of anti-corrosion, scale-inhibiting magnadure wire drawing liquid
Technical field
The present invention relates to a kind of wire drawing liquid, be specifically related to a kind of anti-corrosion, scale-inhibiting magnadure wire drawing liquid and preparation technology thereof.
Background technology
Drawing process is a kind of metal working process, refer to that metal wire rod passes through mould under pressure by force, obtain the technology processing method of desired sectional area shape and size, wire drawing liquid is requisite adjuvant in drawing process, its main effect is at multiple copper wire, in the multiple wire rod of aluminium wire, draw, little drawing, finely the wire drawing such as draw, lubricate in bracing wire technical process, have protection wire rod concurrently, mould, reach good wire-drawing effect, the quality of wire drawing liquid directly has influence on wire-drawing effect, the wire drawing liquid of function admirable can well be protected mould, reduce wire rod broken end, die wear phenomenon, have concurrently antirust, cooling, the effects such as cleaning, otherwise, can have a strong impact on wire drawing quality, along with the application of drawing process is extensive gradually, market is more and more higher to the quality demand of wire drawing liquid, existing wire drawing liquid mainly exists that stability of emulsion is poor, corroding metal wire rod, energy consumption are high, the problem such as easy cleaning not, restricting wire drawing, drawing quality, be badly in need of improving its composition and engineering, make its more high-efficiency environment friendly.
Summary of the invention
The object of the invention is to, a kind of anti-corrosion, scale-inhibiting magnadure wire drawing liquid is provided, to achieve these goals, the technical solution used in the present invention is as follows:
A kind of anti-corrosion, scale-inhibiting magnadure wire drawing liquid, it is characterized in that, material of the present invention is made up of the raw material of following weight portion: rilanit special 28-32, benzotriazole sodium 2-3, algal polysaccharides 2-3, trimethylolpropane tris oleate 15-18, butylated hydroxy anisole 4-6, sodium lactate 2-3, coptis extract 1-2, potassium dihydrogen phosphate 1-2, laurate polyoxyethylene ester 6-8, Rosmarinic acid 1-2, sulfuration paraffin 2-3, auxiliary agent 4-5, deionized water 800-1000;
Described auxiliary agent is made up of the raw material of following weight portion: epoxidized soybean oil 12-15, pyrophyllite 2-3, polyisobutenyl succimide 3-4, sodium phosphate trimer 0.02-0.05, Sodium Polyacrylate 0.1-0.2, Silane coupling agent KH550 0.01-0.02, chlorinated paraffin wax 421-2, polyglyceryl fatty acid ester 1-2, deionized water 12-15, preparation method is: first by pyrophyllite high-temperature calcination 2-3h at 750-800 DEG C, after cooling, grind to form 300 order powders, powder mixes with Silane coupling agent KH550, after ball milling 10-15min, with sodium phosphate trimer, Sodium Polyacrylate adds in deionized water together, stir 20-30min with the rotating speed of 500-600 rev/min, subsequently solution is sprayed dry, the powder obtaining mixes with other leftover materials, be heated to 40-50 DEG C, continue to stir 40-50min, stir and finish to be cooled to room temperature, obtain slurry.
Described a kind of anti-corrosion, scale-inhibiting magnadure wire drawing liquid, its preparation technology is:
(1) first deionized water is heated to 50-60 DEG C, add algal polysaccharides, potassium dihydrogen phosphate, Rosmarinic acid, be stirred well to material and dissolve dispersion completely, then add sodium lactate, laurate polyoxyethylene ester, continue to stir 20-30min, the mixed solution obtaining insulation is for subsequent use;
(2) rilanit special, trimethylolpropane tris oleate are mixed and heated to 50-60 DEG C, add benzotriazole sodium, coptis extract, sulfuration paraffin, stir 20-30min with the rotating speed of 1200-1500 rev/min, continue subsequently to stir on one side, slowly add step (1) gained material on one side, stir 40-50min, finally add other leftover materials, stir 20-30min, stir and finish rear standing 2-3h, get product.
Wire drawing liquid advantage prepared by the present invention is: mix as base oil using rilanit special, trimethylolpropane tris oleate, there is good high temperature lubricating, algal polysaccharides is that a class has bioactive material, can effectively slow down Oxidation of Fat and Oils, can also with complexing of metal ion, metal ion in can enrichment solution, thus metal ion sedimentation accelerated, avoid Integrated Chip on mould; Reach scale inhibition effect; In the coptis extract adding, contain the antibacterial substance of multiple high-efficiency broad spectrum, can slow down the corruption of bacterium to wire drawing liquid, it is a kind of bactericide of inexpensive efficient Nantural non-toxic, in addition Rosmarinic acid is also the natural multi-functional phenolic acid class of a class, there is antibacterial oxidation resistant effect, again in conjunction with other class additive, make wire drawing liquid of the present invention there is good greasy property, anti-extreme pressure is wear-resisting, the wire surface no marking obtaining, and peace and quiet power is high, and mould is difficult for incrustation, wire drawing liquid is difficult for putrid and deteriorated at normal temperatures, and extended service life.
Detailed description of the invention
Embodiment
The present embodiment wire drawing liquid by following weight portion (kilogram) raw material make: rilanit special 32, benzotriazole sodium 3, algal polysaccharides 2, trimethylolpropane tris oleate 18, butylated hydroxy anisole 6, sodium lactate 3, coptis extract 1, potassium dihydrogen phosphate 2, laurate polyoxyethylene ester 8, Rosmarinic acid 2, sulfuration paraffin 3, auxiliary agent 5, deionized water 1000;
Auxiliary agent is made up of the raw material of following weight portion: epoxidized soybean oil 12, pyrophyllite 3, polyisobutenyl succimide 4, sodium phosphate trimer 0.05, Sodium Polyacrylate 0.1, Silane coupling agent KH550 0.02, chlorinated paraffin wax 422, polyglyceryl fatty acid ester 2, deionized water 15, preparation method is: first by pyrophyllite high-temperature calcination 3h at 750-800 DEG C, after cooling, grind to form 300 order powders, powder mixes with Silane coupling agent KH550, after ball milling 15min, with sodium phosphate trimer, Sodium Polyacrylate adds in deionized water together, stir 30min with the rotating speeds of 600 revs/min, subsequently solution is sprayed dry, the powder obtaining mixes with other leftover materials, be heated to 40-50 DEG C, continue to stir 50min, stir and finish to be cooled to room temperature, obtain slurry.
Described a kind of anti-corrosion, scale-inhibiting magnadure wire drawing liquid, its preparation technology is:
(1) first deionized water is heated to 50-60 DEG C, add algal polysaccharides, potassium dihydrogen phosphate, Rosmarinic acid, be stirred well to material and dissolve dispersion completely, then add sodium lactate, laurate polyoxyethylene ester, continue to stir 30min, the mixed solution obtaining insulation is for subsequent use;
(2) rilanit special, trimethylolpropane tris oleate are mixed and heated to 50-60 DEG C, add benzotriazole sodium, coptis extract, sulfuration paraffin, stir 30min with the rotating speeds of 1500 revs/min, continue subsequently to stir on one side, slowly add step (1) gained material on one side, stir 50min, finally add other leftover materials, stir 200min, stir and finish rear standing 3h, get product.
Wire drawing liquid of the present invention can be stored more than at least 18 months at normal temperatures, more than changing liquid cycle stretch-out to 10 month, is difficult for broken string when wire drawing, the bright and clean no marking of wire surface, and cone pulley cabling is unobstructed, and its concrete test performance index is as follows:
Project Index
Kinematic viscosity (50 DEG C) ≤100mm2/s
Condensation point ≤-5℃
PH value 8.7
Emulsion corrosion (55 ± 2) DEG C, soaks copper sheet 1h entirely Qualified
Emulsion stability (15-35 DEG C) 1h Without layering, without precipitation, separate out without soap, oil
Defoaming (55 ± 2 DEG C, 5min) ≤2mL

Claims (2)

1. an anti-corrosion, scale-inhibiting magnadure wire drawing liquid, it is characterized in that, this wire drawing liquid is made up of the raw material of following weight portion: rilanit special 28-32, benzotriazole sodium 2-3, algal polysaccharides 2-3, trimethylolpropane tris oleate 15-18, butylated hydroxy anisole 4-6, sodium lactate 2-3, coptis extract 1-2, potassium dihydrogen phosphate 1-2, laurate polyoxyethylene ester 6-8, Rosmarinic acid 1-2, sulfuration paraffin 2-3, auxiliary agent 4-5, deionized water 800-1000;
Described auxiliary agent is made up of the raw material of following weight portion: epoxidized soybean oil 12-15, pyrophyllite 2-3, polyisobutenyl succimide 3-4, sodium phosphate trimer 0.02-0.05, Sodium Polyacrylate 0.1-0.2, Silane coupling agent KH550 0.01-0.02, chlorinated paraffin wax 421-2, polyglyceryl fatty acid ester 1-2, deionized water 12-15, preparation method is: first by pyrophyllite high-temperature calcination 2-3h at 750-800 DEG C, after cooling, grind to form 300 order powders, powder mixes with Silane coupling agent KH550, after ball milling 10-15min, with sodium phosphate trimer, Sodium Polyacrylate adds in deionized water together, stir 20-30min with the rotating speed of 500-600 rev/min, subsequently solution is sprayed dry, the powder obtaining mixes with other leftover materials, be heated to 40-50 DEG C, continue to stir 40-50min, stir and finish to be cooled to room temperature, obtain slurry.
2. a kind of anti-corrosion, scale-inhibiting magnadure wire drawing liquid as claimed in claim 1, its preparation technology is as follows:
(1) first deionized water is heated to 50-60 DEG C, add algal polysaccharides, potassium dihydrogen phosphate, Rosmarinic acid, be stirred well to material and dissolve dispersion completely, then add sodium lactate, laurate polyoxyethylene ester, continue to stir 20-30min, the mixed solution obtaining insulation is for subsequent use;
(2) rilanit special, trimethylolpropane tris oleate are mixed and heated to 50-60 DEG C, add benzotriazole sodium, coptis extract, sulfuration paraffin, stir 20-30min with the rotating speed of 1200-1500 rev/min, continue subsequently to stir on one side, slowly add step (1) gained material on one side, stir 40-50min, finally add other leftover materials, stir 20-30min, stir and finish rear standing 2-3h, get product.
CN201410122607.7A 2014-03-28 2014-03-28 A kind of anti-corrosion, scale-inhibiting magnadure wire drawing liquid Active CN104046455B (en)

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CN104528960B (en) * 2014-12-24 2016-07-06 安徽协诚实业股份有限公司 A kind of high efficiency corrosion inhibiting scale retardant
CN105001966B (en) * 2015-06-24 2017-09-08 安阳师范学院 A kind of aluminium and aluminum alloy cutting fluid

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102925266A (en) * 2012-11-13 2013-02-13 南宁飞日润滑科技有限公司 Multipurpose aluminum-magnesium drawing oil and production method thereof

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102925266A (en) * 2012-11-13 2013-02-13 南宁飞日润滑科技有限公司 Multipurpose aluminum-magnesium drawing oil and production method thereof

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