CN106543932A - Impervious container fluid sealant of a kind of heat insulation anti-shock aqueouss containing asbestos fibre and preparation method thereof - Google Patents
Impervious container fluid sealant of a kind of heat insulation anti-shock aqueouss containing asbestos fibre and preparation method thereof Download PDFInfo
- Publication number
- CN106543932A CN106543932A CN201610960774.8A CN201610960774A CN106543932A CN 106543932 A CN106543932 A CN 106543932A CN 201610960774 A CN201610960774 A CN 201610960774A CN 106543932 A CN106543932 A CN 106543932A
- Authority
- CN
- China
- Prior art keywords
- asbestos fibre
- fluid sealant
- heat insulation
- shock
- solid content
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J133/00—Adhesives based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Adhesives based on derivatives of such polymers
- C09J133/04—Homopolymers or copolymers of esters
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/02—Non-macromolecular additives
- C09J11/04—Non-macromolecular additives inorganic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/02—Non-macromolecular additives
- C09J11/06—Non-macromolecular additives organic
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
Abstract
The invention discloses a kind of impervious container fluid sealant of heat insulation anti-shock aqueouss containing asbestos fibre, which is obtained by the raw material of following weight parts：Solid content is 40 50% polyacrylate dispersion 40 60, solid content is 40 50% polychloroprene latex 5 10, and solid content is 40 60% water soluble phenol resin 35, asbestos fibre 10 15, flyash 30 40, Colophonium 35, liquid paraffin 24, titanate coupling agent 35, tributyl citrate 35, potassium sorbate 0.5 1, Lauryl Alcohol ester 0.5 1, water 10 15.The container fluid sealant of the present invention has high resiliency, high waterproof impervious characteristic and excellent sealing property concurrently, while with good heat insulation anti-shock effect, durability is high, long service life, environmental protection.
Description
Technical field
The present invention relates to fluid sealant technical field, more particularly to a kind of impervious packaging of heat insulation anti-shock aqueouss containing asbestos fibre
Case fluid sealant and preparation method thereof.
Background technology
Fluid sealant be guide deform with sealing surface shape, be difficult trickling, have the encapsulant of certain caking property, be for
Filling configuration gap, the adhesive to play sealing function, play important in multiple fields such as building, assembling, transportation
Effect.In recent years, developing rapidly with Container Transport industry, fluid sealant as Production Container during main auxiliary material
Material, its performance are also more paid attention to.Container seals conventionally used solvent-borne type butyl type rubber or neoprene
Class fluid sealant, such fluid sealant abnormal smells from the patient weight, VOC emission amount are big, may result in environmental pollution, or even produce injury to human body,
Environmental requirement cannot be met.Aqueous sealant is increasingly paid close attention to by universal as a kind of environmentally friendly product.
Polyacrylate emulsion has good weatherability and a high-adhesive-strength, environmental protection, good processability, and price is just
Preferably, it is used widely in adhesive field.CN201010199240 discloses a kind of environment-friendly container aqueous sealant,
Physical and mechanical property is good, and sealing is excellent, while having extremely low VOC content, environmental protection.However, above-mentioned fluid sealant product according to
So there is a problem of that impervious, water resistance and elasticity are relatively low, constrain its use range and service life in actual applications,
Need further perfect.
The content of the invention
The object of the invention is exactly for the defect for making up prior art, there is provided a kind of high resiliency, high waterproof impervious characteristic, close
Good, the high impervious container fluid sealant of the heat insulation anti-shock aqueouss containing asbestos fibre of durability and preparation method thereof of envelope property.
The present invention is achieved by the following technical solutions：
A kind of impervious container fluid sealant of heat insulation anti-shock aqueouss containing asbestos fibre, which is by the raw material system of following weight parts
：
Polyacrylate dispersion 40-60 of the solid content for 40-50%, polychloroprene latex 5-10 of the solid content for 40-50%, solid content is
The water soluble phenol resin 3-5 of 40-60%, asbestos fibre 10-15, flyash 30-40, Colophonium 3-5, liquid paraffin 2-4, metatitanic acid
Ester coupling agent 3-5, tributyl citrate 3-5, potassium sorbate 0.5-1, Lauryl Alcohol ester 0.5-1, water 10-15.
