CN103355651B - Preparation method of bamboo fungus and sparassis crispa freeze-drying ultrafine powder capsules - Google Patents
Preparation method of bamboo fungus and sparassis crispa freeze-drying ultrafine powder capsules Download PDFInfo
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- CN103355651B CN103355651B CN201310289059.2A CN201310289059A CN103355651B CN 103355651 B CN103355651 B CN 103355651B CN 201310289059 A CN201310289059 A CN 201310289059A CN 103355651 B CN103355651 B CN 103355651B
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Abstract
The invention provides a preparation method of bamboo fungus and sparassis crispa freeze-drying ultrafine powder capsules. The preparation method of bamboo fungus and sparassis crispa freeze-drying ultrafine powder capsules comprises the following steps of: taking sorted and pedicle-removed sparassis crispa and bamboo fungus according to the weight ratio of 5:1, cleaning, and crushing; inputting into a pulping machine and pulping; milling mixed pulp obtained through pulping by a colloid mill; placing the mixed pulp after milling pulp into a vacuum freezing and drying machine, freezing, and vacuumizing; then drying so as to enable water in the mixed pulp to be sublimated into steam, and capturing the steam by a cold trap of the vacuum freezing and drying machine, and freezing and drying the mixed pulp; crushing the frozen and dried mixed pulp by an ultrafine crusher, and sieving by a 200-mesh mesh screen so as to obtain frozen and dried powder; packaging the frozen and dried powder into capsule shells, and packaging under an aseptic condition, thereby obtaining bamboo fungus and sparassis crispa freeze-drying ultrafine powder capsule finished products. Through the preparation method provided by the invention, not only can the effective ingredients, active substances and nutritional substances of bamboo fungus and sparassis crispa be stored maximally, but also because of the adding of bamboo fungus, natural preservatives are also provided, the nutritional ingredients of capsules are enriched, so that the capsules are difficult to deteriorate.
Description
[technical field]
The present invention relates to a kind of preparation method of health food, relate in particular to a kind of dictyophora phalloidea Sparassis crispa freeze dried superfines capsule preparation method thereof.
[background technology]
Sparassis crispa is non-pleat pore fungi order, silk ball Cordycepps, a kind of very rare immunological regulation edible and medical fungi of silk ball Pseudomonas, and its protein content is about 12.9%, far above general vegetables, fruit; Sparassis crispa, containing 7 kinds of amino acid/11s, is about 9.3%, A wide selection of colours and designs, and wherein 8 seed amino acids of needed by human account for 33.9% of total amount; ; Contain a large amount of beta glucans, silk ball mykol (Sparasso1) and close glycoprotein (claiming again immune modulator), and except being rich in a large amount of beta glucans, Sparassis crispa also contains a large amount of vitamin, mineral matter and polyphenoils.According to surveying and determination, in Sparassis crispa, the content of hepatocuprein (SOD) occupies first of various edible mushrooms; Modern study confirm Sparassis crispa there is antitumor action, immunoloregulation function, promotion wound healing effect, promote hematopoiesis function, hypoglycemic, regulate blood pressure, blood fat, reduce that cholesterol, antiallergy, promotion collagen produce, the effect such as anti-oxidant.Although the protein of Sparassis crispa, amino acid, vitamin, micro elements needed by human content are all higher, its main functional components is fungi activity polysaccharide.
Dictyophora phalloidea is a kind of famous edible mushroom during Phallales Phallaceae dictyophora phalloidea belongs to, and classifies in history " imperial palace tribute " as, and as state banquet famous dish, be also dietotherapy good merchantable brand modern age simultaneously; It is nutritious, according to surveying and determination in dry dictyophora phalloidea containing protein 19.4%, fat 2.6%, carbohydrate total amount 60.4%, wherein bacterium sugar 4.2%, crude fibre 8.4%, ash content 9.3%.The contained polysaccharide of dictyophora phalloidea be take the different polysaccharide such as glucose, mannose, wood sugar and galactolipin as main, also contain simultaneously multiple to the useful composition of human body as carrotene, thiamine, ascorbic acid, niacin etc.The traditional Chinese medical science thinks, dictyophora phalloidea has very large benifit for strengthening digestive function of spleen and stomach, also has the greasy digestant effect of solution, often ediblely can eliminate the unnecessary fat of stomach wall, has obvious fat-reducing effect.Medical research shows, dictyophora phalloidea belongs to physiological alkalinity food, and long-term taking can regulate aliphatic acid and the hematic acid content in person in middle and old age's human body, has the effect that reduces hypertension and body inner cholesterol.Polysaccharide in dictyophora phalloidea all has certain curative effect at antitumor, anti-inflammatory, anticoagulation, immune stimulatory, reduction blood sugar and enhancing immunology, and AIDS is also had to inhibitory action.In addition, dictyophora phalloidea can be brought into play bacteriostasis in neutrality to alkali condition, and antibacterial substance is stable to high temperature, condition of high voltage, can be used as a kind of natural food preservative.
