CN1034413C - 使含铅和/或钡的水晶玻璃制品在与液相接触时减少铅和/或钡释放的方法 - Google Patents
使含铅和/或钡的水晶玻璃制品在与液相接触时减少铅和/或钡释放的方法 Download PDFInfo
- Publication number
- CN1034413C CN1034413C CN93106111A CN93106111A CN1034413C CN 1034413 C CN1034413 C CN 1034413C CN 93106111 A CN93106111 A CN 93106111A CN 93106111 A CN93106111 A CN 93106111A CN 1034413 C CN1034413 C CN 1034413C
- Authority
- CN
- China
- Prior art keywords
- acid
- polishing
- lead
- minutes
- alkali metal
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 238000000034 method Methods 0.000 title claims abstract description 32
- 229910052788 barium Inorganic materials 0.000 title claims abstract description 19
- DSAJWYNOEDNPEQ-UHFFFAOYSA-N barium atom Chemical compound [Ba] DSAJWYNOEDNPEQ-UHFFFAOYSA-N 0.000 title claims abstract description 19
- 239000005355 lead glass Substances 0.000 title claims abstract description 13
- 239000007791 liquid phase Substances 0.000 title claims abstract description 5
- 239000002253 acid Substances 0.000 claims abstract description 57
- 239000011521 glass Substances 0.000 claims abstract description 47
- 238000005498 polishing Methods 0.000 claims abstract description 42
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims abstract description 39
- 150000008044 alkali metal hydroxides Chemical class 0.000 claims abstract description 20
- 238000011282 treatment Methods 0.000 claims description 26
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 25
- KRHYYFGTRYWZRS-UHFFFAOYSA-N Fluorane Chemical compound F KRHYYFGTRYWZRS-UHFFFAOYSA-N 0.000 claims description 20
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 claims description 13
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims description 12
- 239000000203 mixture Substances 0.000 claims description 10
- KRHYYFGTRYWZRS-UHFFFAOYSA-M Fluoride anion Chemical compound [F-] KRHYYFGTRYWZRS-UHFFFAOYSA-M 0.000 claims description 6
- MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 claims description 6
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 6
- OFOBLEOULBTSOW-UHFFFAOYSA-N Malonic acid Chemical compound OC(=O)CC(O)=O OFOBLEOULBTSOW-UHFFFAOYSA-N 0.000 claims description 4
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 claims description 4
- FEWJPZIEWOKRBE-UHFFFAOYSA-N Tartaric acid Natural products [H+].[H+].[O-]C(=O)C(O)C(O)C([O-])=O FEWJPZIEWOKRBE-UHFFFAOYSA-N 0.000 claims description 4
- XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 claims description 4
- 238000010494 dissociation reaction Methods 0.000 claims description 4
- 230000005593 dissociations Effects 0.000 claims description 4
- 239000011975 tartaric acid Substances 0.000 claims description 4
- 235000002906 tartaric acid Nutrition 0.000 claims description 4
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 claims description 3
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 claims description 2
- FEWJPZIEWOKRBE-JCYAYHJZSA-N Dextrotartaric acid Chemical compound OC(=O)[C@H](O)[C@@H](O)C(O)=O FEWJPZIEWOKRBE-JCYAYHJZSA-N 0.000 claims description 2
- 229910000147 aluminium phosphate Inorganic materials 0.000 claims description 2
- 229910052810 boron oxide Inorganic materials 0.000 claims description 2
- JKWMSGQKBLHBQQ-UHFFFAOYSA-N diboron trioxide Chemical compound O=BOB=O JKWMSGQKBLHBQQ-UHFFFAOYSA-N 0.000 claims description 2
- FUJCRWPEOMXPAD-UHFFFAOYSA-N lithium oxide Chemical compound [Li+].[Li+].[O-2] FUJCRWPEOMXPAD-UHFFFAOYSA-N 0.000 claims description 2
- 229910001947 lithium oxide Inorganic materials 0.000 claims description 2
- 235000006408 oxalic acid Nutrition 0.000 claims description 2