A kind of preparation method of the impervious container fluid sealant of heat insulation anti-shock aqueouss containing asbestos fibre, including following step
Suddenly：
（1）Polyacrylate dispersion, polychloroprene latex, water soluble phenol resin mix homogeneously are stirred after 1000-1200/min
0.5-1h, obtains component A；
（2）First Colophonium, liquid paraffin and tributyl citrate are mixed and 0.5-1h is stirred after 80-90 DEG C, be subsequently adding metatitanic acid
Ester coupling agent stirs 10-15min in 100-120 DEG C, adds and water is in 1200-1500r/min stirring 0.5-1h after cooling, then plus
0.5-1h is ground after entering asbestos fibre and flyash mix homogeneously, B component is obtained；
（3）After first mixed component A with B component, 1000-1200r/min stirrings 10-15min, is subsequently adding remaining raw material same
Under the conditions of stir 10-15min, obtain final product the impervious container fluid sealant of heat insulation anti-shock aqueouss containing asbestos fibre.
It is an advantage of the invention that：
One aspect of the present invention improves aqueouss by polyacrylate dispersion, polychloroprene latex, water soluble phenol resin are carried out compounding
Elastic, the water-fast anti-permeability performance of fluid sealant and thermal and insulating performance, on the one hand by Colophonium, liquid paraffin and titanate coupling agent with
Filler is blended, and improves the bond strength and water-fast anti-permeability performance of filler and fluid sealant latex, then by asbestos fibre etc.
The addition of raw material, so as to get container fluid sealant have high resiliency, high waterproof impervious characteristic and excellent sealing property concurrently,
There is good heat insulation anti-shock effect simultaneously, durability is high, long service life, environmental protection.
Specific embodiment
A kind of impervious container fluid sealant of heat insulation anti-shock aqueouss containing asbestos fibre, the component by following weight (kg) are former
Material is prepared from：
Solid content is 40% polyacrylate dispersion 40, and solid content is 40% polychloroprene latex 5, and solid content is 40% water solublity
Phenolic resin 3, asbestos fibre 10, flyash 30, Colophonium 3, liquid paraffin 2, titanate coupling agent 3, tributyl citrate 3, mountain
Potassium sorbate 0.5, Lauryl Alcohol ester 0.5, water 10.
A kind of preparation method of the impervious container fluid sealant of heat insulation anti-shock aqueouss containing asbestos fibre, including following step
Suddenly：
（1）Polyacrylate dispersion, polychloroprene latex, water soluble phenol resin mix homogeneously are stirred into 0.5h after 1000/min,
Obtain component A；
（2）First Colophonium, liquid paraffin and tributyl citrate are mixed and 0.5h is stirred after 80 DEG C, be subsequently adding titanate esters coupling
Agent stirs 10min in 100 DEG C, adds and water stirs 0.5h in 1200r/min, add asbestos fibre and flyash simultaneously after cooling
0.5h is ground after mix homogeneously, B component is obtained；
（3）After first mixed component A with B component, 1000r/min stirrings 10min, is subsequently adding under remaining raw material similarity condition and stirs
10min is mixed, the impervious container fluid sealant of heat insulation anti-shock aqueouss containing asbestos fibre is obtained final product.
Fluid sealant the performance test results obtained above are as follows：
Tensile strength：0.36MPa；
Peel strength：3.9MPa；
Elongation at break：337%；
Resistance to water（48h）：It is non-swelling, do not ftracture.
Claims (2)
1. the impervious container fluid sealant of a kind of heat insulation anti-shock aqueouss containing asbestos fibre, it is characterised in which is by following heavy
The raw material of amount part is obtained：
Polyacrylate dispersion 40-60 of the solid content for 40-50%, polychloroprene latex 5-10 of the solid content for 40-50%, solid content is
The water soluble phenol resin 3-5 of 40-60%, asbestos fibre 10-15, flyash 30-40, Colophonium 3-5, liquid paraffin 2-4, metatitanic acid
Ester coupling agent 3-5, tributyl citrate 3-5, potassium sorbate 0.5-1, Lauryl Alcohol ester 0.5-1, water 10-15.
2. the preparation of the impervious container fluid sealant of a kind of heat insulation anti-shock aqueouss containing asbestos fibre according to claim 1
Method, it is characterised in that comprise the following steps：
（1）Polyacrylate dispersion, polychloroprene latex, water soluble phenol resin mix homogeneously are stirred after 1000-1200/min
0.5-1h, obtains component A；
（2）First Colophonium, liquid paraffin and tributyl citrate are mixed and 0.5-1h is stirred after 80-90 DEG C, be subsequently adding metatitanic acid
Ester coupling agent stirs 10-15min in 100-120 DEG C, adds and water is in 1200-1500r/min stirring 0.5-1h after cooling, then plus
0.5-1h is ground after entering asbestos fibre and flyash mix homogeneously, B component is obtained；
（3）After first mixed component A with B component, 1000-1200r/min stirrings 10-15min, is subsequently adding remaining raw material same
Under the conditions of stir 10-15min, obtain final product the impervious container fluid sealant of heat insulation anti-shock aqueouss containing asbestos fibre.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610960774.8A CN106543932A (en) | 2016-10-28 | 2016-10-28 | Impervious container fluid sealant of a kind of heat insulation anti-shock aqueouss containing asbestos fibre and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610960774.8A CN106543932A (en) | 2016-10-28 | 2016-10-28 | Impervious container fluid sealant of a kind of heat insulation anti-shock aqueouss containing asbestos fibre and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106543932A true CN106543932A (en) | 2017-03-29 |
Family
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610960774.8A Pending CN106543932A (en) | 2016-10-28 | 2016-10-28 | Impervious container fluid sealant of a kind of heat insulation anti-shock aqueouss containing asbestos fibre and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106543932A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107163910A (en) * | 2017-06-14 | 2017-09-15 | 合肥市旺友门窗有限公司 | A kind of energy-saving waterproof fluid sealant and preparation method thereof |
| CN107858126A (en) * | 2017-12-12 | 2018-03-30 | 佛山早稻田科技服务有限公司 | A kind of environment-friendly type fluid sealant |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102952512A (en) * | 2011-08-20 | 2013-03-06 | 朱云利 | Preparation method of unsaturated polyester resin sealant |
| CN102952508A (en) * | 2011-08-25 | 2013-03-06 | 张苏侠 | Preparation method of phenolic resin sealant |
| CN102952504A (en) * | 2011-08-25 | 2013-03-06 | 张苏侠 | Preparation method of polyacrylate sealant |
| CN104212389A (en) * | 2014-08-01 | 2014-12-17 | 广州大禹防漏技术开发有限公司 | SEPS weather-resistant building waterproof sealing glue and preparation method thereof |
-
2016
- 2016-10-28 CN CN201610960774.8A patent/CN106543932A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102952512A (en) * | 2011-08-20 | 2013-03-06 | 朱云利 | Preparation method of unsaturated polyester resin sealant |
| CN102952508A (en) * | 2011-08-25 | 2013-03-06 | 张苏侠 | Preparation method of phenolic resin sealant |
| CN102952504A (en) * | 2011-08-25 | 2013-03-06 | 张苏侠 | Preparation method of polyacrylate sealant |
| CN104212389A (en) * | 2014-08-01 | 2014-12-17 | 广州大禹防漏技术开发有限公司 | SEPS weather-resistant building waterproof sealing glue and preparation method thereof |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107163910A (en) * | 2017-06-14 | 2017-09-15 | 合肥市旺友门窗有限公司 | A kind of energy-saving waterproof fluid sealant and preparation method thereof |
| CN107858126A (en) * | 2017-12-12 | 2018-03-30 | 佛山早稻田科技服务有限公司 | A kind of environment-friendly type fluid sealant |
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| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
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| RJ01 | Rejection of invention patent application after publication | ||
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Application publication date: 20170329 |