CN103374158A - Anticorrosion cable sheath material and preparation method thereof - Google Patents
Anticorrosion cable sheath material and preparation method thereof Download PDFInfo
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- CN103374158A CN103374158A CN2013102499359A CN201310249935A CN103374158A CN 103374158 A CN103374158 A CN 103374158A CN 2013102499359 A CN2013102499359 A CN 2013102499359A CN 201310249935 A CN201310249935 A CN 201310249935A CN 103374158 A CN103374158 A CN 103374158A
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- 239000000463 material Substances 0.000 title claims abstract description 20
- 238000002360 preparation method Methods 0.000 title claims description 8
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 19
- 238000005260 corrosion Methods 0.000 claims abstract description 15
- 230000007797 corrosion Effects 0.000 claims abstract description 15
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 claims abstract description 14
- 235000019832 sodium triphosphate Nutrition 0.000 claims abstract description 13
- 229920001084 poly(chloroprene) Polymers 0.000 claims abstract description 9
- 239000002253 acid Substances 0.000 claims abstract description 8
- 239000002245 particle Substances 0.000 claims abstract description 8
- -1 polyethylene Polymers 0.000 claims abstract description 8
- 239000000843 powder Substances 0.000 claims abstract description 8
- 239000002994 raw material Substances 0.000 claims abstract description 8
- QYEXBYZXHDUPRC-UHFFFAOYSA-N B#[Ti]#B Chemical compound B#[Ti]#B QYEXBYZXHDUPRC-UHFFFAOYSA-N 0.000 claims abstract description 7
- 239000004952 Polyamide Substances 0.000 claims abstract description 7
- 239000004698 Polyethylene Substances 0.000 claims abstract description 7
- 229910033181 TiB2 Inorganic materials 0.000 claims abstract description 7
- BGYHLZZASRKEJE-UHFFFAOYSA-N [3-[3-(3,5-ditert-butyl-4-hydroxyphenyl)propanoyloxy]-2,2-bis[3-(3,5-ditert-butyl-4-hydroxyphenyl)propanoyloxymethyl]propyl] 3-(3,5-ditert-butyl-4-hydroxyphenyl)propanoate Chemical compound CC(C)(C)C1=C(O)C(C(C)(C)C)=CC(CCC(=O)OCC(COC(=O)CCC=2C=C(C(O)=C(C=2)C(C)(C)C)C(C)(C)C)(COC(=O)CCC=2C=C(C(O)=C(C=2)C(C)(C)C)C(C)(C)C)COC(=O)CCC=2C=C(C(O)=C(C=2)C(C)(C)C)C(C)(C)C)=C1 BGYHLZZASRKEJE-UHFFFAOYSA-N 0.000 claims abstract description 7
- 229910000019 calcium carbonate Inorganic materials 0.000 claims abstract description 7
- TVWTZAGVNBPXHU-FOCLMDBBSA-N dioctyl (e)-but-2-enedioate Chemical compound CCCCCCCCOC(=O)\C=C\C(=O)OCCCCCCCC TVWTZAGVNBPXHU-FOCLMDBBSA-N 0.000 claims abstract description 7
- FWDBOZPQNFPOLF-UHFFFAOYSA-N ethenyl(triethoxy)silane Chemical compound CCO[Si](OCC)(OCC)C=C FWDBOZPQNFPOLF-UHFFFAOYSA-N 0.000 claims abstract description 7
- 229920002647 polyamide Polymers 0.000 claims abstract description 7
- 229920000573 polyethylene Polymers 0.000 claims abstract description 7
- 239000011734 sodium Substances 0.000 claims abstract description 7
- 229910052708 sodium Inorganic materials 0.000 claims abstract description 7
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 4