Vacuum Freezing & Drying Technology is that wet stock or solution are frozen into solid-state at lower temperature (one 10 ℃ 30 ℃ one by one), then in vacuum, (under (1.3-13 handkerchief), make moisture wherein be directly sublimed into gaseous state without liquid state, finally make the dry technology of material dewatering.China is production of raw medicine big country, so the application prospect of Vacuum Freezing & Drying Technology is very wide.Vacuum Freezing & Drying Technology is promoted very fastly in China in recent years, but uses Lyophilisation technique for making fewer on plant, mushroom, especially the application on Sparassis crispa.Because fresh Sparassis crispa water content is greater than 90%, be not easy to deep processing and storage, necessary stored dry; General drying means is all high temperature drying or microwave drying, but active ingredient in fresh Sparassis crispa will be destroyed when temperature surpasses 45 ℃, and in Sparassis crispa, polyoses content can drop to below 10%, and health-care effect is reduced greatly.
Therefore, can work out and a kind ofly can guarantee Sparassis crispa and dictyophora phalloidea active constituent content, at utmost reduce polysaccharide loss, the health products preparation method that can extend the shelf life is again practitioner's letter major issue to be solved simultaneously.
[summary of the invention]
Technical problem to be solved by this invention is to provide a kind of dictyophora phalloidea Sparassis crispa freeze dried superfines capsule preparation method thereof.
The present invention solves the problems of the technologies described above by the following technical programs: a kind of dictyophora phalloidea Sparassis crispa freeze dried superfines capsule preparation method thereof, specifically comprises following operation:
(1) pluck respectively Sparassis crispa, dictyophora phalloidea sorting and remove the base of a fruit, by the weight ratio of 5:1, get sorting afterwards and go Sparassis crispa and the dictyophora phalloidea after the base of a fruit, and clean and fragmentation; Then by the Sparassis crispa after fragmentation and dictyophora phalloidea input beater, and add with the pure water of the weight such as dictyophora phalloidea and pull an oar; Then by the mixing slurry colloid mill defibrination of the Sparassis crispa dictyophora phalloidea obtaining after making beating;
(2) the mixing slurry after defibrination is placed in vacuum freeze drier, by 8～12kg/m
2stone, and in 2 hours～4 hours, the temperature of mixing slurry is down to-15 ℃～-27 ℃, make to mix slurry and freeze; Then in 30 minutes～1 hour, the condenser temperature of vacuum freeze drier is down to-30 ℃～-35 ℃; Again vacuum freeze drier is evacuated to 0.6mmhg～1.0mmhg; Dry afterwards that the water sublimate that makes to mix in slurry becomes steam and by the cold trap trapping of vacuum freeze drier, make to mix slurry freeze-drying;
Wherein, the temperature and time of oven dry is specially: drying initial temperature is 120 ℃, keeps temperature 3 hours; In 1 hour, be down to 100 ℃ from 120 ℃, and locate to keep temperature 1 hour at 100 ℃; In 1 hour, from 100 ℃, drop to 80 ℃; In 0.5 hour, drop to 60 ℃ from 80 ℃, and locate to keep temperature 5.5 hours at 60 ℃;
(3) the mixing slurry after freeze-drying is adopted to ultramicro grinding crusher machine, cross 200 order mesh screens to obtain freeze-dried powder, afterwards freeze-dried powder is incapsulated and under aseptic condition, pack and obtain described dictyophora phalloidea Sparassis crispa freeze dried superfines capsule finished product.
Further, this preparation method also comprises following operation: the dictyophora phalloidea Sparassis crispa freeze dried superfines capsule finished product of gained after packing is adopted to co-60 radiation.
Further, described capsule shells is No. 1 capsule shells, and in every seed lac softgel shell, packs freeze-dried powder described in 290mg into.
