CN103422128B - 利用超声-脉冲电铸制备高反光度微棱镜反光膜工作模的方法 - Google Patents
利用超声-脉冲电铸制备高反光度微棱镜反光膜工作模的方法 Download PDFInfo
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- CN103422128B CN103422128B CN201310388231.XA CN201310388231A CN103422128B CN 103422128 B CN103422128 B CN 103422128B CN 201310388231 A CN201310388231 A CN 201310388231A CN 103422128 B CN103422128 B CN 103422128B
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- electroforming
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- 238000005323 electroforming Methods 0.000 title claims abstract description 74
- 238000000034 method Methods 0.000 title claims abstract description 18
- 239000012528 membrane Substances 0.000 title 1
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 claims abstract description 44
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 40
- 229910052759 nickel Inorganic materials 0.000 claims abstract description 22
- DBMJMQXJHONAFJ-UHFFFAOYSA-M Sodium laurylsulphate Chemical compound [Na+].CCCCCCCCCCCCOS([O-])(=O)=O DBMJMQXJHONAFJ-UHFFFAOYSA-M 0.000 claims abstract description 17
- 235000019333 sodium laurylsulphate Nutrition 0.000 claims abstract description 17
- 229910021586 Nickel(II) chloride Inorganic materials 0.000 claims abstract description 16
- KGBXLFKZBHKPEV-UHFFFAOYSA-N boric acid Chemical compound OB(O)O KGBXLFKZBHKPEV-UHFFFAOYSA-N 0.000 claims abstract description 16
- 239000004327 boric acid Substances 0.000 claims abstract description 16
- QMMRZOWCJAIUJA-UHFFFAOYSA-L nickel dichloride Chemical compound Cl[Ni]Cl QMMRZOWCJAIUJA-UHFFFAOYSA-L 0.000 claims abstract description 16
- CVHZOJJKTDOEJC-UHFFFAOYSA-N saccharin Chemical compound C1=CC=C2C(=O)NS(=O)(=O)C2=C1 CVHZOJJKTDOEJC-UHFFFAOYSA-N 0.000 claims abstract description 16
- 229940081974 saccharin Drugs 0.000 claims abstract description 16
- 235000019204 saccharin Nutrition 0.000 claims abstract description 16
- 239000000901 saccharin and its Na,K and Ca salt Substances 0.000 claims abstract description 16
- 238000002310 reflectometry Methods 0.000 claims abstract description 15
- DLDJFQGPPSQZKI-UHFFFAOYSA-N but-2-yne-1,4-diol Chemical compound OCC#CCO DLDJFQGPPSQZKI-UHFFFAOYSA-N 0.000 claims abstract description 8
- RRIWRJBSCGCBID-UHFFFAOYSA-L nickel sulfate hexahydrate Chemical compound O.O.O.O.O.O.[Ni+2].[O-]S([O-])(=O)=O RRIWRJBSCGCBID-UHFFFAOYSA-L 0.000 claims abstract description 7
- 229940116202 nickel sulfate hexahydrate Drugs 0.000 claims abstract description 7
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims description 10
- 238000009835 boiling Methods 0.000 claims description 6
- 229910052938 sodium sulfate Inorganic materials 0.000 claims description 2
- 235000011152 sodium sulphate Nutrition 0.000 claims description 2
- SNRUBQQJIBEYMU-UHFFFAOYSA-N Dodecane Natural products CCCCCCCCCCCC SNRUBQQJIBEYMU-UHFFFAOYSA-N 0.000 claims 1
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 claims 1
- 125000003438 dodecyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 claims 1
- 239000007788 liquid Substances 0.000 claims 1
- 238000002360 preparation method Methods 0.000 abstract description 4
- 239000008367 deionised water Substances 0.000 description 28
- 229910021641 deionized water Inorganic materials 0.000 description 28
- LGQLOGILCSXPEA-UHFFFAOYSA-L nickel sulfate Chemical compound [Ni+2].[O-]S([O-])(=O)=O LGQLOGILCSXPEA-UHFFFAOYSA-L 0.000 description 12
- 229940053662 nickel sulfate Drugs 0.000 description 12
- 229910000363 nickel(II) sulfate Inorganic materials 0.000 description 12
- 238000003756 stirring Methods 0.000 description 10
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 9
- 238000005266 casting Methods 0.000 description 8
- KMUONIBRACKNSN-UHFFFAOYSA-N potassium dichromate Chemical compound [K+].[K+].[O-][Cr](=O)(=O)O[Cr]([O-])(=O)=O KMUONIBRACKNSN-UHFFFAOYSA-N 0.000 description 6