- 239000002244 precipitate Substances 0.000 claims description 2
- 230000035484 reaction time Effects 0.000 claims description 2
- 239000011787 zinc oxide Substances 0.000 claims description 2
- 239000000047 product Substances 0.000 claims 3
- MFEVGQHCNVXMER-UHFFFAOYSA-L 1,3,2$l^{2}-dioxaplumbetan-4-one Chemical compound [Pb+2].[O-]C([O-])=O MFEVGQHCNVXMER-UHFFFAOYSA-L 0.000 claims 2
- 229910000003 Lead carbonate Inorganic materials 0.000 claims 1
- 235000011089 carbon dioxide Nutrition 0.000 claims 1
- 238000007517 polishing process Methods 0.000 claims 1
- BYTCDABWEGFPLT-UHFFFAOYSA-L potassium;sodium;dihydroxide Chemical compound [OH-].[OH-].[Na+].[K+] BYTCDABWEGFPLT-UHFFFAOYSA-L 0.000 claims 1
- 159000000009 barium salts Chemical class 0.000 abstract description 4
- 230000001476 alcoholic effect Effects 0.000 abstract description 3
- -1 for example Substances 0.000 abstract description 2
- 239000007788 liquid Substances 0.000 abstract description 2
- 235000015041 whisky Nutrition 0.000 abstract description 2
- 235000014101 wine Nutrition 0.000 abstract description 2
- 235000020094 liqueur Nutrition 0.000 abstract 1
- 239000000243 solution Substances 0.000 description 15
- 230000035622 drinking Effects 0.000 description 11
- HTUMBQDCCIXGCV-UHFFFAOYSA-N lead oxide Chemical compound [O-2].[Pb+2] HTUMBQDCCIXGCV-UHFFFAOYSA-N 0.000 description 7
- 238000002203 pretreatment Methods 0.000 description 7
- 238000002474 experimental method Methods 0.000 description 4
- 239000007864 aqueous solution Substances 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 230000002378 acidificating effect Effects 0.000 description 2
- 239000003513 alkali Substances 0.000 description 2
- 239000012670 alkaline solution Substances 0.000 description 2
- 238000004458 analytical method Methods 0.000 description 2
- 238000007796 conventional method Methods 0.000 description 2
- 230000003247 decreasing effect Effects 0.000 description 2
- 230000003628 erosive effect Effects 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- YCKRFDGAMUMZLT-UHFFFAOYSA-N Fluorine atom Chemical compound [F] YCKRFDGAMUMZLT-UHFFFAOYSA-N 0.000 description 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
- 101710169169 Polyprenol monophosphomannose synthase Proteins 0.000 description 1
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 1
- 150000007513 acids Chemical class 0.000 description 1
- 229910052783 alkali metal Inorganic materials 0.000 description 1
- 229910001413 alkali metal ion Inorganic materials 0.000 description 1
- 150000001340 alkali metals Chemical class 0.000 description 1
- 229910052784 alkaline earth metal Inorganic materials 0.000 description 1
- 150000001342 alkaline earth metals Chemical class 0.000 description 1
- 239000011260 aqueous acid Substances 0.000 description 1
- 150000001553 barium compounds Chemical class 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000001569 carbon dioxide Substances 0.000 description 1
- 229910002092 carbon dioxide Inorganic materials 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 230000001419 dependent effect Effects 0.000 description 1
- XGZRAKBCYZIBKP-UHFFFAOYSA-L disodium;dihydroxide Chemical compound [OH-].[OH-].[Na+].[Na+] XGZRAKBCYZIBKP-UHFFFAOYSA-L 0.000 description 1
- 238000004049 embossing Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- 229910052731 fluorine Inorganic materials 0.000 description 1
- 239000011737 fluorine Substances 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- 229910000464 lead oxide Inorganic materials 0.000 description 1