The beneficial effect of a kind of dictyophora phalloidea Sparassis crispa of the present invention freeze dried superfines capsule preparation method thereof is: the health products that obtain by this preparation method are that dictyophora phalloidea Sparassis crispa freeze dried superfines capsule not only can larger limit have been preserved active ingredient, active material and the nutriment of dictyophora phalloidea and Sparassis crispa, and largely, kept the contained polysaccharide of Sparassis crispa, adding because of dictyophora phalloidea also, natural antiseptic agent is also provided when having enriched nutritional labeling, make capsule not perishable, can carry, edible at any time, facilitate feasible.
[specific embodiment]
A kind of dictyophora phalloidea Sparassis crispa of the present invention freeze dried superfines capsule preparation method thereof, specifically comprises following operation: (1) is plucked respectively Sparassis crispa, dictyophora phalloidea sorting and removed the base of a fruit, gets sorting afterwards and goes Sparassis crispa and the dictyophora phalloidea after the base of a fruit, and clean and fragmentation by the weight ratio of 5:1; Then by the Sparassis crispa after fragmentation and dictyophora phalloidea input beater, and add with the pure water of the weight such as dictyophora phalloidea and pull an oar; Then by the mixing slurry colloid mill defibrination of the Sparassis crispa dictyophora phalloidea obtaining after making beating; (2) the mixing slurry after defibrination is placed in vacuum freeze drier, by 8～12kg/m
2stone, and in 2 hours～4 hours, the temperature of mixing slurry is down to-15 ℃～-27 ℃, make to mix slurry and freeze; Then in 30 minutes～1 hour, the condenser temperature of vacuum freeze drier is down to-30 ℃～-35 ℃; Again vacuum freeze drier is evacuated to 0.6mmhg～1.0mmhg; Dry afterwards that the water sublimate that makes to mix in slurry becomes steam and by the cold trap trapping of vacuum freeze drier, make to mix slurry freeze-drying; Wherein, the temperature and time of oven dry is specially: drying initial temperature is 120 ℃, keeps temperature 3 hours; In 1 hour, be down to 100 ℃ from 120 ℃, and locate to keep temperature 1 hour at 100 ℃; In 1 hour, from 100 ℃, drop to 80 ℃; In 0.5 hour, drop to 60 ℃ from 80 ℃, and locate to keep temperature 5.5 hours at 60 ℃; (3) the mixing slurry after freeze-drying is adopted to ultramicro grinding crusher machine, cross 200 order mesh screens to obtain freeze-dried powder, afterwards freeze-dried powder is incapsulated to shell and under aseptic condition, pack and obtain described dictyophora phalloidea Sparassis crispa freeze dried superfines capsule finished product.
In addition, in order to extend the shelf-life of the capsule finished product that the present invention prepares, can packing after the dictyophora phalloidea Sparassis crispa freeze dried superfines capsule finished product of gained adopt co-60 radiation; Described capsule shells is No. 1 capsule shells, and in every seed lac softgel shell, packs freeze-dried powder described in 290mg into.
In order better method of the present invention to be set forth to explanation, the present invention has exemplified following embodiment.
Embodiment 1
Pluck fresh bamboo fungi and Sparassis crispa, and sorting goes the base of a fruit to remove root, standby; 20 kilograms of fresh bamboo fungis and the 100 kilograms of Sparassis crispas of removing root are cleaned up with running water and fragmentation; Then the Sparassis crispa after fragmentation and dictyophora phalloidea are put in beater, added 20 kilograms of pure water making beating; By the mixing slurry colloid mill defibrination of 140 kilograms of dictyophora phalloidea Sparassis crispas after making beating; Mixing slurry after defibrination is placed in vacuum freeze drier (Lima, Xiamen freezing equipment Co., Ltd, UFD-180 model), by 12kg/m
2pave; With 4 hours, the temperature of mixing slurry is down to one 15 ℃, makes to mix slurry freezing icing; Then in 30 minutes, just the condenser temperature of vacuum freeze drier is down to one 30 ℃, opens vacuum equipment, and vacuum freeze drier is vacuumized and reaches 0.8mmhg; Dry afterwards that the water sublimate that makes to mix in slurry becomes steam and by the cold trap trapping of vacuum freeze drier, make to mix slurry freeze-drying; Mixing slurry after freeze-drying is adopted to ultramicro grinding crusher machine, cross 200 order mesh screens to obtain freeze-dried powder, afterwards freeze-dried powder is incapsulated to shell and under aseptic condition, pack and obtain described dictyophora phalloidea Sparassis crispa freeze dried superfines capsule finished product.