- KUAZQDVKQLNFPE-UHFFFAOYSA-N thiram Chemical compound CN(C)C(=S)SSC(=S)N(C)C KUAZQDVKQLNFPE-UHFFFAOYSA-N 0.000 claims abstract description 4
- 238000002156 mixing Methods 0.000 claims description 9
- 239000000377 silicon dioxide Substances 0.000 claims description 9
- CMGDVUCDZOBDNL-UHFFFAOYSA-N 4-methyl-2h-benzotriazole Chemical compound CC1=CC=CC2=NNN=C12 CMGDVUCDZOBDNL-UHFFFAOYSA-N 0.000 claims description 6
- OGSPWJRAVKPPFI-UHFFFAOYSA-N Alendronic Acid Chemical compound NCCCC(O)(P(O)(O)=O)P(O)(O)=O OGSPWJRAVKPPFI-UHFFFAOYSA-N 0.000 claims description 6
- 101710194948 Protein phosphatase PhpP Proteins 0.000 claims description 6
- 229940062527 alendronate Drugs 0.000 claims description 6
- 229940037003 alum Drugs 0.000 claims description 6
- 235000013312 flour Nutrition 0.000 claims description 6
- 239000000203 mixture Substances 0.000 claims description 6
- YWFWDNVOPHGWMX-UHFFFAOYSA-N n,n-dimethyldodecan-1-amine Chemical compound CCCCCCCCCCCCN(C)C YWFWDNVOPHGWMX-UHFFFAOYSA-N 0.000 claims description 6
- HWGNBUXHKFFFIH-UHFFFAOYSA-I pentasodium;[oxido(phosphonatooxy)phosphoryl] phosphate Chemical compound [Na+].[Na+].[Na+].[Na+].[Na+].[O-]P([O-])(=O)OP([O-])(=O)OP([O-])([O-])=O HWGNBUXHKFFFIH-UHFFFAOYSA-I 0.000 claims description 6
- 229920000728 polyester Polymers 0.000 claims description 6
- ULWHHBHJGPPBCO-UHFFFAOYSA-N propane-1,1-diol Chemical compound CCC(O)O ULWHHBHJGPPBCO-UHFFFAOYSA-N 0.000 claims description 6
- 239000004575 stone Substances 0.000 claims description 6
- UNXRWKVEANCORM-UHFFFAOYSA-I triphosphate(5-) Chemical compound [O-]P([O-])(=O)OP([O-])(=O)OP([O-])([O-])=O UNXRWKVEANCORM-UHFFFAOYSA-I 0.000 claims description 6
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 3
- 238000000498 ball milling Methods 0.000 claims description 3
- 238000001816 cooling Methods 0.000 claims description 3
- 229960000935 dehydrated alcohol Drugs 0.000 claims description 3
- AFZSMODLJJCVPP-UHFFFAOYSA-N dibenzothiazol-2-yl disulfide Chemical compound C1=CC=C2SC(SSC=3SC4=CC=CC=C4N=3)=NC2=C1 AFZSMODLJJCVPP-UHFFFAOYSA-N 0.000 claims description 3
- 238000007599 discharging Methods 0.000 claims description 3
- 238000001035 drying Methods 0.000 claims description 3
- 230000000630 rising effect Effects 0.000 claims description 3
- 238000003756 stirring Methods 0.000 claims description 3
- 238000004073 vulcanization Methods 0.000 claims description 3
- 230000032683 aging Effects 0.000 abstract description 4
- CBENFWSGALASAD-UHFFFAOYSA-N Ozone Chemical compound [O-][O+]=O CBENFWSGALASAD-UHFFFAOYSA-N 0.000 abstract description 2
- LBOQZDCAYYCJBU-UHFFFAOYSA-N 4-methyl-2h-benzotriazole;5-methyl-2h-benzotriazole Chemical compound C1=C(C)C=CC2=NNN=C21.CC1=CC=CC2=NNN=C12 LBOQZDCAYYCJBU-UHFFFAOYSA-N 0.000 abstract 1
- NZPINPSAMMIMHP-UHFFFAOYSA-N CC(O)CO.OC(=O)CCCCC(O)=O.OC(=O)CCCCC(O)=O Chemical compound CC(O)CO.OC(=O)CCCCC(O)=O.OC(=O)CCCCC(O)=O NZPINPSAMMIMHP-UHFFFAOYSA-N 0.000 abstract 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 abstract 1
- ABLZXFCXXLZCGV-UHFFFAOYSA-N Phosphorous acid Chemical compound OP(O)=O ABLZXFCXXLZCGV-UHFFFAOYSA-N 0.000 abstract 1
- 150000004985 diamines Chemical class 0.000 abstract 1
- 229910021485 fumed silica Inorganic materials 0.000 abstract 1
- 229910052900 illite Inorganic materials 0.000 abstract 1
- VGIBGUSAECPPNB-UHFFFAOYSA-L nonaaluminum;magnesium;tripotassium;1,3-dioxido-2,4,5-trioxa-1,3-disilabicyclo[1.1.1]pentane;iron(2+);oxygen(2-);fluoride;hydroxide Chemical compound [OH-].[O-2].[O-2].[O-2].[O-2].[O-2].[F-].[Mg+2].[Al+3].[Al+3].[Al+3].[Al+3].[Al+3].[Al+3].[Al+3].[Al+3].[Al+3].[K+].[K+].[K+].[Fe+2].O1[Si]2([O-])O[Si]1([O-])O2.O1[Si]2([O-])O[Si]1([O-])O2.O1[Si]2([O-])O[Si]1([O-])O2.O1[Si]2([O-])O[Si]1([O-])O2.O1[Si]2([O-])O[Si]1([O-])O2.O1[Si]2([O-])O[Si]1([O-])O2.O1[Si]2([O-])O[Si]1([O-])O2 VGIBGUSAECPPNB-UHFFFAOYSA-L 0.000 abstract 1
- 238000002485 combustion reaction Methods 0.000 description 2
- 239000003921 oil Substances 0.000 description 2
- 244000043261 Hevea brasiliensis Species 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 238000005336 cracking Methods 0.000 description 1
- 230000018109 developmental process Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000003063 flame retardant Substances 0.000 description 1
- 239000010721 machine oil Substances 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 229920003052 natural elastomer Polymers 0.000 description 1
- 229920001194 natural rubber Polymers 0.000 description 1
- 238000011056 performance test Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 229920003051 synthetic elastomer Polymers 0.000 description 1
- 239000005061 synthetic rubber Substances 0.000 description 1
- 239000002446 δ-tocopherol Substances 0.000 description 1
Landscapes
- Compositions Of Macromolecular Compounds (AREA)
- Insulated Conductors (AREA)
- Organic Insulating Materials (AREA)
Abstract
The invention discloses an anticorrosion cable sheath material which is characterized by consisting of the following raw materials in parts by weight: 90 to 105 parts of neoprene A90, 15 to 20 parts of polyethylene, 10 to 12 parts of fumed silica, 16 to 20 parts of illite powder, 15 to 25 parts of light calcium carbonate, 6 to 8 parts of polyamide wax micro powder, 3 to 4 parts of dioctyl maleate, 1 to 2 parts of extylene diamine tetra (mextylene phosphonic acid) sodium, 1 to 2 parts of di-methyl-dodecyl amine, 1 to 2 parts of methyl-1H-benzotriazole, 4 to 6 parts of titanium diboride, 2 to 3 parts of alumpowder, 1 to 2 parts of adipic acid-propylene glycol adipate, 1 to 2 parts of ethenyltriethyloxy-silane, 1 to 2 parts of an antioxidant 1010, 1 to 2 parts of a promoter DM, 0.8 to 1 part of a promoter TMTD, 0.6 to 1 part of a sulfurizing agent, 0.2 to 0.4 part of sodium tripolyphosphate and 0.2 to 0.3 part of alkanolamide. The cable sheath material has a good physical mechanical property, excellent oil resistance, heat resistance, fire resistance, sunshine resistance, ozone resistance, aging resistance, acid resistance and alkaline resistance. By adding particles produced by the material, the compatibility amoing raw materials can be enhanced, and the tearing strength, the resilience and the corrosion resistance can be further enhanced.
Description
Technical field
The present invention relates generally to a kind of sheath material, relates in particular to a kind of corrosion cable sheath material and preparation method thereof.
Background technology
The over-all properties of chloroprene rubber is good, natural rubber and other synthetic rubber are all incomparable on a lot of performances, good physical and mechanical properties is arranged, oil resistant, heat-resisting, anti-combustion, anti-daylight, anti-ozone, ageing-resistant, acid and alkali-resistance, chemical-resistant reagent, therefore be used as widely cable jacket material, and CABLE MATERIALS is higher for the requirement of performance, to accept for a long time to be exposed to the sun, wind and rain, high temperature, low cold etc., corrosion-resistant for it, the performance requriements of the each side such as fire-retardant is all higher, therefore need a kind of new method to improve and strengthen the overall performance of chloroprene rubber, necessary for the development of cable cause.
Summary of the invention
The object of the invention just provides a kind of corrosion cable sheath material and preparation method thereof.
The present invention is achieved by the following technical solutions:
A kind of corrosion cable sheath material, it is comprised of the raw material of following weight parts
Chloroprene rubber A90 90-105, polyethylene 15-20, gas-phase silica 10-12, the stone flour 16-20 of Erie, light calcium carbonate 15-25, polyamide wax micropowder 6-8, dioctyl maleate 3-4, ethylenediamine tetramethylene fork Alendronate 1-2, Dodecyl Dimethyl Amine 1-2, tolyltriazole 1-2, TiB2 4-6, alum powder 2-3, hexanodioic acid propanediol polyester 1-2, vinyltriethoxysilane 1-2, antioxidant 1010 1-2, altax 1-2, Vulcanization accelerator TMTD 0.8-1, vulcanizing agent DCBP0.6-1, tripoly phosphate sodium STPP 0.2-0.4, alkylolamide 0.2-0.3.
A kind of preparation method of corrosion cable sheath material may further comprise the steps:
Above-mentioned Dodecyl Dimethyl Amine is mixed with TiB2, stirring and dissolving, add gas-phase silica, vinyltriethoxysilane, stirred 1-2 hour at 50-60 ℃ of lower constant temperature, will add behind above-mentioned tolyltriazole and the 2-3 dehydrated alcohol mix and blend doubly, add again alum powder, tripoly phosphate sodium STPP, the rising temperature is to 90-100 ℃, and low speed 300-500 rev/min was disperseed the ball milling post-drying 30-40 minute, sieve, get the particle of 2-3 μ m; Above-mentioned chloroprene rubber A90 and polyethylene, polyamide wax micropowder, dioctyl maleate, hexanodioic acid propanediol polyester are mixed to join in the Banbury mixer, descended mixing 2-4 minute at 82-90 ℃, add again particle obtained above and gas-phase silica, Erie's stone flour, light calcium carbonate, ethylenediamine tetramethylene fork Alendronate, antioxidant 1010, be under 85-90 ℃ in temperature, mixing 4-5 minute; Add each raw material of residue again, be 55-60 ℃ in temperature and descended mixing 2-3 minute, the discharging cooling namely gets described corrosion cable sheath material.
Advantage of the present invention is:
The cable jacket material that the present invention produces has good physical and mechanical properties, oil resistant, heat-resisting, anti-combustion, anti-daylight, anti-ozone, ageing-resistant, acid-proof alkaline is excellent, by add particle of the present invention in preparation, strengthen the consistency of each stock yard, further strengthened tearing toughness, rebound performance, corrosion resistance nature.
Embodiment
Embodiment 1
A kind of corrosion cable sheath material, it is comprised of the raw material of following weight parts (kilogram)
Chloroprene rubber A90 105, polyethylene E309 20, gas-phase silica 12, Erie's stone flour 20, light calcium carbonate 25, polyamide wax micropowder 8, dioctyl maleate 4, ethylenediamine tetramethylene fork Alendronate 2, Dodecyl Dimethyl Amine 1, tolyltriazole 2, TiB2 6, alum powder 3, hexanodioic acid propanediol polyester 2, vinyltriethoxysilane 2, antioxidant 1010 2, altax 2, Vulcanization accelerator TMTD 0.8, vulcanizing agent DCBP0.6, tripoly phosphate sodium STPP 0.4, alkylolamide 0.3.
A kind of preparation method of corrosion cable sheath material may further comprise the steps:
Above-mentioned Dodecyl Dimethyl Amine is mixed with TiB2, stirring and dissolving, add gas-phase silica, vinyltriethoxysilane, stirred 2 hours at 60 ℃ of lower constant temperature, add behind the dehydrated alcohol mix and blend with above-mentioned tolyltriazole and 3 times, add again alum powder, tripoly phosphate sodium STPP, rising temperature to 100 ℃, 500 rev/mins of low speed disperseed the ball milling post-drying 40 minutes, sieve, get the particle of 3 μ m; Above-mentioned chloroprene rubber A90 and polyethylene, polyamide wax micropowder, dioctyl maleate, hexanodioic acid propanediol polyester are mixed to join in the Banbury mixer, descended mixing 4 minutes at 90 ℃, add again particle obtained above and gas-phase silica, Erie's stone flour, light calcium carbonate, ethylenediamine tetramethylene fork Alendronate, antioxidant 1010, be under 90 ℃ in temperature, mixing 5 minutes; Add each raw material of residue again, be 60 ℃ in temperature and descended mixing 3 minutes, the discharging cooling namely gets described corrosion cable sheath material.
Performance test:
Tensile strength: 18.3MPa;
Elongation at break: 712%;
Oil-proofness: 100 ℃ * 75h of 20# machine oil, elongation at break conservation rate 73.1%, tensile strength conservation rate 78.2%;
Anti-ozone: 25 ℃, 30h, ozone concn 0.024%, without cracking;
Ageing-resistant: 120 ℃, 200h, tensile strength conservation rate 90.8%, elongation at break conservation rate 80.1%.
Claims (2)
1. corrosion cable sheath material is characterized in that what it was comprised of the raw material of following weight parts:
Chloroprene rubber A90 90-105, polyethylene 15-20, gas-phase silica 10-12, the stone flour 16-20 of Erie, light calcium carbonate 15-25, polyamide wax micropowder 6-8, dioctyl maleate 3-4, ethylenediamine tetramethylene fork Alendronate 1-2, Dodecyl Dimethyl Amine 1-2, tolyltriazole 1-2, TiB2 4-6, alum powder 2-3, hexanodioic acid propanediol polyester 1-2, vinyltriethoxysilane 1-2, antioxidant 1010 1-2, altax 1-2, Vulcanization accelerator TMTD 0.8-1, vulcanizing agent DCBP0.6-1, tripoly phosphate sodium STPP 0.2-0.4, alkylolamide 0.2-0.3.
2. the preparation method of a corrosion cable sheath material as claimed in claim 1 is characterized in that may further comprise the steps:
Above-mentioned Dodecyl Dimethyl Amine is mixed with TiB2, stirring and dissolving, add gas-phase silica, vinyltriethoxysilane, stirred 1-2 hour at 50-60 ℃ of lower constant temperature, will add behind above-mentioned tolyltriazole and the 2-3 dehydrated alcohol mix and blend doubly, add again alum powder, tripoly phosphate sodium STPP, the rising temperature is to 90-100 ℃, and low speed 300-500 rev/min was disperseed the ball milling post-drying 30-40 minute, sieve, get the particle of 2-3 μ m; Above-mentioned chloroprene rubber A90 and polyethylene, polyamide wax micropowder, dioctyl maleate, hexanodioic acid propanediol polyester are mixed to join in the Banbury mixer, descended mixing 2-4 minute at 82-90 ℃, add again particle obtained above and gas-phase silica, Erie's stone flour, light calcium carbonate, ethylenediamine tetramethylene fork Alendronate, antioxidant 1010, be under 85-90 ℃ in temperature, mixing 4-5 minute; Add each raw material of residue again, be 55-60 ℃ in temperature and descended mixing 2-3 minute, the discharging cooling namely gets described corrosion cable sheath material.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310249935.9A CN103374158B (en) | 2013-06-21 | 2013-06-21 | A kind of Anticorrosion cable sheath material and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310249935.9A CN103374158B (en) | 2013-06-21 | 2013-06-21 | A kind of Anticorrosion cable sheath material and preparation method thereof |
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| Publication Number | Publication Date |
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| CN103374158A true CN103374158A (en) | 2013-10-30 |
| CN103374158B CN103374158B (en) | 2016-01-27 |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105647037A (en) * | 2016-03-01 | 2016-06-08 | 苏州科茂电子材料科技有限公司 | Cable sheath material resistant to acid and base corrosion and preparation method of cable sheath material |
| CN106432804A (en) * | 2016-11-08 | 2017-02-22 | 承德人和矿业有限责任公司 | Illite powder reinforcer, preparation method thereof and rubber containing reinforcer |
| CN107841013A (en) * | 2017-11-03 | 2018-03-27 | 万帅 | A kind of computer flame-proof weather-resisting stretch-proof cable and preparation method thereof |
| CN108864708A (en) * | 2018-07-18 | 2018-11-23 | 曹佳男 | Anticorrosive cable material of a kind of acid and alkali-resistance and preparation method thereof |
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| CN101089039A (en) * | 2006-06-12 | 2007-12-19 | 深圳市迅特科技有限公司 | Chlorinated polyethylene-neoprene mixed polymer |
| CN101544790A (en) * | 2009-04-17 | 2009-09-30 | 安徽纵横高科电缆股份有限公司 | 125 DEG C resistance low smoke non-halogen rubber-sheathed cable shielding material |
| CN102746549A (en) * | 2012-06-07 | 2012-10-24 | 安徽胜华电缆集团有限公司 | Polyethylene insulation power cable material for coal and method for preparing the same |
| CN102993521A (en) * | 2012-11-13 | 2013-03-27 | 安徽文峰电子科技集团有限公司 | Environmental-friendly termite-resistant cable sheath insulating material and method for preparing same |
| CN103102545A (en) * | 2012-11-14 | 2013-05-15 | 安徽金桥电缆有限公司 | Cable sheath insulating material for computer and preparation method thereof |
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Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN101089039A (en) * | 2006-06-12 | 2007-12-19 | 深圳市迅特科技有限公司 | Chlorinated polyethylene-neoprene mixed polymer |
| CN101544790A (en) * | 2009-04-17 | 2009-09-30 | 安徽纵横高科电缆股份有限公司 | 125 DEG C resistance low smoke non-halogen rubber-sheathed cable shielding material |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105647037A (en) * | 2016-03-01 | 2016-06-08 | 苏州科茂电子材料科技有限公司 | Cable sheath material resistant to acid and base corrosion and preparation method of cable sheath material |
| CN106432804A (en) * | 2016-11-08 | 2017-02-22 | 承德人和矿业有限责任公司 | Illite powder reinforcer, preparation method thereof and rubber containing reinforcer |
| CN107841013A (en) * | 2017-11-03 | 2018-03-27 | 万帅 | A kind of computer flame-proof weather-resisting stretch-proof cable and preparation method thereof |
| CN108864708A (en) * | 2018-07-18 | 2018-11-23 | 曹佳男 | Anticorrosive cable material of a kind of acid and alkali-resistance and preparation method thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN103374158B (en) | 2016-01-27 |
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