- 238000011160 research Methods 0.000 description 5
- 238000010907 mechanical stirring Methods 0.000 description 4
- 238000002161 passivation Methods 0.000 description 4
- TXUICONDJPYNPY-UHFFFAOYSA-N (1,10,13-trimethyl-3-oxo-4,5,6,7,8,9,11,12,14,15,16,17-dodecahydrocyclopenta[a]phenanthren-17-yl) heptanoate Chemical compound C1CC2CC(=O)C=C(C)C2(C)C2C1C1CCC(OC(=O)CCCCCC)C1(C)CC2 TXUICONDJPYNPY-UHFFFAOYSA-N 0.000 description 3
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 description 3
- 229910021626 Tin(II) chloride Inorganic materials 0.000 description 3
- 229910017604 nitric acid Inorganic materials 0.000 description 3
- 230000003287 optical effect Effects 0.000 description 3
- 239000001119 stannous chloride Substances 0.000 description 3
- 235000011150 stannous chloride Nutrition 0.000 description 3
- 239000002131 composite material Substances 0.000 description 2
- 238000009713 electroplating Methods 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 238000001000 micrograph Methods 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- -1 alkyl sodium sulfate Chemical compound 0.000 description 1
- 238000003491 array Methods 0.000 description 1
- 235000010338 boric acid Nutrition 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000009472 formulation Methods 0.000 description 1
- 238000007654 immersion Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000011089 mechanical engineering Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 238000000465 moulding Methods 0.000 description 1
- 238000007747 plating Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 230000036326 tumor accumulation Effects 0.000 description 1
- 238000004506 ultrasonic cleaning Methods 0.000 description 1
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- Cleaning By Liquid Or Steam (AREA)
- Electroplating And Plating Baths Therefor (AREA)
Abstract
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CN201310388231.XA CN103422128B (zh) | 2013-08-30 | 2013-08-30 | 利用超声-脉冲电铸制备高反光度微棱镜反光膜工作模的方法 |
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Families Citing this family (5)
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CN103882483B (zh) * | 2014-04-11 | 2016-06-15 | 集美大学 | 高反光度微棱镜工作模制备装置及其制备方法 |
CN104032335A (zh) * | 2014-06-26 | 2014-09-10 | 集美大学 | 后续可连续加工的微棱镜工作模制备方法 |
CN105586611A (zh) * | 2014-10-24 | 2016-05-18 | 中丰田光电科技(珠海)有限公司 | 特殊圆型镍板的制备方法 |
CN111304701B (zh) * | 2020-04-01 | 2021-02-26 | 集美大学 | 一种利用氧化石墨烯辅助超精密电铸脱模的制备方法 |
CN111394759B (zh) * | 2020-04-01 | 2021-04-06 | 集美大学 | 一种利用超声和双向脉冲电流增加电镀铜硬度的制备方法 |
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JP4971061B2 (ja) * | 2007-07-23 | 2012-07-11 | 東洋鋼鈑株式会社 | 光反射板及びその製造方法及び光反射装置 |
CN101571606B (zh) * | 2009-06-01 | 2011-05-04 | 浙江工业大学 | 一种大尺寸微棱镜型反光材料模具及制备方法 |
CN102662207B (zh) * | 2012-04-28 | 2014-04-02 | 浙江道明光学股份有限公司 | 带微棱镜阵列结构的反光材料模具的制作方法 |
CN103009016A (zh) * | 2013-01-14 | 2013-04-03 | 常州华日升反光材料股份有限公司 | 具有微棱镜阵列的无缝镍薄板的生产方法 |
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Effective date of registration: 20160607 Address after: 362241 Fujian city of Quanzhou province Jinjiang city Longhu Kam Po Development Zone Patentee after: YEAGOOD Inc. Address before: Yinjiang road in Jimei District of Xiamen City, Fujian Province, No. 185 361021 Patentee before: Jimei University |
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Effective date of registration: 20230419 Address after: No. 6, Pujin Village Nursery Industrial Zone, Longhu Town, Jinjiang City, Quanzhou City, Fujian Province, 362241 Patentee after: Fujian Yueliang New Materials Co.,Ltd. Address before: 362241 Longhu Pujin Development Zone, Jinjiang City, Quanzhou City, Fujian Province Patentee before: YEAGOOD Inc. |