- 239000002932 luster Substances 0.000 description 1
- 239000011259 mixed solution Substances 0.000 description 1
- 230000003287 optical effect Effects 0.000 description 1
- 239000011591 potassium Substances 0.000 description 1
- 229910052700 potassium Inorganic materials 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- KKCBUQHMOMHUOY-UHFFFAOYSA-N sodium oxide Chemical compound [O-2].[Na+].[Na+] KKCBUQHMOMHUOY-UHFFFAOYSA-N 0.000 description 1
- 229910001948 sodium oxide Inorganic materials 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C4/00—Compositions for glass with special properties
- C03C4/04—Compositions for glass with special properties for photosensitive glass
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C23/00—Other surface treatment of glass not in the form of fibres or filaments
- C03C23/008—Other surface treatment of glass not in the form of fibres or filaments comprising a lixiviation step
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C15/00—Surface treatment of glass, not in the form of fibres or filaments, by etching
- C03C15/02—Surface treatment of glass, not in the form of fibres or filaments, by etching for making a smooth surface
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Surface Treatment Of Glass (AREA)
- Glass Compositions (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE4217057A DE4217057A1 (de) | 1992-05-22 | 1992-05-22 | Verfahren zur Verminderung der Blei- und/oder Bariumemission von Blei und/oder Barium enthaltenden Kristallglasgegenständen bei Berührung mit einer flüssigen Phase |
| DEP4217057.5 | 1992-05-22 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1078960A CN1078960A (zh) | 1993-12-01 |
| CN1034413C true CN1034413C (zh) | 1997-04-02 |
Family
ID=6459548
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN93106111A Expired - Fee Related CN1034413C (zh) | 1992-05-22 | 1993-05-22 | 使含铅和/或钡的水晶玻璃制品在与液相接触时减少铅和/或钡释放的方法 |
Country Status (10)
| Country | Link |
|---|---|
| US (1) | US5372633A (en, 2012) |
| EP (1) | EP0575740B1 (en, 2012) |
| JP (1) | JP3262637B2 (en, 2012) |
| KR (1) | KR100253613B1 (en, 2012) |
| CN (1) | CN1034413C (en, 2012) |
| CZ (1) | CZ283877B6 (en, 2012) |
| DE (2) | DE4217057A1 (en, 2012) |
| PL (1) | PL174191B1 (en, 2012) |
| SK (1) | SK279093B6 (en, 2012) |
| TW (1) | TW222613B (en, 2012) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105585255B (zh) * | 2016-03-07 | 2017-12-19 | 秦皇岛玻璃工业研究设计院 | 一种防止含铅玻璃铅离子溶出的钝化设备和钝化方法 |
| FR3101076B1 (fr) * | 2019-09-20 | 2022-01-14 | Commissariat Energie Atomique | Procédé de traitement d’un verre comprenant du plomb permettant de limiter la migration en solution du plomb contenu dans ce verre |
Family Cites Families (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1185780B (de) * | 1962-11-10 | 1965-01-21 | Erich Saelzle Dipl Chem Dr | Verfahren zum Polieren von Gegenstaenden aus Kristall- oder Bleikristallglas |
| DE1496666C3 (de) * | 1965-05-26 | 1974-04-04 | Erich Dipl.-Chem.Dr. 8000 Muenchen Saelzle | Verfahren zum Polieren von Glasgegenständen in einem Flußsäure und Schwefelsäure enthaltenden Polierbad |
| FR1497041A (fr) * | 1965-10-20 | 1967-10-06 | Monsanto Co | Perfectionnements aux procédés pour améliorer la résistance au choc de verres de sécurité stratifiés, et aux articles ainsi obtenus |
| US3389047A (en) * | 1965-10-20 | 1968-06-18 | Monsanto Co | Treatment of coverplates for glass laminates |
| DE2949383C2 (de) * | 1979-12-07 | 1982-01-21 | Sälzle, Erich, Dr., 8000 München | Verfahren zur Schwefelsäure-Flußsäure-Polieren von Glasgegenständen |