Embodiment 2
Pluck fresh bamboo fungi and Sparassis crispa, and sorting goes the base of a fruit to remove root, standby; 20 kilograms of fresh bamboo fungis and the 100 kilograms of Sparassis crispas of removing root are cleaned up with running water and fragmentation; Then the Sparassis crispa after fragmentation and dictyophora phalloidea are put in beater, added 20 kilograms of pure water making beating; By the mixing slurry colloid mill defibrination of 140 kilograms of dictyophora phalloidea Sparassis crispas after making beating; Mixing slurry after defibrination is placed in vacuum freeze drier (Lima, Xiamen freezing equipment Co., Ltd, UFD-180 model), by 10kg/m
2pave; With 3 hours, the temperature of mixing slurry is down to one 27 ℃, makes to mix slurry freezing icing; Then in 45 minutes, just the condenser temperature of vacuum freeze drier is down to one 33 ℃, opens vacuum equipment, and vacuum freeze drier is vacuumized and reaches 0.6mmhg; Dry afterwards that the water sublimate that makes to mix in slurry becomes steam and by the cold trap trapping of vacuum freeze drier, make to mix slurry freeze-drying; Mixing slurry after freeze-drying is adopted to ultramicro grinding crusher machine, cross 200 order mesh screens to obtain freeze-dried powder, afterwards freeze-dried powder is incapsulated to shell and under aseptic condition, pack and obtain described dictyophora phalloidea Sparassis crispa freeze dried superfines capsule finished product.
Embodiment 3
Pluck fresh bamboo fungi and Sparassis crispa, and sorting goes the base of a fruit to remove root, standby; 7 kilograms of fresh bamboo fungis and the 35 kilograms of Sparassis crispas of removing root are cleaned up with running water and fragmentation; Then the Sparassis crispa after fragmentation and dictyophora phalloidea are put in beater, added 7 kilograms of pure water making beating; By the mixing slurry colloid mill defibrination of 49 kilograms of dictyophora phalloidea Sparassis crispas after making beating; Mixing slurry after defibrination is placed in vacuum freeze drier (Lima, Xiamen freezing equipment Co., Ltd, UFD-180 model), by 8kg/m
2pave; With 2 hours, the temperature of mixing slurry is down to one 20 ℃, makes to mix slurry freezing icing; Then in 1 hour, just the condenser temperature of vacuum freeze drier is down to one 35 ℃, opens vacuum equipment, and vacuum freeze drier is vacuumized and reaches 1.0mmhg; Dry afterwards that the water sublimate that makes to mix in slurry becomes steam and by the cold trap trapping of vacuum freeze drier, make to mix slurry freeze-drying; Mixing slurry after freeze-drying is adopted to ultramicro grinding crusher machine, cross 200 order mesh screens to obtain freeze-dried powder, afterwards freeze-dried powder is incapsulated to shell and under aseptic condition, pack and obtain described dictyophora phalloidea Sparassis crispa freeze dried superfines capsule finished product.
It should be noted that, actual temp and the time of in the various embodiments described above, drying are: drying initial temperature is 120 ℃, keep temperature 3 hours; In 1 hour, be down to 100 ℃ from 120 ℃, and locate to keep temperature 1 hour at 100 ℃; In 1 hour, from 100 ℃, drop to 80 ℃; In 0.5 hour, drop to 60 ℃ from 80 ℃, and locate to keep temperature 5.5 hours at 60 ℃.
To sum up, the health products that obtain by preparation method of the present invention are that dictyophora phalloidea Sparassis crispa freeze dried superfines capsule not only can larger limit have been preserved active ingredient, active material and the nutriment of dictyophora phalloidea and Sparassis crispa, and largely, kept the contained polysaccharide of Sparassis crispa, adding because of dictyophora phalloidea also, natural antiseptic agent is also provided when having enriched nutritional labeling, has made capsule not perishable, can carry, edible at any time, facilitate feasible.
Claims (3)
1. a dictyophora phalloidea Sparassis crispa freeze dried superfines capsule preparation method thereof, is characterized in that: specifically comprise following operation:
(1) pluck respectively Sparassis crispa, dictyophora phalloidea sorting and remove the base of a fruit, by the weight ratio of 5:1, get sorting afterwards and go Sparassis crispa and the dictyophora phalloidea after the base of a fruit, and clean and fragmentation; Then by the Sparassis crispa after fragmentation and dictyophora phalloidea input beater, and add with the pure water of the weight such as dictyophora phalloidea and pull an oar; Then by the mixing slurry colloid mill defibrination of the Sparassis crispa dictyophora phalloidea obtaining after making beating;
(2) the mixing slurry after defibrination is placed in vacuum freeze drier, by 8～12kg/m
2stone, and in 2 hours～4 hours, the temperature of mixing slurry is down to-15 ℃～-27 ℃, make to mix slurry and freeze; Then in 30 minutes～1 hour, the condenser temperature of vacuum freeze drier is down to-30 ℃～-35 ℃; Again vacuum freeze drier is evacuated to 0.6mmhg～1.0mmhg; Dry afterwards that the water sublimate that makes to mix in slurry becomes steam and by the cold trap trapping of vacuum freeze drier, make to mix slurry freeze-drying;
Wherein, the temperature and time of oven dry is specially: drying initial temperature is 120 ℃, keeps temperature 3 hours; In 1 hour, be down to 100 ℃ from 120 ℃, and locate to keep temperature 1 hour at 100 ℃; In 1 hour, from 100 ℃, drop to 80 ℃; In 0.5 hour, drop to 60 ℃ from 80 ℃, and locate to keep temperature 5.5 hours at 60 ℃;
(3) the mixing slurry after freeze-drying is adopted to ultramicro grinding crusher machine, cross 200 order mesh screens to obtain freeze-dried powder, afterwards freeze-dried powder is incapsulated to shell and under aseptic condition, pack and obtain described dictyophora phalloidea Sparassis crispa freeze dried superfines capsule finished product.
2. a kind of dictyophora phalloidea Sparassis crispa freeze dried superfines capsule preparation method thereof according to claim 1, is characterized in that: also comprise following operation: the dictyophora phalloidea Sparassis crispa freeze dried superfines capsule finished product of gained after packing is adopted to co-60 radiation.
3. a kind of dictyophora phalloidea Sparassis crispa freeze dried superfines capsule preparation method thereof according to claim 1, is characterized in that: described capsule shells is No. 1 capsule shells, and in every seed lac softgel shell, packs freeze-dried powder described in 290mg into.
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| CN106262798A (en) * | 2016-10-10 | 2017-01-04 | 贵州高山生物科技有限公司 | Dictyophora rubrovalvata volva dry powder and preparation method and application |
| CN114698831A (en) * | 2022-04-28 | 2022-07-05 | 贵州省现代农业发展研究所(贵州省现代农村发展研究中心、贵州省农村经济与社会发展科学研究所、贵州省农产品加工研究所) | Instant bamboo fungus flavor nutrition powder for reducing cholesterol and preparation method thereof |
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| CN1686495A (en) * | 2005-03-22 | 2005-10-26 | 贵州三力制药有限责任公司 | Soft capsule using Zhushen fungus as raw material and its preparation method |
| CN101703530A (en) * | 2009-06-08 | 2010-05-12 | 上海荷仙菇生物科技股份有限公司 | Mixed fungus ultrafine powder and preparation method thereof |
| CN102919832A (en) * | 2012-11-01 | 2013-02-13 | 黑龙江省麒麟工贸公司 | Preparation method of health care sparassis crispa capsule |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| JP2004290156A (en) * | 2003-03-28 | 2004-10-21 | Unitika Ltd | Enzymically treated mushroom product of sparassis crispa, and food and drink therefrom |
| GB0421520D0 (en) * | 2004-09-28 | 2004-10-27 | Qinetiq Ltd | Frequency modulated continuous wave (FMCW) radar having improved frquency sweep linearity |
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| CN1686495A (en) * | 2005-03-22 | 2005-10-26 | 贵州三力制药有限责任公司 | Soft capsule using Zhushen fungus as raw material and its preparation method |
| CN101703530A (en) * | 2009-06-08 | 2010-05-12 | 上海荷仙菇生物科技股份有限公司 | Mixed fungus ultrafine powder and preparation method thereof |
| CN102919832A (en) * | 2012-11-01 | 2013-02-13 | 黑龙江省麒麟工贸公司 | Preparation method of health care sparassis crispa capsule |
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