CN103374158B - A kind of Anticorrosion cable sheath material and preparation method thereof - Google Patents
A kind of Anticorrosion cable sheath material and preparation method thereof Download PDFInfo
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- CN103374158B CN103374158B CN201310249935.9A CN201310249935A CN103374158B CN 103374158 B CN103374158 B CN 103374158B CN 201310249935 A CN201310249935 A CN 201310249935A CN 103374158 B CN103374158 B CN 103374158B
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- 239000000463 material Substances 0.000 title claims abstract description 19
- 238000002360 preparation method Methods 0.000 title claims abstract description 9
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 20
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 claims abstract description 14
- 235000019832 sodium triphosphate Nutrition 0.000 claims abstract description 14
- 239000000377 silicon dioxide Substances 0.000 claims abstract description 10
- 229920001084 poly(chloroprene) Polymers 0.000 claims abstract description 9
- 239000002994 raw material Substances 0.000 claims abstract description 9
- 239000002253 acid Substances 0.000 claims abstract description 8
- 239000002245 particle Substances 0.000 claims abstract description 8
- CMGDVUCDZOBDNL-UHFFFAOYSA-N 4-methyl-2h-benzotriazole Chemical compound CC1=CC=CC2=NNN=C12 CMGDVUCDZOBDNL-UHFFFAOYSA-N 0.000 claims abstract description 7
- OGSPWJRAVKPPFI-UHFFFAOYSA-N Alendronic Acid Chemical compound NCCCC(O)(P(O)(O)=O)P(O)(O)=O OGSPWJRAVKPPFI-UHFFFAOYSA-N 0.000 claims abstract description 7
- QYEXBYZXHDUPRC-UHFFFAOYSA-N B#[Ti]#B Chemical compound B#[Ti]#B QYEXBYZXHDUPRC-UHFFFAOYSA-N 0.000 claims abstract description 7
- 239000004952 Polyamide Substances 0.000 claims abstract description 7
- 239000004698 Polyethylene Substances 0.000 claims abstract description 7
- 101710194948 Protein phosphatase PhpP Proteins 0.000 claims abstract description 7
- 229910033181 TiB2 Inorganic materials 0.000 claims abstract description 7
- BGYHLZZASRKEJE-UHFFFAOYSA-N [3-[3-(3,5-ditert-butyl-4-hydroxyphenyl)propanoyloxy]-2,2-bis[3-(3,5-ditert-butyl-4-hydroxyphenyl)propanoyloxymethyl]propyl] 3-(3,5-ditert-butyl-4-hydroxyphenyl)propanoate Chemical compound CC(C)(C)C1=C(O)C(C(C)(C)C)=CC(CCC(=O)OCC(COC(=O)CCC=2C=C(C(O)=C(C=2)C(C)(C)C)C(C)(C)C)(COC(=O)CCC=2C=C(C(O)=C(C=2)C(C)(C)C)C(C)(C)C)COC(=O)CCC=2C=C(C(O)=C(C=2)C(C)(C)C)C(C)(C)C)=C1 BGYHLZZASRKEJE-UHFFFAOYSA-N 0.000 claims abstract description 7
- 229940062527 alendronate Drugs 0.000 claims abstract description 7
- 229940037003 alum Drugs 0.000 claims abstract description 7
- 229910000019 calcium carbonate Inorganic materials 0.000 claims abstract description 7
- TVWTZAGVNBPXHU-FOCLMDBBSA-N dioctyl (e)-but-2-enedioate Chemical compound CCCCCCCCOC(=O)\C=C\C(=O)OCCCCCCCC TVWTZAGVNBPXHU-FOCLMDBBSA-N 0.000 claims abstract description 7
- FWDBOZPQNFPOLF-UHFFFAOYSA-N ethenyl(triethoxy)silane Chemical compound CCO[Si](OCC)(OCC)C=C FWDBOZPQNFPOLF-UHFFFAOYSA-N 0.000 claims abstract description 7
- 235000013312 flour Nutrition 0.000 claims abstract description 7
- YWFWDNVOPHGWMX-UHFFFAOYSA-N n,n-dimethyldodecan-1-amine Chemical compound CCCCCCCCCCCCN(C)C YWFWDNVOPHGWMX-UHFFFAOYSA-N 0.000 claims abstract description 7
- HWGNBUXHKFFFIH-UHFFFAOYSA-I pentasodium;[oxido(phosphonatooxy)phosphoryl] phosphate Chemical compound [Na+].[Na+].[Na+].[Na+].[Na+].[O-]P([O-])(=O)OP([O-])(=O)OP([O-])([O-])=O HWGNBUXHKFFFIH-UHFFFAOYSA-I 0.000 claims abstract description 7
- 229920002647 polyamide Polymers 0.000 claims abstract description 7
- 229920000728 polyester Polymers 0.000 claims abstract description 7
- -1 polyethylene Polymers 0.000 claims abstract description 7
- 229920000573 polyethylene Polymers 0.000 claims abstract description 7
- 239000000843 powder Substances 0.000 claims abstract description 7
- ULWHHBHJGPPBCO-UHFFFAOYSA-N propane-1,1-diol Chemical compound CCC(O)O ULWHHBHJGPPBCO-UHFFFAOYSA-N 0.000 claims abstract description 7
- 239000011734 sodium Substances 0.000 claims abstract description 7
- 229910052708 sodium Inorganic materials 0.000 claims abstract description 7
- 239000004575 stone Substances 0.000 claims abstract description 7
- UNXRWKVEANCORM-UHFFFAOYSA-I triphosphate(5-) Chemical compound [O-]P([O-])(=O)OP([O-])(=O)OP([O-])([O-])=O UNXRWKVEANCORM-UHFFFAOYSA-I 0.000 claims abstract description 7
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 4
- AFZSMODLJJCVPP-UHFFFAOYSA-N dibenzothiazol-2-yl disulfide Chemical compound C1=CC=C2SC(SSC=3SC4=CC=CC=C4N=3)=NC2=C1 AFZSMODLJJCVPP-UHFFFAOYSA-N 0.000 claims abstract description 4
- KUAZQDVKQLNFPE-UHFFFAOYSA-N thiram Chemical compound CN(C)C(=S)SSC(=S)N(C)C KUAZQDVKQLNFPE-UHFFFAOYSA-N 0.000 claims abstract description 4
- 238000004073 vulcanization Methods 0.000 claims abstract description 4
- 238000002156 mixing Methods 0.000 claims description 9
- 239000000203 mixture Substances 0.000 claims description 6
- 238000003756 stirring Methods 0.000 claims description 6
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 3
- 238000000498 ball milling Methods 0.000 claims description 3
- 229960000935 dehydrated alcohol Drugs 0.000 claims description 3
- 238000007599 discharging Methods 0.000 claims description 3
- 238000001035 drying Methods 0.000 claims description 3
- 239000006185 dispersion Substances 0.000 claims description 2
- CBENFWSGALASAD-UHFFFAOYSA-N Ozone Chemical compound [O-][O+]=O CBENFWSGALASAD-UHFFFAOYSA-N 0.000 abstract description 5
- 230000032683 aging Effects 0.000 abstract description 4
- 238000002485 combustion reaction Methods 0.000 abstract description 3
- 238000005260 corrosion Methods 0.000 abstract description 3
- 230000007797 corrosion Effects 0.000 abstract description 3
- 230000002708 enhancing effect Effects 0.000 abstract description 2
- 230000014759 maintenance of location Effects 0.000 description 2
- 239000003921 oil Substances 0.000 description 2
- 244000043261 Hevea brasiliensis Species 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 238000005336 cracking Methods 0.000 description 1
- 230000018109 developmental process Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000003063 flame retardant Substances 0.000 description 1
- 239000010721 machine oil Substances 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 229920003052 natural elastomer Polymers 0.000 description 1
- 229920001194 natural rubber Polymers 0.000 description 1
- 238000011056 performance test Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 229920003051 synthetic elastomer Polymers 0.000 description 1
- 239000005061 synthetic rubber Substances 0.000 description 1
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- Compositions Of Macromolecular Compounds (AREA)
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Abstract
The invention discloses a kind of Anticorrosion cable sheath material, it is characterized in that what it was made up of the raw material of following weight parts: chloroprene rubber A90? 90-105, polyethylene 15-20, gas-phase silica 10-12, Erie stone flour 16-20, light calcium carbonate 15-25, polyamide wax micropowder 6-8, dioctyl maleate 3-4, ethylenediamine tetramethylene fork Alendronate 1-2, Dodecyl Dimethyl Amine 1-2, tolyltriazole 1-2, TiB2 4-6, alum powder 2-3, hexanodioic acid propanediol polyester 1-2, vinyltriethoxysilane 1-2, antioxidant 1010? 1-2, altax? 1-2, Vulcanization accelerator TMTD? 0.8-1, vulcanizing agent DCBP0.6-1, tripoly phosphate sodium STPP 0.2-0.4, alkylolamide 0.2-0.3.The cable jacket material that the present invention produces has good physical and mechanical properties, oil resistant, heat-resisting, resistance to combustion, resistance to daylight, resistance to ozone, ageing-resistant, acid-proof alkaline is excellent, by adding particle of the present invention in preparation, enhance the consistency between each raw material, further enhancing tearing toughness, rebound performance, corrosion resistance nature.
Description
Technical field
The present invention relates generally to a kind of sheath material, particularly relates to a kind of Anticorrosion cable sheath material and preparation method thereof.
Background technology
The over-all properties of chloroprene rubber is good, natural rubber is all incomparable in a lot of performance with other synthetic rubber, there is good physical and mechanical properties, oil resistant, heat-resisting, resistance to combustion, resistance to daylight, resistance to ozone, ageing-resistant, acid and alkali-resistance, chemical-resistant reagent, therefore cable jacket material is widely used as, and CABLE MATERIALS is higher for the requirement of performance, want to accept for a long time to be exposed to the sun, wind and rain, high temperature, low cold etc., corrosion-resistant for it, the performance requriements of each side such as fire-retardant is all higher, therefore a kind of new method is needed to improve and strengthen the overall performance of chloroprene rubber, development for cable cause is necessary.
Summary of the invention
The object of the invention is just to provide a kind of Anticorrosion cable sheath material and preparation method thereof.
The present invention is achieved by the following technical solutions:
A kind of Anticorrosion cable sheath material, it is made up of the raw material of following weight parts
Chloroprene rubber A9090-105, polyethylene 15-20, gas-phase silica 10-12, Erie stone flour 16-20, light calcium carbonate 15-25, polyamide wax micropowder 6-8, dioctyl maleate 3-4, ethylenediamine tetramethylene fork Alendronate 1-2, Dodecyl Dimethyl Amine 1-2, tolyltriazole 1-2, TiB2 4-6, alum powder 2-3, hexanodioic acid propanediol polyester 1-2, vinyltriethoxysilane 1-2, antioxidant 1010 1-2, altax 1-2, Vulcanization accelerator TMTD 0.8-1, vulcanizing agent DCBP0.6-1, tripoly phosphate sodium STPP 0.2-0.4, alkylolamide 0.2-0.3.
A preparation method for Anticorrosion cable sheath material, comprises the following steps:
Above-mentioned Dodecyl Dimethyl Amine is mixed with TiB2, stirring and dissolving, add gas-phase silica, vinyltriethoxysilane, at 50-60 DEG C, constant temperature stirs 1-2 hour, adds after above-mentioned tolyltriazole and 2-3 dehydrated alcohol mix and blend doubly, add alum powder, tripoly phosphate sodium STPP again, raised temperature is to 90-100 DEG C, and low speed 300-500 rev/min is disperseed 30-40 minute, ball milling post-drying, sieve, obtain the particle of 2-3 μm; Above-mentioned chloroprene rubber A90 and polyethylene, polyamide wax micropowder, dioctyl maleate, hexanodioic acid propanediol polyester are mixed to join in Banbury mixer, mixing 2-4 minute at 82-90 DEG C, add particle obtained above and gas-phase silica, Erie's stone flour, light calcium carbonate, ethylenediamine tetramethylene fork Alendronate, antioxidant 1010 again, at temperature is 85-90 DEG C, mixing 4-5 minute; Add each raw material of residue again, mixing 2-3 minute at temperature is 55-60 DEG C, discharging cools and obtains described Anticorrosion cable sheath material.
Advantage of the present invention is:
The cable jacket material that the present invention produces has good physical and mechanical properties, oil resistant, heat-resisting, resistance to combustion, resistance to daylight, resistance to ozone, ageing-resistant, acid-proof alkaline is excellent, by adding particle of the present invention in preparation, enhance the consistency between each raw material, further enhancing tearing toughness, rebound performance, corrosion resistance nature.
Embodiment
Embodiment 1
A kind of Anticorrosion cable sheath material, it is made up of the raw material of following weight parts (kilogram)
Chloroprene rubber A90105, polyethylene E30920, gas-phase silica 12, Erie's stone flour 20, light calcium carbonate 25, polyamide wax micropowder 8, dioctyl maleate 4, ethylenediamine tetramethylene fork Alendronate 2, Dodecyl Dimethyl Amine 1, tolyltriazole 2, TiB2 6, alum powder 3, hexanodioic acid propanediol polyester 2, vinyltriethoxysilane 2, antioxidant 1010 2, altax 2, Vulcanization accelerator TMTD 0.8, vulcanizing agent DCBP0.6, tripoly phosphate sodium STPP 0.4, alkylolamide 0.3.
A preparation method for Anticorrosion cable sheath material, comprises the following steps:
Above-mentioned Dodecyl Dimethyl Amine is mixed with TiB2, stirring and dissolving, add gas-phase silica, vinyltriethoxysilane, at 60 DEG C, constant temperature stirs 2 hours, adds after the dehydrated alcohol mix and blend of above-mentioned tolyltriazole and 3 times, add alum powder, tripoly phosphate sodium STPP again, raised temperature to 100 DEG C, low speed 500 revs/min dispersion 40 minutes, ball milling post-drying, sieve, obtain the particle of 3 μm; Above-mentioned chloroprene rubber A90 and polyethylene, polyamide wax micropowder, dioctyl maleate, hexanodioic acid propanediol polyester are mixed to join in Banbury mixer, at 90 DEG C mixing 4 minutes, add particle obtained above and gas-phase silica, Erie's stone flour, light calcium carbonate, ethylenediamine tetramethylene fork Alendronate, antioxidant 1010 again, at temperature is 90 DEG C, mixing 5 minutes; Add each raw material of residue again, at temperature is 60 DEG C mixing 3 minutes, discharging cooled and obtains described Anticorrosion cable sheath material.
Performance test:
Tensile strength: 18.3MPa;
Elongation at break: 712%;
Oil-proofness: 20# machine oil 100 DEG C × 75h, elongation at break conservation rate 73.1%, tensile strength retention 78.2%;
Resistance to ozone: 25 DEG C, 30h, ozone concn 0.024%, without cracking;
Ageing-resistant: 120 DEG C, 200h, tensile strength retention 90.8%, elongation at break conservation rate 80.1%.
Claims (2)
1. an Anticorrosion cable sheath material, it is characterized in that what it was made up of the raw material of following weight parts: chloroprene rubber A9090-105, polyethylene 15-20, gas-phase silica 10-12, Erie stone flour 16-20, light calcium carbonate 15-25, polyamide wax micropowder 6-8, dioctyl maleate 3-4, ethylenediamine tetramethylene fork Alendronate 1-2, Dodecyl Dimethyl Amine 1-2, tolyltriazole 1-2, TiB2 4-6, alum powder 2-3, hexanodioic acid propanediol polyester 1-2, vinyltriethoxysilane 1-2, antioxidant 1010 1-2, altax 1-2, Vulcanization accelerator TMTD 0.8-1, vulcanizing agent DCBP0.6-1, tripoly phosphate sodium STPP 0.2-0.4, alkylolamide 0.2-0.3.
2. the preparation method of an Anticorrosion cable sheath material as claimed in claim 1, it is characterized in that comprising the following steps: above-mentioned Dodecyl Dimethyl Amine is mixed with TiB2, stirring and dissolving, add gas-phase silica, vinyltriethoxysilane, at 50-60 DEG C, constant temperature stirs 1-2 hour, add after above-mentioned tolyltriazole and 2-3 dehydrated alcohol mix and blend doubly, add alum powder again, tripoly phosphate sodium STPP, raised temperature is to 90-100 DEG C, low speed 300-500 rev/min of dispersion 30-40 minute, ball milling post-drying, sieve, obtain the particle of 2-3 μm, above-mentioned chloroprene rubber A90 and polyethylene, polyamide wax micropowder, dioctyl maleate, hexanodioic acid propanediol polyester are mixed to join in Banbury mixer, mixing 2-4 minute at 82-90 DEG C, add particle obtained above and gas-phase silica, Erie's stone flour, light calcium carbonate, ethylenediamine tetramethylene fork Alendronate, antioxidant 1010 again, at temperature is 85-90 DEG C, mixing 4-5 minute, add each raw material of residue again, mixing 2-3 minute at temperature is 55-60 DEG C, discharging cools and obtains described Anticorrosion cable sheath material.
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| CN201310249935.9A CN103374158B (en) | 2013-06-21 | 2013-06-21 | A kind of Anticorrosion cable sheath material and preparation method thereof |
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Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN105647037A (en) * | 2016-03-01 | 2016-06-08 | 苏州科茂电子材料科技有限公司 | Cable sheath material resistant to acid and base corrosion and preparation method of cable sheath material |
| CN106432804A (en) * | 2016-11-08 | 2017-02-22 | 承德人和矿业有限责任公司 | Illite powder reinforcer, preparation method thereof and rubber containing reinforcer |
| CN107841013A (en) * | 2017-11-03 | 2018-03-27 | 万帅 | A kind of computer flame-proof weather-resisting stretch-proof cable and preparation method thereof |
| CN108864708A (en) * | 2018-07-18 | 2018-11-23 | 曹佳男 | Anticorrosive cable material of a kind of acid and alkali-resistance and preparation method thereof |
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| CN101089039A (en) * | 2006-06-12 | 2007-12-19 | 深圳市迅特科技有限公司 | Chlorinated polyethylene-neoprene mixed polymer |
| CN101544790A (en) * | 2009-04-17 | 2009-09-30 | 安徽纵横高科电缆股份有限公司 | 125 DEG C resistance low smoke non-halogen rubber-sheathed cable shielding material |
| CN102746549A (en) * | 2012-06-07 | 2012-10-24 | 安徽胜华电缆集团有限公司 | Polyethylene insulation power cable material for coal and method for preparing the same |
| CN102993521A (en) * | 2012-11-13 | 2013-03-27 | 安徽文峰电子科技集团有限公司 | Environmental-friendly termite-resistant cable sheath insulating material and method for preparing same |
| CN103102545A (en) * | 2012-11-14 | 2013-05-15 | 安徽金桥电缆有限公司 | Cable sheath insulating material for computer and preparation method thereof |
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2013
- 2013-06-21 CN CN201310249935.9A patent/CN103374158B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101089039A (en) * | 2006-06-12 | 2007-12-19 | 深圳市迅特科技有限公司 | Chlorinated polyethylene-neoprene mixed polymer |
| CN101544790A (en) * | 2009-04-17 | 2009-09-30 | 安徽纵横高科电缆股份有限公司 | 125 DEG C resistance low smoke non-halogen rubber-sheathed cable shielding material |
| CN102746549A (en) * | 2012-06-07 | 2012-10-24 | 安徽胜华电缆集团有限公司 | Polyethylene insulation power cable material for coal and method for preparing the same |
| CN102993521A (en) * | 2012-11-13 | 2013-03-27 | 安徽文峰电子科技集团有限公司 | Environmental-friendly termite-resistant cable sheath insulating material and method for preparing same |
| CN103102545A (en) * | 2012-11-14 | 2013-05-15 | 安徽金桥电缆有限公司 | Cable sheath insulating material for computer and preparation method thereof |
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