| ES525932A0 (es) * | 1982-10-13 | 1984-11-16 | Saelzle Erich | Metodo de pulir articulos de vidrio |
| FR2627768B1 (fr) * | 1988-02-29 | 1990-06-29 | Baccarat Cristalleries | Recipient en cristal traite pour empecher la migration du plomb vers son contenu |
| DK0458713T3 (da) * | 1990-05-23 | 1994-11-07 | Baccarat Cristalleries | Fremgangsmåde til minimering af blymigrering fra en krystalflaske til en væske, som rummes i flasken, samt en genstand behandlet ifølge fremgangsmåden |
| US5232753A (en) * | 1990-05-23 | 1993-08-03 | Compagnie Des Cristalleries De Baccarat | Crystal flask treated with an alumino-silicate slip and heat |
-
1992
- 1992-05-22 DE DE4217057A patent/DE4217057A1/de not_active Withdrawn
-
1993
- 1993-05-12 JP JP13383893A patent/JP3262637B2/ja not_active Expired - Fee Related
- 1993-05-12 SK SK460-93A patent/SK279093B6/sk unknown
- 1993-05-13 DE DE59300939T patent/DE59300939D1/de not_active Expired - Fee Related
- 1993-05-13 EP EP93107806A patent/EP0575740B1/de not_active Expired - Lifetime
- 1993-05-14 PL PL93298962A patent/PL174191B1/pl unknown
- 1993-05-14 TW TW082103782A patent/TW222613B/zh active
- 1993-05-18 CZ CZ93932A patent/CZ283877B6/cs not_active IP Right Cessation
- 1993-05-21 US US08/065,265 patent/US5372633A/en not_active Expired - Fee Related
- 1993-05-21 KR KR1019930008726A patent/KR100253613B1/ko not_active Expired - Fee Related
- 1993-05-22 CN CN93106111A patent/CN1034413C/zh not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| TW222613B (en, 2012) | 1994-04-21 |
| EP0575740B1 (de) | 1995-11-15 |
| EP0575740A1 (de) | 1993-12-29 |
| DE4217057A1 (de) | 1993-11-25 |
| PL298962A1 (en) | 1993-11-29 |
| CZ93293A3 (en) | 1994-11-16 |
| JP3262637B2 (ja) | 2002-03-04 |
| PL174191B1 (pl) | 1998-06-30 |
| CN1078960A (zh) | 1993-12-01 |
| KR930023292A (ko) | 1993-12-18 |
| KR100253613B1 (ko) | 2000-04-15 |
| US5372633A (en) | 1994-12-13 |
| CZ283877B6 (cs) | 1998-06-17 |
| SK46093A3 (en) | 1993-12-08 |
| SK279093B6 (sk) | 1998-06-03 |
| JPH069248A (ja) | 1994-01-18 |
| DE59300939D1 (de) | 1995-12-21 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| US9926225B2 (en) | Media and methods for etching glass | |
| US5093196A (en) | Dealkalized sheet glass | |
| US4164402A (en) | Strengthening of thin-walled, light glass containers | |
| IE832401L (en) | Polishing glass articles in an acid bath | |
| CN1034413C (zh) | 使含铅和/或钡的水晶玻璃制品在与液相接触时减少铅和/或钡释放的方法 | |
| CN1662464A (zh) | 用于在含有硫酸和氢氟酸的抛光浴中抛光玻璃制品时减少和控制形成的六氟硅酸根的方法 | |
| US4939001A (en) | Process for sealing anodized aluminum | |
| CN114656159A (zh) | 玻璃强化液及其制备方法和应用 | |
| CN119735375A (zh) | 玻璃强化方法以及强化玻璃 | |
| US5292354A (en) | Method of producing dealkalized sheet glass | |
| JPH09295833A (ja) | フロートガラス基板の平坦化方法 | |
| CN1229518C (zh) | 铝或铝合金的表面处理方法及为此使用的处理液 | |
| US4508991A (en) | Halogen cycle incandescent lamp and method for the protection of its inner surface | |
| CN111117624B (zh) | 玻璃蒙砂液及其制备方法和应用 | |
| CN1821447A (zh) | 能降低no2烟害的铝材二步化学抛光法 | |
| JPS6365620B2 (en, 2012) | ||
| US3560281A (en) | Process for regenerating an acid bath | |
| RU2840580C1 (ru) | Способ упрочнения стекла | |
| KR0142932B1 (ko) | 불소함유 폐수의 처리방법 | |
| CN115058762B (zh) | 一种电镀锡工艺用锡沉降剂及其使用方法 | |
| JPH0741335A (ja) | ガラス容器の処理方法 | |
| SU1110765A1 (ru) | Раствор дл обработки стеклоизделий | |
| CN1373241A (zh) | 一种不锈钢化学抛光方法 | |
| CN113200686A (zh) | 光学元件的高温热处理方法 | |
| JP2730261B2 (ja) | 二酸化珪素被膜の製造方法 |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| C19 | Lapse of patent right due to non-payment of the annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |